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Surface plasmon (SP) excitation in metal-coated tilted fiber Bragg gratings (TFBGs) has been a focal point for highly sensitive surface biosensing. Previous efforts focused on uniform metal layer deposition around the TFBG cross section and temperature self-compensation with the Bragg mode, requiring both careful control of the core-guided light polarization and interrogation over most of the C + L bands. To circumvent these two important practical limitations, we studied and developed an original platform based on partially coated TFBGs. The partial metal layer enables the generation of dual-comb resonances, encompassing highly sensitive (TM/EH mode families) and highly insensitive (TE/HE mode families) components in unpolarized transmission spectra. The interleaved comb of insensitive modes acts as wavelength and power references within the same spectral region as the SP-active modes. Despite reduced fabrication and measurement complexity, refractometric accuracy is not compromised through statistical averaging over seven individual resonances within a narrowband window of 10 nm. Consequently, measuring spectra over 60 nm is no longer needed to compensate for small temperature or power fluctuations. This sensing platform brings the following important practical assets: (1) a simpler fabrication process, (2) no need for polarization control, (3) limited bandwidth interrogation, and (4) maintained refractometric accuracy, which makes it a true game changer in the ever-growing plasmonic sensing domain.

Plasmonic tilted fiber Bragg gratings (TFBGs) have emerged as versatile tools for refractometric analyses and biochemical sensing. Their applications have significantly blossomed these last years, from proteins and cellular bioassays to operando monitoring in batteries, to cite just a few. They are widely recognized for their cutting‐edge performance and low limits of detection, arising from their dense multimodal spectral nature featuring tens of narrowband cladding mode resonances. Their comb‐like spectrum is so rich that numerous demodulation techniques have been reported, without benchmark of their relative performance while they possess important distinctions. This review highlights developments in detangling techniques from the pioneering works based on single‐peak analysis up to the most recent approaches involving Fourier analysis, the implementation of machine learning, and cascaded spectral decomposition processes. To fairly compare the different techniques of the literature, we implemented each analysis on original experimental refractometric calibrations, revealing the assets of the most updated methods. This paper therefore reviews these demodulation techniques based on the same datasets, obtained under the same conditions. We show and discuss the results obtained from bioassays and pinpoint the importance of advanced analytical methodologies to maximize the reproducibility, reliability and performance of plasmonic‐based TFBGs biosensors. [ABSTRACT FROM AUTHOR]

Gold-coated tilted fiber Bragg gratings (TFBGs) have been highly studied over the last years, mainly for biosensing purposes. They present a comb-like spectrum of narrow-band cladding mode resonances that is often demodulated by tracking the change of a selected peak. In this paper, we report a twentyfold more sensitive demodulation method based on the intersection of the upper and lower envelopes of gold-coated TFBG spectra. This method has been successfully applied in biosensing experiments towards the detection of HER2 (Human Epidermal Growth Factor Receptor-2) proteins, a relevant biomarker for breast cancer. Practical improvements have also been implemented. First, a uniform FBG has been superimposed on the TFBG to reduce the read-out wavelength span to 10 nm instead of 70 nm while keeping the temperature-compensated measurements. Second, a micro-fluidic system has been implemented to smoothly deliver the samples to the sensor. These 3 originalities make this sensing platform even more attractive for use in practical applications. [ABSTRACT FROM AUTHOR]

The apparent increase in magnetic field measurement has led to a growing demand for new sensing technologies. However, a long-lasting challenge unaddressed is how to achieve ultrahigh sensitive magnetic field measurement in both amplitude and orientation. Here, we demonstrate a compact-in-size and simple-to-implement fiber-optic magnetometer for highly sensitive vector magnetic field measurement. The sensor is based on magnetic nanoparticles coated tilted fiber Bragg grating inscribed in a commercial single mode fiber. The sensing mechanism stems from the backward coupled cladding mode resonances with narrow bandwidth (Q factor > 104), which is highly sensitive to slight surface refractive index perturbation. The switching of the magnetic field direction on the surface of fiber induces redistribution of coated magnetic nanoparticles with spatial anisotropy density and scattering by formation of magnetic chains hereafter the effective index is changed, which in turn modulates the cladding mode resonance with wavelength shift and amplitude attenuation. Through calculating the peak-to-peak intensity of target cladding modes of TFBG, the external magnetic field was precisely measured with an intensity sensitivity of 0.39 dB/mT and a direction sensitivity of 0.038 dB/rad. The inherent core mode can be used as a reference to get rid of temperature crosstalk and light source disturbance. The proposed sensor is compact in size and easy to be used in hard-to-reach place, showing good potentials for industrial applications. [ABSTRACT FROM AUTHOR]

