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In this study, the effect of high strain rate on the dynamic mechanical properties of shear thickening fluid (STF) impregnated felt of ultra‐high molecular weight polyethylene (UHMWPE) was investigated by split‐hopkinson pressure bar. UHMWPE felts are randomly oriented nonwoven fabric that holds each other due to inter‐fiber coupling either by thermal calendaring or mechanical entanglement. Its lower areal density and highly porous structure can be utilized in lightweight ballistic resistance material. The junction points inside its porous structure make it easier to hold abundant STF. Shear thickening fluid was prepared by dispersing 100 nm dry silica powder into polypropylene glycol at 67.5 wt% concentration using probe ultrasonicator at 25°C. Rheological characterization of prepared STF was conducted using MCR702 advanced Anton Paar rheometer. It was done by performing a steady shear rate and thixotropy tests for shear thickening and structural regeneration behavior. In‐house fabricated split‐hopkinson pressure bar setup was used to evaluate dynamic compressive behavior at different strain rates by changing triggering pressure. It was found that STF impregnated felt shows a higher amplitude of strain rate augmentation and energy absorption than a neat felt. The impact energy absorption increases with increasing strain rate. However, the peak stress shows an opposite trend with an increased strain rate in STF impregnated felt. [ABSTRACT FROM AUTHOR]

Material systems capable of handling both the ballistic impact and blast waves are necessary for security forces. In this study, the high strain rate performance of monolithic and bonded ultra‐high molecular weight polyethylene (UHMWPE) with high‐temperature resistant basalt/polyetherimide (B/PEI) composite is presented. Individual composite laminates were fabricated using vacuum‐assisted compression molding. Subsequently, cylindrical test coupons were cut using a high‐pressure waterjet. A suitable adhesive grade was used for the bonding of two different composite types. The dynamic compression studies were conducted on a split‐Hopkinson pressure bar (SHPB). For identical incident energies, the range of strain rates attained by monolithic UHMWPE, B/PEI and bonded composites differed significantly. Monolithic UHMWPE achieved the highest rates of loading, whereas higher stresses were recorded for the B/PEI composite. Yet, monolithic UHMWPE, owing to higher constant stress plastic flow, results in higher toughness. Bonded composites revealed hybrid properties with delamination of UHMWPE as the primary failure mode. High‐speed imaging exposed severe deformation of UHMWPE during dynamic compression. SEM micrographs revealed fiber pull‐out and deforming behavior of UHMWPE and brittle failure of B/PEI composite. B/PEI in a bonded composite system never failed under dynamic compression within the experimental range, thus providing a window of opportunity to tailor‐make better ballistic and blast protection materials. [ABSTRACT FROM AUTHOR]

An investigation of the effect of strain rate on the dynamic compressive behavior of glass/polytetrafluoroethylene (PTFE) composite is presented. Experimental studies were carried out on two dimensional (2D), satin weave (SW) and three dimensional (3D) woven glass/PTFE composites using split Hopkinson pressure bar (SHPB) apparatus. Commercial grades of glass/PTFE fabrics were autoclaved to prepare the composite laminates and circular specimens were cut out using a high‐pressure water jet. High strain rate studies confirmed the rate‐dependent behavior of all the woven composite systems under consideration. The highest rates of loading were attained by 3D woven specimens for identical incident energies. The highest peak stress attained by 3D woven specimens was 501 MPa, which was trailed by 2D woven specimens with 482 MPa stress. The advantage of satin weave was not reflected in the small specimens as the peak stress attained for identical loading was limited to 405 MPa. Similarly, the highest strain and toughness were recorded for 3D woven composites. However, the SW pattern unlocked a new possibility of controlling the primary damage axis. Furthermore, an analytical method is presented based on variable rate power law to predict the dynamic compressive stress of glass/PTFE. [ABSTRACT FROM AUTHOR]

