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Background: The stability of implant-abutment connection is crucial to minimize mechanical and biological complications. Therefore, an assessment of the microgap behavior and abutment displacement in different implant-abutment designs was performed., Methods: Four implant systems were tested, three with a conical implant-abutment connection based on friction fit and a cone angle < 12 ° (Medentika, Medentis, NobelActive) and a system with an angulated connection (< 40°) (Semados). In different static loading conditions (30 N - 90º, 100 N - 90º, 200 N - 30º) the microgap and abutment displacement was evaluated using synchrotron-based microtomography and phase-contrast radioscopy with numerical forward simulation of the optical Fresnel propagation yielding an accuracy down to 0.1 μm., Results: Microgaps were present in all implant systems prior to loading (0.15-9 μm). Values increased with mounting force and angle up to 40.5 μm at an off axis loading of 100 N in a 90° angle., Conclusions: In contrast to the implant-abutment connection with a large cone angle (45°), the conical connections based on a friction fit (small cone angles with < 12°) demonstrated an abutment displacement which resulted in a deformation of the outer implant wall. The design of the implant-abutment connection seems to be crucial for the force distribution on the implant wall which might influence peri-implant bone stability., (© 2024. The Author(s).)

Objective: This study evaluates the effect of dynamic-loading on the microgap of the IAC when different supratructure heights are applied., Materials and Methods: Forty-eight dental implants (24 each of butt-joint (H) and internal-conical connections (C)) were tested in this study. Each group was further divided into three groups (n = 8) according to the applied suprastructure height (H1, C1: 10 mm, H2, C2: 14 mm and H3, C3: 18 mm). All specimens were subjected to cyclic loading in a chewing-simulator with a load of 98 N for 5 × 10 6 chewing cycles. The microgap at the IAC was inspected before and after loading, using synchrotron-based micro computed tomography (SRμCT) and light microscopy (LM)., Results: SRμCT revealed an internal microgap range between 0.26 μm and 0.5 μm in the group C, whereas the group H exhibited a microgap range between 0.26 μm and 0.47 μm prior to loading. After chewing simulation, a smaller microgap size in all groups was detected ranging from 0.11 μm to 0.26 μm (group C: 0.11μm-0.26 μm; group H: 0.21μm-0.25 μm). The LM investigation showed mean microgap values at the outer IAC junction before loading from 5.8 μm to 11.3 μm and from 3.9 μm to 7.2 μm after loading. All specimens exhibited a vertical intrusion displacement of the abutment., Conclusion: Regardless of the crown height, the microgap between the abutment and implant systematically decreased after loading in both butt-joint and internal-conical connections., (Copyright © 2021 Elsevier Ltd. All rights reserved.)

The purpose of this study was to describe a refined method using high-resolution synchrotron radiation microtomography (SRmicro-CT) to evaluate osseointegration and peri-implant bone volume fraction after titanium dental implant insertion. SRmicro-CT is considered gold standard evaluating bone microarchitecture. Its high resolution, high contrast, and excellent high signal-to-noise-ratio all contribute to the highest spatial resolutions achievable today. Using SRmicro-CT at a voxel size of 5 μm in an experimental goat mandible model, the peri-implant bone volume fraction was found to quickly increase to 50% as the radial distance from the implant surface increased, and levelled out to approximately 80% at a distance of 400 μm. This method has been successful in depicting the bone and cavities in three dimensions thereby enabling us to give a more precise answer to the fraction of the bone-to-implant contact compared to previous methods., (Copyright © 2015 European Association for Cranio-Maxillo-Facial Surgery. Published by Elsevier Ltd. All rights reserved.)

The ESRF synchrotron beamline ID22, dedicated to hard X-ray microanalysis and consisting of the combination of X-ray fluorescence, X-ray absorption spectroscopy, diffraction and 2D/3D X-ray imaging techniques, is one of the most versatile instruments in hard X-ray microscopy science. This paper describes the present beamline characteristics, recent technical developments, as well as a few scientific examples from recent years of the beamline operation. The upgrade plans to adapt the beamline to the growing needs of the user community are briefly discussed.