The coupling of less than 80 µW of in‐plane polarized near‐infrared light in a 6 nm‐thick graphene layer deposited on an optical fiber produces important permittivity changes leading to bistability and self‐starting 50% modulation of over 1 W of continuous wave light in the core. These features arise from resonant coupling of core‐guided light into the cladding by a 12‐degree tilted, 1 cm long fiber Bragg grating via narrowband, polarization‐dependent resonances that allow the selection of cladding modes with electric fields polarized in the plane of the graphene. The pulse repetition rate of the modulation increases from 10 to 269 Hz for input powers ranging from 0.3 to 1.33 W in the core, with no evidence of saturation. Investigations into the origin of these effects through physical modelling and different experimental conditions point to photo‐induced Joule heating in the graphene layer giving rise to temperature increases of the order of 60 °C and corresponding permittivity changes in the graphene and underlying silica fiber. Those changes lead to shifts in the resonance positions which result in the equivalent of saturable absorption for light guided in the core without direct contact with the absorbing graphene layer. [ABSTRACT FROM AUTHOR]

This study focuses on the tilted fiber Bragg gratings. The paper describes the method of their inscription into optical fiber using the Talbot interferometer and KrF excimer laser system. The method allows precise selection of the resonant wavelengths and tilt angles of the created structures in a wide range of values. In course of the study, an original method was proposed for inscription of a superposition comprising two structures being identical in parameters but having the opposite tilt angles of grating strokes relative to the optical fiber cross-section. The described method makes it possible to compensate the decrease in the reflective efficiency of fiber Bragg gratings with an increase in their tilt angle. [ABSTRACT FROM AUTHOR]

Multicore optical fibers are of great interest in the optical sensing field. Their core diversity and spatial distribution enable the development of sensing mechanisms that are not possible in single-core fibers. In this paper, we study the use of the inter-core crosstalk phenomena for the implementation of a surrounding refractive index (SRI) sensor. The selective inscription of a tilted fiber Bragg grating (TFBG) intentionally increases the inter-core crosstalk between the inscribed cores and makes it sensitive to the SRI. With this technique we simplify the measurement of the SRI and improve the identification and tracking of the excited cladding modes, as compared with the analysis of the transmission spectrum of a TFBG in single-core fibers. The proposed device is also sensitive to temperature. Temperature is obtained from the crosstalk wavelength shift with a measured sensitivity of 9.75 pm/°C. The SRI is obtained from the measurement of the crosstalk optical power. For increasing SRIs the cladding modes gradually fade, reducing the crosstalk optical power. We observed that the higher the tilt, the higher the sensor sensitivity. For a 7° TFBG the SRI sensitivity obtained is −74.2 dB/RIU from 1.31 to 1.39 and −250.8 dB/RIU from 1.39 to 1.44. [ABSTRACT FROM AUTHOR]

A reflective fiber-optic refractometer based on a broadband cladding-to-core recoupling for a wide range of refractive index measurement is proposed and experimentally demonstrated. The sensing probe contains a tilted fiber Bragg grating (TFBG) together with an in-fiber “cladding” mirror upstream. The “cladding” mirror is made by a 0.3-μm-thick gold film with a transparent aperture to permit all the core-guided light go through but reflect the light in the cladding. The downstream TFBG couples the forward propagating core mode to backward propagating cladding modes and such cladding modes are reflected to the TFBG again by the in-fiber “cladding” mirror and recoupled to the fiber core through the same TFBG. With this special design, all the transmitted cladding modes now can be effectively monitored in reflection. Compared with the reported “in-fiber” and “fiber-to-fiber” coupling TFBG refractometer, our sensor demonstrates a much broader surrounding refractive index operating range with a very linear sensitivity of 528 nm/RIU. A tunable laser is used to improve the measured accuracy and a sensitivity of 7973 dB/RIU was obtained, with a limit of detection of 10−6 RIU. The sensor works with very controllable cross-sensitivities because the core mode is temperature dependent but insensitive to surrounding refractive index. [ABSTRACT FROM AUTHOR]

