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AZ61 and AM60 magnesium alloys, with higher mechanical strengths than that of the most commonly used AZ31 alloy, were subjected to high-temperature rolling. Although the basal textures of the as-rolled sheets of both alloys were significantly weakened by annealing, the texture weakening was more significant in the latter than in the former. In addition, splitting of the basal pole was not retained after annealing for the AZ61 alloy, but this type of texture was preserved in the case of the AM60 alloy. The formation of statically recrystallized grains with dispersed orientations resulted in the aforementioned change in texture. The difference in the static recrystallization behavior could be attributed to the solute effect of zinc atoms. The annealed AZ61 and AM60 alloy sheets exhibited excellent stretch formability at room temperature, with Erichsen values of 7.8 and 8.5 mm, respectively, comparable to those of aluminum alloys. The higher Erichsen value for the AM60 alloy compared to that of the AZ61 alloy resulted from the more weakened basal texture and the splitting of the basal pole with an inclination angle of ±20° in the rolling direction, which are favorable for basal slip during sheet forming. [ABSTRACT FROM AUTHOR]

Abstract: Mg–3Al–1Zn magnesium alloy sheets rolled at 350°C, 450°C and 525°C, which exhibit approximately the same grain size but a significant decrease in basal texture intensity with increasing rolling temperature, were used for investigating the influence of initial texture on deep drawing behaviour at room temperature. The sheets rolled at 350°C and 450°C fracture at drawing ratios of 1.5 and 1.7, respectively, while the sheet rolled at 525°C can be successfully drawn at a large drawing ratio of 1.8. The fracture site changes from the shoulder of drawn cup to the edge of the flange with the weakening of initial basal texture. At the flange, the basal texture dramatically changes to the TD-texture with basal planes perpendicular to the sheet plane accompanied with sheet thickening. Both tensile twinning and basal slip contribute to this texture change due to compressive stress along the circumferential direction. In the case of weak initial texture, relatively restricted tensile twinning and more activated basal slip delay the development of the TD-texture, which is favoured for maintaining deformation capability at the flange and in turn enhances deep drawability. The deformation behaviour is discussed in terms of the change in Schmid factor for basal slip during deep drawing. [Copyright &y& Elsevier]

Abstract: The annealing behaviours of Mg–3Al–1Zn magnesium alloy sheets warm rolled at 225°C and 150°C using differential speed rolling, which are mainly characterized by dynamic recrystallized microstructure and deformation microstructure, respectively, were investigated at different annealing stages. Static recrystallization occurs for the sheet rolled at 150°C while only grain growth proceeds for the sheet rolled at 225°C. For the sheet rolled at 225°C, the grain growth of dynamic recrystallized grains eliminates the basal pole inclination in the rolling direction. In contrast, for the sheet rolled at 150°C, the grain growth after static recrystallization retains the basal pole inclination, which is favoured for sheet forming. This difference in texture evolution may be attributed to the dynamic or static recrystallization prior to grain growth, which results in residual dislocation densities for the former and thus leads to the preferential growth of harder oriented basal grains at the centre of (0001) pole figure with lower dislocation densities during annealing. [Copyright &y& Elsevier]

Poor formability of rolled magnesium (Mg) alloys extremely restricts applications in form of sheets originating from formation of strong basal texture. Recently, we found that increasing rolling temperature from 723 to 798 K for a AZ31 Mg alloy can significantly improve stretch formability due to remarkable texture weakening after annealing. In this study, static recrystallization behaviors of AZ31 alloy sheets rolled at 723 and 798 K were investigated by electron backscattered diffraction analyses at different annealing stages in order to understand the origin of high temperature rolling on texture weakening. For both sheets, similar deformation microstructures with approximately the same types and fractions of twins exist in the as-rolled condition and recrystallized grains are mainly formed at pre-existing grain boundaries due to discontinuous recrystallization during subsequent annealing. However, only the basal texture of the latter remarkably weakens due to the formation of new recrystallized grains with well-dispersed orientations. Non-basal slips enhanced during high temperature rolling at 798 K are most likely responsible for the texture randomization as a result of rotations of recrystallization nuclei. [ABSTRACT FROM AUTHOR]

Abstract: The microstructural and textural evolution during post-annealing as well as mechanical properties of a Mg–4Y–3RE magnesium alloy sheet processed by differential speed rolling at 823K were investigated. The as-rolled sheet exhibits deformation microstructure regardless of the high rolling temperature. Static recrystallization occurs around second-phase particles as a result of particle-stimulated nucleation and also at pre-existing grain boundaries due to solute effects of rare-earth elements, resulting in randomization of basal texture. Despite a large amount of second-phase particles, the weakened texture leads to a moderate stretch formability with an Erichsen value of 4.4. [Copyright &y& Elsevier]