Kevlar reinforced composite material systems are widely used for personal body armors. Due to aging or minor damage while in service, body armor may get exposed to external weather conditions, including moisture. The present study investigates the effect of moisture on the high strain rate behavior of Kevlar/Polypropylene (K‐PP) composite. Flat K‐PP composite laminate was manufactured using a vacuum‐assisted compression molding followed by laser machining. Dynamic compressive loading tests were performed using split Hopkinson pressure bar setup. The phenomenological modeling approach was adopted to characterize the rate‐dependent behavior of dry and wet composites. For identical dynamic compressive loading, different strain rates, strains, and stresses were attained by the dry and wet composite specimens. Macroscopic and microscopic imaging was done to expose the variation in damage behavior as a function of moisture absorption. Significant property reduction as a function of moisture absorption emphasizes the need for moisture proofing and protecting the armor products from minor damages leading to sites for moisture ingress. [ABSTRACT FROM AUTHOR]

In this study, the influence of hybridization on the compression response of thermoplastic matrix-based composites under high strain rate loading was investigated. The intra-ply and inter-ply hybrid composites were manufactured with Kevlar/Basalt yarns as the reinforcements with Polypropylene as a matrix. Cylindrical composite specimens were laser cut from the flat compression moulded laminates. The composite specimens were loaded under high strain rate using split-Hopkinson pressure bar setup at strain rates ranging from 2815/s to 5481/s. The study revealed differences in the rate-dependent growth of peak stress, peak strain and toughness with the strain rate. Intra-ply hybrid composites with alternate weaving of Kevlar and basalt yarns exhibited highest peak stress as compared to the Inter-ply hybrid composites (alternate layers of Kevlar and basalt fabrics) and another intra-ply composite containing Kevlar in the warp and basalt in the weft direction. Whereas in inter-ply hybrid composite, with Kevlar as the loading face attained higher stress, while composite with Basalt as the loading face attained higher strain. SEM micrographs revealed that Kevlar on the loading face can bear the impact with lesser delamination as compared to the Basalt on the loading face. Damage studies revealed that Kevlar fiber surface loading results in higher stress as compared to basalt (brittle) surface loading with lower overall damage. • The influence of hybization on the high strain rate resposne of thermoplastic composites. • Intra-ply hybridization excels over inter-ply hybridization. • Placement and direction of yarns is crucial in intra-ply hybridization. • Higher areal density fabrics are replacable with hybrid fabrics of lower areal density. [ABSTRACT FROM AUTHOR]

The dynamic behaviour of the High Strength Low Alloy (HSLA) Steel before and after heat treatment was examined experimentally by performing quasi-static and high strain rate testing at room temperature and cryogenic temperatures. The high strain rate tensile testing of the material was performed on a Split Hopkinson Tensile Bar (SHTB) setup. A customized liquid nitrogen chamber equipped with UTM and SHTB was used to perform the cryogenic temperature testing. The stress–strain response of the material under different loading conditions was recorded and a modified Johnson–Cook material model was derived. It was observed that the flow stress of the material increased when tested at a high strain rate and it further increased at a cryogenic high strain rate loading environment. The microstructure of the material before and after heat treatment was also observed to identify the dominant phase change in microstructure contributing towards improvement in strength after heat treatment. The failure analysis of each category of the samples was examined under the Scanning Electron Microscope (SEM) after the testing. The formation of small and deep dimples for as-received samples and bigger and shallow dimples for heat-treated samples distinguished the type of failure between the quasi-static, high strain rate and cryogenic high strain rate material testing. • High Strength Low Alloy Steel (HSLA) were characterized at Quasi-Static and high strain rate tensile testing at room temperature and cryogenic temperature in both annealed and post heat treated conditions. • The customized Split Hopkinson Tensile Bar equipped with liquid nitrogen chamber and on-board temperature measurement system was developed to perform high strain rate cryogenic testing of HSLA steel. • The fractured surface of annealed and post heat treated samples were examined to understand the underlying effect contributing towards improvement in mechanical properties of the HSLA steel. • The modified Johnson–Cook material model parameters were derived based on the experimental results. The numerical simulations were performed to verify the developed constituent model. [ABSTRACT FROM AUTHOR]

