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Tibito Tephra was first recorded in the central highlands of Papua New Guinea (PNG) in 1971. By the late 1970s, the tephra had been mapped across tens of thousands of square kilometres, traced to its source on Long Island in the Bismarck Sea, and linked to pyroclastic density currents in the Matapun Beds on the island. With a tephra fall volume >10 km3, this eruption was clearly one of the 10 largest globally in the past 600 years. Although almost certainly in the AD 17th or 18th centuries, determining just when this VEI 6 eruption occurred has proved difficult. Whether this eruption occurred before or after William Dampier sailed past, named, described and drew a profile of Long Island has been debated also. Dating the Long Island eruption has implications for assessing the rate of revegetation of the island, recolonisation of the island and caldera lake, Jared Diamond’s theory of ‘supertramp’ birds, correlations between major eruptions and ice core chronologies, the constant rate of supply model of 210Pb concentration in lake sediments, reservoir effects in Lake Kutubu in the southern highlands of PNG, the timing of a prehistoric phase of agriculture in the Western Highlands and the longevity of oral histories recording a taim tudak (time of darkness) when sand fell from the sky, houses collapsed, crops were ruined and people died. This paper reviews early dates based on radiocarbon, 210Pb and paleosecular magnetic variation, historical reports and genealogical dates from oral histories, and speculation based on tree ring and ice core evidence. Analyses of 10 new radiocarbon dates from the Matapun Beds on Long Island are reported. Our best estimate places the eruption between 1651 and 1671 AD with a 95.4% probability and between 1655 and 1665 AD with a 68.2% probability. [ABSTRACT FROM AUTHOR]

Sample preparation protocols for concentrating organic material from sediments for radiocarbon dating often include a large number of steps and the use of hazardous chemicals. Thus, these protocols are often problematic for pollen-poor sediments as material can get lost or may become degraded. Pyrite in samples for radiocarbon dating hinders an effective graphitisation process and thus needs to be removed during sample preparation. Standard protocols require the use of nitric acid, a strong oxidant that corrodes organic material. Therefore, the use of nitric acid needs to be avoided when preparing pollen-poor but pyrite-rich sediments. We present a method that minimises the sample preparation steps by replacing acid treatment with heavy liquid separation. Using non-toxic LST at a density of 2.0 g cm −3 is shown to be effective for separating the organic fraction from sulphides, silicates and carbonates. We applied this method to pyrite-rich and pollen-poor sediments from Western Australia that had previously been problematic to date. The successful AMS radiocarbon dating of all samples pre-treated with LST demonstrates the effectiveness of this method. [ABSTRACT FROM AUTHOR]

Marine reservoir ages are a key element in calculating and constraining uncertainty in radiocarbon age estimates and are also essential to better understand regional ocean circulation. In this study, we present a new method to reconstruct long-term, high-resolution sea surface reservoir ages based on analysis of the organic skeleton of deep-sea (560 m) black coral (Anthozoa, Antipatharia). Our results confirm that antipatharians are extremely slow growing (typical radial growth rate for a South Pacific specimen around 0.03 mm/yr). Coupled uranium series and radiocarbon measurements were made on black coral collected live from the Norfolk Ridge (north Tasman Sea) to provide the first modern reservoir ages for this region. At the Norfolk Ridge, the average reservoir age between 1790 AD and 1900 AD was ∼330 years. This was followed by a steep decrease over time of about 70 years to 1950 AD (our most modern value). This indicates an increase in surface ocean ventilation of water masses in this region. These results are consistent with observational studies for the early twentieth century, which suggest significant changes in regional circulation of the southwest pacific. [ABSTRACT FROM AUTHOR]

Abstract: We have studied two young speleothems, SC4 from Smiths Cave (Christmas Island, eastern Indian Ocean) and WM7 from Wollondilly Cave (Wombeyan caves, SE Australia). Attempts to date these speleothems by the Th/U method have proved unsuccessful with some age reversals for SC4 due to multiple sources of non-authigenic Th. This method has also resulted in imprecise ages for WM7 because of low U concentrations (<10 ppb) and consequently very low levels of authigenic 230Th relative even to the very low levels of detrital 230Th present. Here, we present an alternative method for reliable dating of these young speleothems using radiocarbon. Approximately 100 carbonate samples from SC4 and WM7 were analysed for 14C by accelerator mass spectrometry (AMS). The AMS results indicate that bomb 14C was evident in the youngest parts of both stalagmites. Two different approaches were used to estimate dead carbon fraction (DCF) values for these stalagmites for the pre-bomb period. For SC4, the DCF values were estimated based on the timing of 14C dates for that period determined by high-resolution δ18O recorded in the speleothem, and the timing of the onset of bomb 14C. For WM7, a “maximum” range of pre-bomb DCF was determined. Chronologies of these speleothems were built based on a dense sequence of DCF-corrected ages using three different age-depth models: Clam (Classical method), and Bacon and OxCal (Bayesian statistical approach). Good agreement between these age-depth models were observed indicating that the top 170 mm of SC4 and the top 50 mm of WM7 grew during the past 550–750 years and 1360–1740 years, respectively. [Copyright &y& Elsevier]