Abstract: The effects of increasing rolling temperature from 723K to 828K at the last rolling pass on microstructure, texture, mechanical properties and stretch formability of a Mg–3Al–1Zn magnesium alloy previously rolled at 723K were investigated. In the as-rolled condition, the basal texture strengthens slightly with increasing the rolling temperature whereas it weakens more remarkably after static recrystallization during annealing for the sheets rolled at higher temperatures. Only by increasing the rolling temperature from 723K to 798K, the Erichsen value is significantly increased from 4.5 to 8.6 due to the weakened texture for the annealed sheets. Further increasing the last rolling temperature does not appear to further improve the stretch formability. [Copyright &y& Elsevier]

Abstract: The recrystallization and grain growth behaviour of Mg–3Al–1Zn alloy sheets with a deformation microstructure, obtained by a combination of high-temperature rolling and subsequent warm rolling, was investigated at different stages of annealing. The basal texture was significantly weakened as a result of the formation of new grains with a largely altered c-axis orientation relative to the initial basal orientation owing to discontinuous static recrystallization during primary recrystallization. The new grains nucleated mostly at the pre-existing grain boundaries rather than at the intersections of twins or within the twins. Subsequent grain growth led to further progression of the texture weakening accompanied by an enhancement in the basal pole inclination. [Copyright &y& Elsevier]

The Mg–3Al–1Zn magnesium alloy sheets with initial extrusion and casting microstructures were symmetrically rolled at a high temperature of 823K, followed by a warm rolling at 498K. The initial texture plays a vital role in texture development and results in inclination angle of split basal pole varying from ±15° to ±40°. The sheet rolled perpendicular to extrusion direction exhibits a homogeneous microstructure with an inclination angle of ±25° and the highest Erichsen value of 9.7. [Copyright &y& Elsevier]

Mg–3Al–1Zn alloy sheets were rolled at high temperatures up to 823K and subsequently rolled at 498K using differential speed rolling. The basal texture intensity dramatically weakens with a largely tilted basal pole after annealing. The Erichsen value significantly increases from 3.7 to 9.5 with an increase in the rolling temperature from 498 to 823K prior to warm rolling due to texture effects. This high Erichsen value is comparable to those of aluminum alloys. [Copyright &y& Elsevier]

Abstract: The microstructural and textural evolution of the hot-extruded AZ31 alloy plate during differential speed rolling (DSR) has been investigated. For the hot-extruded plate, a large texture gradient exists in the thickness direction while the grain size distribution is nearly homogenous. The textural evolutions at near-surface and mid-layer regions are different between the DSR processed and the normal symmetric rolled sheets. The inclination of basal pole at the mid-layer increases at an accelerating rate with progress of the DSR processing due to the enhancement of the unidirectional shear bands. The deformation tends to concentrate on the previously formed shear bands, which exhibit a favored crystalline orientation for further shear localization. [Copyright &y& Elsevier]

The influence of reduction per pass over the range of 9–63% on the microstructure and texture of Mg–3Al–1Zn magnesium alloy sheets processed by differential speed rolling at the same total reduction of 63% have been investigated. With increasing reduction per pass, the number of unidirectional shear bands increases, resulting in a more homogeneous microstructure and a weaker basal texture at mid-layer. The inclination direction of the basal pole with respect to the rolling direction depends on the reduction per pass. [Copyright &y& Elsevier]

Abstract: A heat-treatable AZ80 magnesium alloy has been subjected to differential speed rolling (DSR) at a large thickness reduction per pass of 33%, and microstructure, texture, mechanical properties, stretch formability as well as texture evolution during stretch forming have been investigated. The basal pole of the DSR-processed sheet tilts toward the rolling direction at 15°. The as-rolled sheet exhibits a combination of high strength (tensile strength: 329MPa) and high ductility (fracture elongation: 25%). The Erichsen value at room temperature improves from 3.7 to 4.5 compared with the normal-rolled sheet. The enhancement of the stretch formability can be attributed to the texture effects due to the same grain size of 7μm. The DSR-processed sheet exhibits a larger Schmid factor for basal slip and the inclination of basal pole retains during the stretch forming. The aging treatment remarkably enhances the mechanical strength further while it significantly deteriorates the formability. [Copyright &y& Elsevier]

Mg–6Al–1Zn magnesium alloy sheets were rolled at high temperatures of 723–793K using differential speed rolling. The Erichsen value remarkably increases about 1.5 times due to the weakened basal texture regardless of the coarser grains with increasing the rolling temperature from 723 to 793K. The sheet rolled at 793K exhibits a combination of a superior stretch formability with an Erichsen value of 7.0 and a high tensile strength of 300MPa at room temperature. [Copyright &y& Elsevier]

Abstract: The differential speed rolling (DSR) with a roll speed ratio of 1.167 was carried out on an AZ31B magnesium alloy in order to investigate its effects on the formability. Compared with the normal rolled sheet exhibiting approximately the same average grain size, the Erichsen values of the DSR processed sheet with an inclination of basal pole in the rolling direction significantly increased by about 1.5 and 1.9 times at room temperature and at 423K, respectively. The deep-drawing temperature limit for a drawing ratio of 1.5 was also lowered from 443K to 423K. The improvement of the press formability at low temperatures can be attributed to the texture modifications, which led to a lower 0.2% proof stress, a larger uniform elongation, a smaller Lankford value and a larger strain hardening exponent. [Copyright &y& Elsevier]