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In recent years, the quest for effective lubrication in micro deep drawing (MDD) has seen promising advancements. In this study, the influence of TiO2 nanolubricants and graphene lubricants on the performance of 301 stainless steel foil in MDD is examined. The MDD undergoes an extensive evaluation of various lubrication conditions, including dry, TiO2 nanolubricant, graphene lubricant at concentrations of 2.5 mg/mL, 5.0 mg/mL, and 10.0 mg/mL, as well as combined applications of TiO2 and graphene lubricants. Utilising a 5.0 mg/mL graphene lubricant together with TiO2 nanolubricants led to a significant reduction in drawing force, highlighting the synergistic efficacy of this combined lubricant. A pronounced enhancement in the consistency of the produced microcups was also attained. These results emphasise the promise of TiO2 nanolubricant and graphene lubricants in optimising the MDD process. [ABSTRACT FROM AUTHOR]

To improve the quality of products produced from microforming, various nanolubricants have been applied in the field of micromanufacturing in recent years. In this paper, the effects of glycerol-based lubricant containing TiO2 NPs (NPs) on micro deep drawing (MDD) of austenitic stainless steel (ASS) SUS301 were studied, and the lubrication mechanism involved was discussed. The MDD experiments were conducted with the SUS301 foils under dry, 1, 2, and 4 wt% TiO2 NP lubrication conditions. The results show that the use of the TiO2 nanolubricants can significantly improve the quality of the drawn cups in terms of decreased wrinkling and surface roughness. Besides, the concentration of TiO2 NPs influences lubricity by reducing friction during the MDD process. The peak drawing force is the lowest when 2 wt% nanolubricant is applied, which drops to 72.54 N from 77.38 N under dry conditions. The micro cup drawn under 2 wt% TiO2 nanolubricant has the best quality among those obtained under all the lubrication conditions. The lubrication mechanisms are derived from the mending effects of TiO2 NPs and the formation of thin lubricant films associated with the open lubricant pockets (OLPs) and close lubricant pocket (CLPs) theory in the MDD. The CLPs function as reservoirs that retain lubricants to counteract the load pressure, whereas the OLPs lead to lubricant leakage due to the higher flow resistance. It was found that the lubricant film and NPs are insufficient at a low concentration (1 wt%), while the lubrication performance can be enhanced with increased NP concentration. However, there exist apparent agglomerations on the surface of the produced micro cup when using 4 wt% nanolubricant, which greatly deteriorates the lubricant performance in the MDD process. It is concluded that the lubricant containing 2 wt% TiO2 NPs demonstrates the best lubrication performance during the MDD of ASS SUS301. [ABSTRACT FROM AUTHOR]

The microstructure of Cr–Mn–Ni–N stainless steel is regulated by a combination of cold deformation and subsequent martensite reversed annealing. The yield strength and tensile strength of the tested steel are greatly improved to 1220 and 1357 MPa, respectively, by conventional heavy cold rolling (66% thickness reduction) and a subsequent annealing process (750 °C for 5 min) relative to those before cold rolling (austenized state); at the same time, the total elongation keeps an appropriate value. The results show that the grain refinement strengthening acts as the primary factor for the strengthening of the tested steels while the precipitation behavior from the M23C6‐type carbides is not quite effective. Additionally, different yield phenomena and microstructural evolution for tested steels with 66% thickness reduction annealed at 750 °C with different holding times are systematically analyzed and discussed. Lüders‐like deformation features noticeably appear but become weakening with the longer annealing time. The change in initial free mobile dislocation density is the core cause of the preyield plateau phenomenon. [ABSTRACT FROM AUTHOR]