A new technique of depositing a poly(vinyl alcohol) (PVA) coating with an airbrush on the cylindrical surface of an optical fiber with real‐time spectral monitoring is presented. The method is applied for creating hygroscopic PVA coating as a part of the tilted‐fiber Bragg‐grating (TFBG)‐assisted fiber hygrometer samples. By monitoring the transmission spectra of the samples placed in a climatic chamber with variable relative humidity, the performance of the resulting coating is evaluated. Experimental data are presented, demonstrating the effectiveness of the described technique for humidity‐sensing purposes. [ABSTRACT FROM AUTHOR]

Optical fibers are of growing interest for biosensing, especially for point-of-care and biomedical assays. Their intrinsic properties bestow them sought-after assets for the detection of low concentrations of analytes. Tilted fiber Bragg gratings (TFBGs) photo-inscribed in the core of telecommunication-grade optical fibers are known to be highly-sensitive refractometers. In this work, we present different strategies to use them for label-free immunoassays. Bare, gold-sputtered, gold-electroless-plated (ELP) and hybrid configurations are biofunctionalized with antibodies, aiming at the detection of cancer biomarkers. We discuss the relative performances of the tested configurations and show that each leads to singular key features, which therefore drives their selection as a function of the target application. The most sensitive configuration presents a limit of detection of 10−12 g/mL in laboratory settings and was successfully used ex vivo in freshly resected lung tissues.

Tilted fiber Bragg gratings (TFBGs) have shown to be a suitable tool for exciting surface plasmon waves in a comparable manner as in typical attenuated total reflection Kretschmann configurations. In this paper, we present a comparative analysis of the characteristics of prism and grating configurations for generating surface plasmon resonance (SPR) for 800 and 1550 nm wavelengths. Results indicate that longer wavelength SPR may present advantages in sensing. Recent label-free biochemical sensing results using NIR TFBGs with and without SPR coatings demonstrate limits of detection ranging from the nM to the pM range without the need for thermal stabilization. [ABSTRACT FROM PUBLISHER]

The tilted fiber Bragg grating (TFBG), as a versatile and robust tool for many sensing applications with a particular focus on vapor deposition processes, is reviewed. Recent work employing the TFBG as an optical probe for monitoring the metal-organic (MO)CVD of noble-metal, single-source precursors is discussed extensively. This work also establishes the broad scope that utilizes TFBGs and other optical fiber configurations to interrogate thin film growth and the associated optical properties. While it cannot possibly cover the full scope of applications with respect to the TFBG device, this review highlights the recent advances of TFBG-based sensing for CVD, and progress towards the applicability of TFBGs as evanescent field-based sensors. [ABSTRACT FROM AUTHOR]

Optical fibers are of growing interest for biosensing, especially for point-of-care and biomedical assays. Their intrinsic properties bestow them sought-after assets for the detection of low concentrations of analytes. Tilted fiber Bragg gratings (TFBGs) photo-inscribed in the core of telecommunication-grade optical fibers are known to be highly-sensitive refractometers. In this work, we present different strategies to use them for label-free immunoassays. Bare, gold-sputtered, gold-electroless-plated (ELP) and hybrid configurations are biofunctionalized with antibodies, aiming at the detection of cancer biomarkers. We discuss the relative performances of the tested configurations and show that each leads to singular key features, which therefore drives their selection as a function of the target application. The most sensitive configuration presents a limit of detection of 10−12 g/mL in laboratory settings and was successfully used ex vivo in freshly resected lung tissues. [ABSTRACT FROM AUTHOR]