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In this study, new ZnO/TEMs composites were prepared using the electrostatic gravitational method, which combines the high reflectivity of ZnO with the low thermal conductivity of TEMs to create materials with excellent thermal insulation and heat preservation properties. The initial test results indicate that the ZnO‐coated TEMs are effective in blocking thermal radiation from sunlight, with thermal conductivity of 0.0523 W/m ⋅ K for the ZnO/TEMs microsphere coating. In addition, the internal and external temperature difference of ZnO/TEM‐C 1200 is 7 °C lower than that of cotton fabric under an optical power of 350 mW/cm2. Moreover, the ZnO/TEM‐C 1200 has a UPF value of up to 1894 and a total solar reflectance of 81.40 % in the 200–2500 nm wavelength range. These findings demonstrate the potential of ZnO/TEMs composites for use in thermal insulation and UV protection applications. [ABSTRACT FROM AUTHOR]

Thermally expandable microspheres (TEMs) are hollow polymeric particles in which a blowing gas has been encapsulated. This property makes them excellent for thermal insulation applications, such as lightweight fillers. This study has developed a viable technology for further improving thermal insulation properties in the field that needs excellent thermal insulation of textile fabrics. The ATO/TEMs composites were designed and prepared to reduce sunlight radiation by the charge gravity method. The test results showed that the ATO‐coated TEMs effectively block thermal radiation from sunlight. The temperature difference between ATO/TEMs treated cotton and the uncoated cotton fabric was 9 °C, and the thermal conductivity coatings were 0.0432 W/m⋅K. The UPF value of ATO/TEMs (ILs) coated cotton fabric is 440, significantly higher than pure cotton. This approach can provide insight into the design of high‐performance solar insulation composite structures. [ABSTRACT FROM AUTHOR]