This paper presents the initial radiocarbon ages from the Lower Murray Archaeological Project developed in conjunction with the Ngarrindjeri Heritage Committee in South Australia. As part of this community based research program, a total of 59 shell (V. ambiguus) and charcoal samples were selected for radiocarbon dating. Radiocarbon ages varied significantly between sites within the region and ranged from 150-490 calBP at Pomberuk (Hume Reserve Midden and Historic Campsite) to 8190-8390 calBP at Glen Lossie Midden and Burial Site (GLMBS). These results will contribute to developing a more comprehensive understanding of human occupation in Ngarrindjeri ruwe (lands and waters) and assist in developing a local chronology for the region. [ABSTRACT FROM AUTHOR]

Radiocarbon dates on multiple individual charcoal fragments floating together down the Macdonald River, New South Wales, Australia, have calibrated ages spanning >1700 years. Partial explanations of this range of inherited ages can be attributed to the inbuilt age of living biomass, charcoalisation conditions, hillslope transport and storage and/or valley floor (fluvial) transport and storage, but the contribution of each of these components can be constrained only rarely. These results caution against using radiocarbon dating of charcoal as the sole dating technique to interpret Late-Holocene sedimentary histories. These findings also show that it is unlikely that deposit age has a dependable relationship to charcoal age. [ABSTRACT FROM AUTHOR]

Radiocarbon measurements reveal that soil carbon is often hundreds to thousands of years old; significantly older than the annual flux of carbon through the soil would suggest. Models deal with this discrepancy by conceptualizing soil carbon as having fast and slow cycling pools. The Rothamsted Soil Carbon Model contains an inert pool for this reason. Here we use a unique record of time-series radiocarbon measurements from long-term trials to demonstrate that the inert pool is hardly inert, and that its mean age varies from 2000 to as little as 90 years depending on carbon flow through the soil. This finding suggests that the concept of truly inert organic matter requires redefinition to account for the enhanced probability that microorganisms will overcome barriers to previously inaccessible organic matter as their activity increases. [ABSTRACT FROM AUTHOR]

Abstract: Assigning accurate dates to hypersaline sediments opens important terrestrial records of local and regional paleoecologies and paleoclimatology. However, as of yet no conventional method of dating hypersaline systems has been widely adopted. Biomarker, mineralogical, and radiocarbon analyses of sediments and organic extracts from a shallow (13cm) core from a hypersaline playa, Lake Tyrrell, southeastern Australia, produce a coherent age-depth curve beginning with modern microbial mats and extending to ~7500calyrBP. These analyses are furthermore used to identify and constrain the timing of the most recent change in hydrological regime at Lake Tyrrell, a shift from a clay deposit to the precipitation of evaporitic sands occurring at some time between ~4500 and 7000yr. These analyses show the potential for widespread dating of hypersaline systems integrating the biomarker approach, reinforce the value of the radiocarbon content of biomarkers in understanding the flow of carbon in modern ecologies, and validate the temporal dimension of data provided by biomarkers when dating late Quaternary sediments. [Copyright &y& Elsevier]

Deep-sea corals are an important component of benthic ecosystems, but are potentially very vulnerable to ecological disturbance due to their extreme longevity and slow growth rates. Among the slowest growing genera are the 'Black Corals' (Family Antipatharia), which can have lifespans of millennia. The waters around New Zealand contain a variety of black corals, including species that grow at shallow depths in the southern Fjords. However, while growth rates in black corals have been reported for many other parts of the world, New Zealand's black corals have received little attention. Here we present a series of high-resolution radiocarbon dates for coral colonies of the genera Antipathella , Leiopathes and Antipathes. Our results illustrate some corals have lifespans of up to 3000 years and slow but highly variable growth (averaging 10–100 μm/yr) for genera Leiopathes and Antipathes and fast growth (averaging 2–3 cm/yr) for genera Antipathella , with no obvious regional variability in growth rates over time. Our results are broadly consistent with other black coral growth rate studies, and reinforce that New Zealand's black corals likely have low resilience to any disturbance. • Deep-sea black corals show extreme longevity on the order of several millennia. • Slow growth suggests black corals are highly susceptible to any disturbances. • Growth rates do not exhibit regional patterns based on food availability. • Growth rate is intrinsic to species. [ABSTRACT FROM AUTHOR]