The investigation of lithium-ion battery failures is a major challenge for personnel and equipment due to the associated hazards (thermal reaction, toxic gases and explosions). To perform such experiments safely, a battery abuse-test chamber has been developed and installed at the microtomography beamline ID19 of the European Synchrotron Radiation Facility (ESRF). The chamber provides the capability to robustly perform in situ abuse tests through the heatresistant and gas-tight design for flexible battery geometries and configurations, including single-cell and multi-cell assemblies. High-speed X-ray imaging can be complemented by supplementary equipment, including additional probes (voltage, pressure and temperature) and thermal imaging. Together with the test chamber, a synchronization graphical user interface was developed, which allows an initial interpretation by time-synchronous visualization of the acquired data. Enabled by this setup, new meaningful insights can be gained into the internal processes of a thermal runaway of current and future energystorage devices such as lithium-ion cells. [ABSTRACT FROM AUTHOR]

In situ investigations of cracks propagating at up to 2.5 km s-1 along an (001) plane of a silicon single crystal are reported, using X-ray diffraction megahertz imaging with intense and time-structured synchrotron radiation. The studied system is based on the Smart Cut process, where a buried layer in a material (typically Si) is weakened by microcracks and then used to drive a macroscopic crack (10-1 m) in a plane parallel to the surface with minimal deviation (10-9 m). A direct confirmation that the shape of the crack front is not affected by the distribution of the microcracks is provided. Instantaneous crack velocities over the centimetre-wide field of view were measured and showed an effect of local heating by the X-ray beam. The post-crack movements of the separated wafer parts could also be observed and explained using pneumatics and elasticity. A comprehensive view of controlled fracture propagation in a crystalline material is provided, paving the way for the in situ measurement of ultra-fast strain field propagation. [ABSTRACT FROM AUTHOR]

Two sections of heat-treated (HT) and non-heat-treated (NHT) Cable-in-Conduit Conductor (CICC) of a design similar to the ITER tokomak have been imaged using very high energy X-ray tomography at the ESRF beamline ID19. The sample images were collected at four temperatures down to 77 K. These results showed a greater degree of movement, bundle distortion and touching strands in the NHT sample. The HT sample showed non-linear movements with temperature especially close to 77 K; increasing non-circularity of the superconducting fibre bundles towards the periphery of the CICC, and touching bundles throughout the CICC. The images have highlighted where future design might improve potential weakness, in particular at the outer perimeters of the conductor and the individual sub-cable, 'petal' wraps. [ABSTRACT FROM AUTHOR]

A hard X-ray transparent triaxial deformation apparatus, called HADES, has been developed by Sanchez Technologies and installed on the microtomography beamline ID19 at the European Radiation Synchrotron Facility (ESRF). This rig can be used for time-lapse microtomography studies of the deformation of porous solids (rocks, ceramics, metallic foams) at conditions of confining pressure to 100 MPa, axial stress to 200 MPa, temperature to 250°C, and controlled aqueous fluid flow. It is transparent to high-energy X-rays above 60 keV and can be used for in situ studies of coupled processes that involve deformation and chemical reactions. The rig can be installed at synchrotron radiation sources able to deliver a high-flux polychromatic beam in the hard X-ray range to acquire tomographic data sets with a voxel size in the range 0.7-6.5 µm in less than two minutes. [ABSTRACT FROM AUTHOR]

Synchrotron real-time radioscopy and in situ microtomography are the only techniques providing direct visible information on a micrometre scale of local deformation in the implant-abutment connection (IAC) during and after cyclic loading. The microgap formation at the IAC has been subject to a number of studies as it has been proposed to be associated with long-term implant success. The next step in this scientific development is to focus on the in situ fatigue procedure of two-component dental implants. Therefore, an apparatus has been developed which is optimized for the in situ fatigue analysis of dental implants. This report demonstrates both the capability of in situ radioscopy and microtomography at the ID19 beamline for the study of cyclic deformation in dental implants. The first results show that it is possible to visualize fatigue loading of dental implants in real-time radioscopy in addition to the in situ fatigue tomography. For the latter, in situ microtomography is applied during the cyclic loading cycles in order to visualize the opening of the IAC microgap. These results concur with previous ex situ studies on similar systems. The setup allows for easily increasing the bending force, to simulate different chewing situations, and is, therefore, a versatile tool for examining the fatigue processes of dental implants and possibly other specimens. [ABSTRACT FROM AUTHOR]

The application of synchrotron radiation X-ray computed micro-tomography (SR X-μCT) as a non-invasive approach to the microstructural investigation of Portland cement binders during hydration is presented. The two- and three-dimensional µm-scale imaging of undisturbed samples at hydration ages from ~1.5 h to 3 days is used to obtain a direct visualization of the spatial and temporal relationships between different cement paste components. The microstructural evolution of two cementitious systems during the early stages of hydration is successfully monitored from the comparison of tomographic slices and volumes, clearly showing the progressive growth of hydration phases; the changes in the amount of porosity and unreacted clinker are also quantified. Some critical issues related to the experimental setup and data processing are addressed and discussed as well. Furthermore, a simple procedure to estimate the mean X-ray absorption coefficient of cement pastes from X-ray radiographs is illustrated. The results confirm the potentialities of synchrotron-based X-ray computed micro-tomography for the three-dimensional investigation of µm-scale modifications in hydrating cement pastes with an adequate time resolution, thus providing a real in-situ monitoring of the microstructural evolution of such complex materials. [ABSTRACT FROM AUTHOR]

