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Diamond-like carbon (DLC) is a promising new wall coating material for use in applications with Ultracold Neutrons (UCN). It can potentially replace the toxic beryllium which has been widely used for the storage and transport of UCN. Our aim is to produce DLC-coated neutron guide tubes of up to 1.2 m length with a Pulsed Laser Deposition (PLD) setup which is currently under construction. In order to find optimal process parameters and appropriate settings for the tube coating facility, we are carrying out a research program which includes the production and characterization of DLC films on small test samples. The characterization of the test samples is done by Raman spectroscopy, X-ray Photoelectron Spectroscopy (XPS) and Neutron Reflectometry. We report on first results from the test samples with sp 3 fractions up to 55% and give an overview of the tube coating setup.

Solid deuterium (sD2) will be used for the production of ultra-cold neutrons (UCN) in a new generation of UCN sources. Scattering cross sections of UCN in sD2 determine the source yield but until now have not been investigated. We report first results from transmission and scattering experiments with cold, very cold and ultra-cold neutrons on sD2 along with light transmission and Raman scattering studies showing the influence of the sD2 crystal properties.

The production rates of ultracold neutrons (UCN) from cold neutrons on gaseous, liquid, and solid deuterium targets have been measured. The comparison of the measured and calculated UCN production on gaseous ${}^{2}{H}_{2}$ is used to calibrate the simulated target extraction and transport efficiencies of the experimental apparatus. The production cross section in solid ${}^{2}{H}_{2}$ at 8 K for UCN with energies between 0 and 250 neV is ${R}_{\mathrm{solid},8 K}={\ensuremath{\sigma}}_{\mathrm{solid},8 K}^{\mathrm{CN}\ensuremath{\rightarrow}\mathrm{UCN}} \ensuremath{\rho}=(1.11\ifmmode\pm\else\textpm\fi{}0.23)\ifmmode\times\else\texttimes\fi{}{10}^{\ensuremath{-}8}\phantom{\rule{0.3em}{0ex}}{\mathrm{cm}}^{\ensuremath{-}1}$. This value is consistent with other experiments in which UCN had been extracted from ${}^{2}{H}_{2}$. The value also agrees with calculations using the incoherent approximation and a simple Debye model and corroborates predictions for UCN densities expected at the high-intensity UCN source at the Paul Scherrer Institut. The temperature dependence of the UCN production in solid ${}^{2}{H}_{2}$ down to 8 K can be explained within the same model when multiple-phonon excitation is included.