Over the last decade, two major calving events of the Petermann Ice Tongue in Northwest Greenland have led to speculation on its future stability and contribution to further Greenland Ice Sheet mass loss. However, it has been unclear if these events are anomalous or typical within the context of limited historical observations. We extend the historical record of the floating ice tongue using the stratigraphy of Petermann Fjord sediments to provide a longer-term perspective. Computed tomography (CT) scans, X-Ray Fluorescence (XRF) scans, Ice-Rafted Debris (IRD) counts, and the magnetic properties of specific particle size fractions constrain changes in depositional processes and sediment sources at our core sites, allowing for reconstructions of past behavior of the Petermann Ice Tongue. Radiocarbon dating of foraminifera, 210Pb, and paleomagnetic secular variation (PSV) provide age control and help to address uncertainties in radiocarbon reservoir ages. A floating ice tongue in Petermann Fjord formed in late glacial time as Petermann Glacier retreated from an advanced grounded position. This paleo-ice tongue broke-up during the early Holocene when high northern latitude summer insolation was higher than present. After gradual regrowth of the ice tongue associated with regional cooling, the ice tongue reached its historical extent only within the last millennium. Little or no ice tongue was present for nearly 5000 years during the middle Holocene, when decadal mean regional temperatures are estimated to be 0.8–2.9 °C higher than preindustrial (1750 CE) and seasonal sea-ice in the Lincoln Sea was reduced. This pre-historical behavior shows that recent anthropogenic warming may already be in the range of ice tongue instability and future projected warming increases the risk of ice tongue break-up by the mid-21st Century. • A transect of sediment cores constrain past retreat and advance of Petermann Glacier's floating ice tongue. • Particle-size specific properties disentangle sedimentary source and transport signals. • Multi-proxy age-depth modeling constrains the timing of glacial changes. • Petermann Ice Tongue broke-up during early Holocene warming and was absent for nearly five of the last seven thousand years. • Historically observed ice tongue extents of Petermann Glacier are only characteristic of the latest Holocene. [ABSTRACT FROM AUTHOR]

We describe new radiocarbon-dated evidence for the late survival of beavers from an upland site in northern England. A wood specimen with beaver gnaw marks was recovered from the bank of the Scaup Burn in Kielder Forest in Northumberland. The marks were analysed, the tree species were identified and the sample was radiocarbon dated to between 1269 and 1396. Other wood remains in the same context suggest a most likely dating between 1330 and 1390. This find represents the most recent radiocarbon-dated physical evidence of beaver yet found in Britain, by at least 400 years. In conjunction with documentary and other archaeological evidence from the period, this discovery indicates beaver were present within the Tyne River catchment up until at least the 14th century ad. In addition, this find highlights the need to investigate all possible evidence of beaver fully when discovered and to remain open-minded about the possibility of making finds in unexpected locations and contexts. [ABSTRACT FROM AUTHOR]

Abstract: Fish otoliths from the Willandra Lakes Region World Heritage Area (south-western New South Wales, Australia) have been analysed for oxygen isotopes and trace elements using in situ techniques, and dated by radiocarbon. The study focused on the lunettes of Lake Mungo, an overflow lake that only filled during flooding events and emptied by evaporation, and Lake Mulurulu, which was part of the running Willandra Creek system. Samples were collected from two different contexts: from hearths directly associated with human activity, and isolated surface finds. AMS radiocarbon dating constrains the human activity documented by five different hearths to a time span of less than 240 years around 19,350 cal. BP. These hearths were constructed in aeolian sediments with alternating clay and sand layers, indicative of fluctuating lake levels and occasional drying out. The geochemistry of the otoliths confirms this scenario, with shifts in Sr/Ca and Ba/Ca marking the entry of the fish into Lake Mungo several years before their death, and a subsequent increase in the δ18O by ∼4‰ indicating increasing evaporation of the lake. During sustained lake-full conditions there are considerably fewer traces of human presence. It seems that the evaporating Lake Mungo attracted people to harvest fish that might have become sluggish through oxygen starvation in an increasingly saline water body (easy prey hypothesis). In contrast, surface finds have a much wider range in radiocarbon age as a result of reworking, and do not necessarily indicate evaporative conditions, as shown by comparison with otoliths from upstream Lake Mulurulu. [Copyright &y& Elsevier]