In Europe, there had previously been a series of synchrotron X-ray computed tomography (XCT) workshops, so-called "Beamline Jockey Days" workshops, organized by national synchrotron radiation facilities. In this virtual workshop, we shared the experience of beamline and computational scientists directly involved with operation, presenting the current pipeline for data acquisition and reconstruction at the XCT beamlines. The virtual workshop on "X-ray Tomography at Synchrotron Facilities: Pipeline for Data Acquisition and Reduction" was held February 22-26, 2021, hosted by Elettra Sincrotrone Trieste (Italy) and organized through a joint collaboration between the Advanced Light Source (USA), the Advanced Photon Source (USA), the Diamond Light Source (UK), the European Synchrotron Radiation Facility (France), and Elettra Sincrotrone Trieste (Italy). [Extracted from the article]

Deformation of the first crystal of an X-ray monochromator under the heat load of a high-power beam, commonly referred to as `heat bump', is a challenge frequently faced at synchrotron beamlines. Here, quantitative measurements of the deformations of an externally water-cooled silicon (111) double-crystal monochromator tuned to a photon energy of 17.6 keV are reported. These measurements were made using two-dimensional hard X-ray grating interferometry, a technique that enables in situ at-wavelength wavefront investigations with high angular sensitivity. The observed crystal deformations were of the order of 100 nm in the meridional and 5 nm in the sagittal direction, which lead to wavefront slope errors of up to 4 µrad in the meridional and a few hundred nanoradians in the sagittal direction. [ABSTRACT FROM AUTHOR]

X-ray detector systems are powerful tools: in combination with tomographic methods they provide volumetric data of samples in a non-destructive manner which is of high interest for, e.g., biology, medicine or materials research. The detector able to provide images with submicrometer spatial resolution frequently consists of a scintillator screen, light microscopy optics and a digital camera. Here, the scintillator converts the X-rays into a visible light image which is projected onto the camera by the light optics. In order to perform high resolution imaging Single Crystal Film (SCF) scintillators 1 μm to 30 μm thin are required due to the limited depth of focus of the microscopy optics. Thin SCFs can be obtained via liquid phase epitaxy (LPE). A drawback is that a detector working with SCFs suffers from low efficiency (2% at 50 keV) owing to their limited thickness. The detective quantum efficiency (DQE) is here mainly limited by the low ab- sorption of X-rays and the light yield in the thin scintillator layer. Performances, i.e absorption, light yield, afterglow of operational systems at the European Synchrotron Radiation Facility (ESRF) using YAG:Ce (Y3Al5O12:Ce), LAG:Eu (Lu3Al5O12:Eu) and GGG:Eu (Gd3 Ga5O12 :Eu) scintillators [1] will be presented and compared to new LSO:Tb (Lu2SiO5 :Tb) scintillators developed in the framework of an European project [2], [3] A new concept to improve the efficiency of detection in the 20 keV - 40 keV energy range with 1 μm spatial resolution will be presented. This concept based on multilayer scintillators is realised by the LPE process as well. First results will be illustrated with X-ray images and will demonstrate the absorption efficiency improvement of the X-ray detector. The expected performance is 7 times better than the LAG-based scintillators. [ABSTRACT FROM AUTHOR]

Prevention and mitigation of hazardous battery failure scenarios can be achieved through the integration of different safety systems. These mechanisms are routinely evaluated post-testing in a static fashion but lack insights to their dynamic behavior. However, thanks to fast X-ray imaging one can assess the function of these safety mechanisms in-situ. In this work, micro batteries equipped with a combined venting and current interruption mechanism have been subjected to abuse testing in combination with synchrotron high-speed X-ray imaging. Acquired radiography reveals that the current interrupting system was not always activated as described by the manufacturer, and thus provides insights into potential improvements of the system. In addition, the cell was tested in a different configuration where this mechanism was impeded and we conclude that in-situ visualization with X-ray imaging is a crucial tool for validation of safety mechanisms integrated into batteries. • We show that synchrotron high-speed X-ray imaging is a valuable tool for in-situ evaluation of integrated safety mechanisms. • We investigated the dependence of the cell state of charge on the function of safety mechanisms and found no difference in their activation reliance. • We conducted tests on the cell in various configurations, including one where the cell was pressed between two surfaces and blocked the safety vent. In this particular configuration, we found that the cell reached higher failure temperatures, thus highlighting the importance of battery orientation in device design. • We found that the CID was not activated as expected in any of the cases. [ABSTRACT FROM AUTHOR]