Microstructure and texture evolution of a low-Ni Cr–Mn–N austenitic stainless steel were analysed during three-point bending process. The electron back-scattering diffraction (EBSD) was used to characterise the microstructural evolution with respect to two regions encompassing (I) near the inner corner and (II) near the outer corner. The fraction of deformation-induced martensite of either types (ε- and α′-martensite) was analysed in both regions. The region (I) possessed a considerably higher fraction of ε-martensite than that in the region (II). In the region (II), the fraction of austenite 60°/〈111〉 twins was increased. Moreover, in the region (I), the 10 1 ¯ 2 ⟨ 1 ¯ 011 ⟩ extension twinning was depicted in ε-martensite. The mean kernel average misorientation of ε-martensite experienced a trivial change with increasing bending angle after reaching to a saturation point. Upon bending, texture measurements of austenite returned the αγ-fibre orientations with the dominant Brass component. However, a decrease in the Cube and S texture components was identified. The ε-martensite texture revealed strong intensities along the h k i l ε -fibre. Besides, the α′-martensite developed 001 0 1 ¯ 0 α ′ and 001 001 α ′ orientations with a trace of 113 4 7 ¯ 1 α ′ orientation. [ABSTRACT FROM AUTHOR]

Bimetal composites have wide applications due to their excellent overall performance and relatively low cost. In this study, the formability of stainless/carbon steel bimetal medium-thick composite in the stamping process without blank holder was investigated by finite element (FE) simulations and experiments. Uniaxial tensile tests on substrate metal (carbon steel) and clad metal (stainless steel) were first conducted, respectively, in order to obtain the material properties of each metal layer required in the FE simulation. Processing variables, including the layer stacking sequence, relative thickness ratios of two layers and friction conditions, were considered, and their effects on the magnitude of press load and distributions of thickness strain for predicting the high-risk region of necking during stamping were discussed. Experimental tests were carried out to verify the simulation results. It is indicated that simulation results can be used as an evaluation indicator to ensure the bimetal medium-thick composite can be safely formed. [ABSTRACT FROM AUTHOR]

• The unique hot flow behaviour of bimetal composite different from that of a single material was analysed. • A physically-based constitutive model considering DRV and DRX softening mechanisms for bimetal composite was established. • A mixture law of bimetal composite considering the strain and stress partitioning was developed. • Analytical, FE and experimental investigations were conducted on the flow behaviour of bimetal composite. The flow behaviour and strain partitioning of 2205 duplex ferritic-austenitic stainless steel/AH36 low carbon steel bimetal composite (2205/AH36 BC) were investigated at elevated temperatures in this study. A physically-based constitutive model was established to describe the flow behaviour of bimetal composite based on the stress–strain relationships obtained from hot tensile tests, which were performed on a Gleeble 3500 thermal-mechanical test simulator over the temperature range of 950–1250 °C and strain rate range of 0.01–1 s−1. The stress and strain partitioning of bimetal composite was analysed to develop a mixture law of flow stress under those hot working conditions, due to the different strain contributions of each material on the total flow behaviour of bimetal composite. The developed constitutive model and the mixture law considering strain partitioning were both adopted to predict the stress–strain curves and used in finite element (FE) simulation model to calculate the peak loads of 2205/AH36 BC at 1000 °C. It is found that the softening mechanisms of 2205/AH36 BC changes depending on the externally imposed working temperatures and strain rates. The contribution of AH36 carbon steel layer on total stress is relatively more than that of 2205 stainless steel layer at high temperatures, as a result of the occurrence of stress partitioning. The proposed constitutive model, instead of the mixture law, is recommended to be used in the FE simulation of practical hot working of bimetal composite due to its high accuracy. [ABSTRACT FROM AUTHOR]

In this study, the micro deep drawing (MDD) experiments of an austenitic stainless steel with 40 μm in thickness were conducted using the lubricants containing different mass fractions of graphene nanosheets (GNS) in ethanol. Prior to the MDD tests, the lubricants with GNS concentrations of 5, 10, and 15 mg/ml were synthesised by mixing different amounts of GNS with pure ethanol, and then sprayed uniformly on the blank surface. The friction-reduction mechanisms of the GNS in the MDD were discussed by analysing the profile and surface roughness of the microcups. The results indicated that the GNS could reduce the friction and improve the surface quality of the micro products during the MDD process. In particular, the lubricant with 10 mg/ml GNS enabled the lowest drawing force, wrinkling, and surface roughness of the drawn microcup. These findings contribute to a better understanding of the friction-reduction mechanisms of using GNS in the MDD of materials. • The coating behaviour of the graphene lubricants are compared. • The role of graphene lubricant in micro deep drawing is shown to be important in reducing the friction. • The effect of utilising graphene lubricants for improving the quality of the micro cups is demonstrated. [ABSTRACT FROM AUTHOR]