As a major challenge, development of light-weight fibre reinforced polymer (FRP) composite body armour, characterization of candidate matrix polymers at high strain rate impact is the focus in this research. Polypropylene (PP) and the nano-composites with 1-5% by weight of NC (nanoclay) platelets are the candidates considered. In the characterization phase, high strain rate impact and quasi-static loading tests were performed to figure out the limiting (failure) responses. Comparison between the material systems is, subsequently, made to nominate one matrix configuration. Enhancements of mechanical properties with increase in weight percentage of the nanoparticles are observed at both quasi-static and dynamic loadings. Observations of dispersed imposed failure modes, development of novel model for failure modulus and evaluation of peak strength values are also attempted. [ABSTRACT FROM AUTHOR]

This study systematically investigates the effect of Shear Thickening Fluid (STF) treatment on the high strain rate properties of UHMWPE (Ultra High Molecular Weight Poly Ethylene) composites. Spherical nanosilica particles of size 100 nm were used for the synthesis of STF. The high strain rate impact studies were accomplished on in-house designed and fabricated Split Hopkinson Pressure Bar (SHPB) experimental set-up. Compression moulded UHMWPE variant Gold Shield ® was used as the ballistic composite. Both STF-treated as well as neat Gold Shield ® specimens were subjected to high strain rate impact testing. From the experimental results and Fractography studies it was revealed that STF treatment enhanced the ballistic resistance of Gold Shield ® composite material. In the SHPB experiments, the improved ballistic performance of STF-treated Gold Shield ® specimens was manifested in terms of higher peak stress, specimen strain rates and impact toughness. [ABSTRACT FROM AUTHOR]

Shear thickening fluids (STFs) are a special class of field responsive fluids which exhibit change of phase from liquid to solid when subjected to imposed shear. This remarkable characteristic of STFs has led to their application in soft body armor technologies, leading the development of concept of Liquid Body Armors (LBAs). LBAs extensively rely upon the symbiotic relationship between STF and high strength FRP (Fiber Reinforced Polymer) composites comprising of high tenacity fibers such as Kevlar, UHMWPE (Ultra High Molecular Weight Poly Ethylene) etc. Although in the past, STFs have been widely characterized by rheometers at low strain rates (≤10 3 s −1 ), but in actual practical scenarios, body armours encounter much higher strain rates (of the order of 10 5 –10 7 s −1 ) under a ballistic impact. The main objective of this study is to capture the dynamics of STFs at such high strain rates by employing Split Hopkinson Pressure Bar (SHPB) technique. The STF sample was synthesized by dispersing 67.5 wt.% of 100 nm silica powder in Poly Propylene Glycol (PPG) and ethanol, using ultrasonic homogenization method. The mechanical response of STF was studied at high strain rates in terms of the stress-strain behavior and variation of the impact toughness with the loading rate of the fluid specimen. It was observed that the impact toughness of STF increased progressively with the specimen loading rate. The peak stress and peak strain rate attained in the SHPB tests were 147 MPa and 22,100 s −1 , respectively. The characteristic transition time of STF was found to be in the range of 13–25 µs. [ABSTRACT FROM AUTHOR]

Shear thickening is a non-Newtonian flow behavior characterized by the increase in apparent viscosity with the increase in applied shear rate, particularly when the shear rate exceeds a critical value termed as the critical shear rate (CSR). Due to this remarkable property of shear-thickening fluids (STFs), they are extensively used in hip protection pads, protective gear for athletes, and more recently in body armor. The use of STFs in body armor has led to the development of the concept of liquid body armor. In this study, the effect of particle size is explored on the low and high strain rate behavior of nanosilica dispersions, so as to predict the efficacy of STF-aided personal protection systems (PPS), specifically for ballistic applications. The low strain rate study was conducted on cone and plate rheometer, whereas the high strain rate characterization of STF was conducted on in-house fabricated split Hopkinson pressure bar (SHPB) system. Spherical nanosilica particles of three different sizes (100, 300, and 500 nm) as well as fumed silica particles of four different specific surface areas (Aerosil A-90, A-130, A-150, and A-200), respectively, were used in this study. The test samples were prepared by dispersing nanosilica particles in polypropylene glycol (PPG) using ultrasonic homogenization method. The low strain rate studies aided in determining the CSR of the synthesized STF dispersions, whereas the high strain rate studies explored the impact-resisting ability of STFs in terms of the impact toughness and the peak stress attained during the impact loading of STF in SHPB testing. [ABSTRACT FROM AUTHOR]