The present study demonstrates experimental evidence of subsurface mesoscale damage initiation and evolution in angle-ply CFRP laminates under high strain-rate loading at low temperatures using synchrotron-based X-ray MHz radiography. A bespoke set of loading, temperature control and in-situ X-ray imaging systems were applied to simultaneously correlate high strain-rate mechanical response with observed subsurface damage in a time-resolved manner. The results demonstrate that independent of temperature, damage evolved following a specific sequence; firstly intra-ply shear cracking along the fibre direction, developing into multi-layer cracking with continued deformation, and finally culminating in inter-ply delamination and complete failure of the specimen. The timescale for this sequence, however, was observed to strongly depend upon temperature, with low temperatures resulting in more rapid damage evolution and loss of mechanical strength. [ABSTRACT FROM AUTHOR]

[Display omitted] • Local mechanical tests of Al/Cu welded joints by MPW under high strain rates. • In-situ damages measurements with X-ray radiography under synchrotron beam. • Different interface evolution of aluminum/copper samples are observed. • Visualization of cracks on the Al/Cu joints along the interface by microtomography. Magnetic Pulse Welding (MPW) is a method of growing interest allowing the joining of dissimilar materials such as aluminum and copper. The global mechanical properties of the joint are often evaluated with conventional tests, using the fully welded joint. However, these cannot elucidate the local mechanical properties of the joint or its interface when subjected to high strain rates loads. Cubic samples of Al/Cu have been designed and extracted from MPW joints, in order to locally characterize the mechanical properties. Samples were exposed to high strain-rate loading using the Split-Hopkinson Pressure Bar (SHPB) coupled to ultra-fast synchrotron X-ray radiography in order to investigate related failure processes in-situ. The measurements of the interface evolution were related to the macroscopic applied load. In addition, synchrotron microtomography was performed on the samples before mechanical deformation. Aside from the feasibility proof, this work provides, for the first time, the correlation of the interfacial opening evolution and the influence of pre-existing cracks of the weld. It is observed that, the pre-existing cracks at the interface correspond to the initiation sites of interfacial separation between the two dissimilar metals. [ABSTRACT FROM AUTHOR]

The relationship between the dynamic mechanical properties of stony meteorites and their microstructures was investigated in-situ for an L-type ordinary chondrite using a split-Hopkinson pressure bar apparatus and ultra-high speed phase-contrast X-ray radiography at the European Synchrotron Radiation Facility (ESRF). Synchrotron X-ray microtomography (μ CT) was performed both prior to and immediately following dynamic compression to correlate key structural features between the initial microstructure and recovered fragments as well as to identify the leading mechanisms for fracture and fragmentation. Real-time visualisation of damage evolution in the specimens revealed the very first cracks to be initiated at the sites of FeNi-metal nodules. These cracks propagated rapidly through the largest group of chondrules (the porphyritic olivine type chondrules) along the loading direction, which led to the formation of column-like fragments. μ CT analysis of the collected fragments confirmed the dominant mode of fracture to be transgranular with a clear link between FeNi-metal nodule statistics and the size distribution of fragments, emphasising their role in mechanical failure and fragmentation process. The resulting fragmentation was used to validate the predictions of brittle fragmentation models, and found to be in good agreement with the laboratory-scale impacts. In turn, these models can help unravel the consequences of impact-induced fragmentation processes that have helped shape the solar system. • Dynamic mechanical properties of an L-type ordinary chondrite are investigated. • Synchrotron X-ray radiography and microtomography results are presented. • Key microstructural features are identified and linked with fragmentation and strength measurements. • Characteristic fragments sizes for planetary-scale impact events are explored. [ABSTRACT FROM AUTHOR]

[Display omitted] • Synchrotron microtomography visualizes tooth movements under compressive load in a non-human primate. • Pressure dominated areas concur with wider periodontal spaces and more vasculature. • Upper and lower molars experience downward tipping motion under load. Mammalian teeth have to sustain repetitive and high chewing loads without failure. Key to this capability is the periodontal ligament (PDL), a connective tissue containing a collagenous fibre network which connects the tooth roots to the alveolar bone socket and which allows the teeth to move when loaded. It has been suggested that rodent molars under load experience a screw-like downward motion but it remains unclear whether this movement also occurs in primates. Here we use synchroton micro-computed tomography paired with an axial loading setup to investigate the form-function relationship between tooth movement and the morphology of the PDL space in a non-human primate, the mouse lemur (Microcebus murinus). The loading behavior of both mandibular and maxillary molars showed a three-dimensional movement with translational and rotational components, which pushes the tooth into the alveolar socket. Moreover, we found a non-uniform PDL thickness distribution and a gradual increase in volumetric proportion of the periodontal vasculature from cervical to apical. Our results suggest that the PDL morphology may optimize the three-dimensional tooth movement to avoid high stresses under loading. [ABSTRACT FROM AUTHOR]