In this study, experimental investigations on Kevlar fiber reinforced polypropylene (PP) woven composites under high strain rate compression loading are discussed. Kevlar/PP composite laminates with 8 and 24 layers are fabricated using vacuum assisted compression molding technique. Maleic anhydride grafted-PP (MAg-PP) is added to PP to improve the interfacial property between Kevlar fiber and PP resin. The through-thickness properties at high strain rates from 1370 to 6066 s −1 are obtained using split Hopkinson pressure bar (SHPB) setup. The behavior of PP resin is found to be different than the commonly used thermoset resins, such as epoxy. Dynamic stress–strain relations are drawn to reveal the mechanical properties at high strain rates and these relations appear to be rate sensitive. As a result, the peak stress increased by three times, toughness increased by almost ten times and strain at peak stress increased by as much as two times with an increase in the strain rate. The final failure of the specimens is examined by scanning electron microscopy (SEM) to explore the possible failure mechanisms such as, delamination, fiber failure and shear fracture. [ABSTRACT FROM AUTHOR]

• Vacuum compression moulded Basalt-Polyeteherimide (PEI) composites manufacturing. • Optimization of Basalt-PEI composite manufacturing moulding parameters. • Basalt-PEI composite under quasi-static and dynamic high strain rate loading. • Elastic recovery of Basalt-PEI composite can help in reflecting the blast wave. High temperature blast and ballistic resistant light weight fibre reinforced plastic composites are very much in demand. Accordingly, the present investigation is focused on the quasi-static and high strain rate behaviour of Basalt/Polyetherimide (PEI) composite. Nine different types of composite samples were fabricated by compression moulding. The moulding pressures and temperatures were varied in the range of 15–25 bars and 325 °C−375 °C, respectively. Quasi-static testing was done at the rate of 3 mm/min to establish the optimum moulding parameters. High strain rate compression tests in the strain rate range of 900/s−3200/s were performed on the optimum moulded composite specimens. High strain rate testing revealed that 40 layered Basalt/PEI composite moulded at 25 bar pressure and 350 °C attained highest stress of 932 MPa whereas, the same was found to attain 446 MPa under quasi-static loading conditons. Thus, establishing the rate depedency of Basalt/PEI composite. Damage studies revealed that Basalt/PEI undergoes brittle damage, typically resulting in shear plane angle of 42°−45°. SEM micrographs revealed brittle fibre failure and matrix free fibre bundles, indicating the importance of process parameter optimiation. [ABSTRACT FROM AUTHOR]

The present study deals with the quasi-static and high strain rate characterization of Kevlar-129 based thermoplastic composites. Two different thermoplastic matrices, namely, Polypropylene (PP) and Polyetherimide (PEI) were used to manufacture composite laminates. Quasi-static compression tests were performed at strain rates of 0.041 s−1 and 0.045 s−1. High strain rate tests were performed using a split Hopkinson pressure bar apparatus within the strain rates ranging from 2548 s−1 to 4379 s−1. Stress-strain relations reveals the rate-sensitive behaviour of composites. Kevlar/PP (K-PP) showed higher peak stress under quasi-static loading as compared to the high strain rate test. Comparable peak stresses were revealed under quasi-static and high strain rate loading for Kevlar/PEI (K-PEI) composite. Also, high strain rate compression properties such as peak stress, peak strain and toughness of K-PP were 25%, 27% and 6% higher than that of the K-PEI composite. The failure mechanisms of both the composites were characterized through macroscopic and scanning electron microscopy. K-PP failed majorly due to matrix crush and fibre failure while K-PEI failed due to shear cracking. Damage study reveals that a single fibre based composite system can be tailored to act as an energy-absorbing or dissipating material system by varying the thermoplastic matrix materials. • Static and dynamic compressive properties of Kevlar reinforced high-performance polymers. • Kevlar/Polypropylene outperforms over Kevlar/Polyetherimide under both the quasi-static and high strain rate loads. • The quasi-static strength of Kevlar/Polypropylene is 25% higher than its high strain rate strength. • Polypropylene matrix results in ductile failure, while the Polyetherimide matrix results in brittle failure. [ABSTRACT FROM AUTHOR]