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Lamellar γ-TiAl has a microstructure that spans multiple length scales: lamellar thickness (10 nm–1 μm), γ domain length (100 nm–10 μm) and colony size (100 μm–1 mm). Only by characterizing the deformation across the different scales can one understand how the microstructure influences plasticity and damage formation in this material. Here, we use digital image correlation and electron backscatter diffraction to map strain and lattice rotation with both sub-colony and sub-lamella spatial resolution in a polycrystalline lamellar γ-TiAl alloy with TiB 2 inclusions. Two lamellar thicknesses and temperatures are tested. It is shown that the hard mode-oriented colonies undergo minimal plastic strain. However, as the temperature is increased, macroscopic deformation bands develop across colonies of different orientations, independent of their local lamellar orientations. Increasing magnification, it is apparent that some segments of these bands occur by slip or twinning parallel to the lamellae, and others by transverse lattice rotation. In the thin lamellar condition, such macroscopic deformation bands also occur along colony boundaries; this causes a significant inhomogeneity in the strain distribution. Such strain inhomogeneities are also further characterised here at the microstructural scale of single lamellae, and locally at boride particles. • Nanoscale resolution digital image correlation (HR-DIC) strain mapping up to 700 °C. • Characterisation of plastic deformation and mechanical damage across multiple length scales in lamellar γ-TiAl. • Macroscopic bands of heightened deformation developed, focused at grain boundaries. • Methods to repress deformation bands by microstructural modifications are discussed. [ABSTRACT FROM AUTHOR]

Abstract The occurrence of plasticity below the macroscopic yield stress during tensile monotonic loading of nearly lamellar Ti-45Al-2Nb-2Mn(at%)-0.8 vol% TiB 2 at both 25 °C and 700 °C, and in two conditions of lamellar thickness, was measured by digital image correlation strain mapping of a remodelled Au surface speckle pattern. Such initial plasticity, not necessarily related to the presence of common stress concentrators such as hard particles or cracks, could occur at applied stresses as low as 64% of the general yield stress. For a same applied strain it was more prominent at room temperature, and located as slip and twinning parallel to, and near to or at (respect.) lamellar interfaces of all types in soft mode-oriented colonies. These stretched the full colony width and the shear strain was most intense in the centre of the colonies. Further, the most highly operative microbands of plasticity at specimen fracture were not those most active prior to yielding. The strain mapping results from polycrystalline tensile loading were further compared to those from microcompression testing of soft-mode stacks of lamellae milled from single colonies performed at the same temperatures. Combined with post-mortem transmission electron microscopy of the pillars, the initial plasticity by longitudinal dislocation glide was found to locate within 30–50 nm of the lamellar interfaces, and not at the interfaces themselves. The highly localised plasticity that precedes high cycle fatigue failure is therefore inherently related to the lamellar structure, which predetermines the locations of plastic strain accumulation, even in a single loading cycle. Graphical abstract Image 1 [ABSTRACT FROM AUTHOR]

• Nanoscale digital image correlation (HR-DIC) strain mapping of HCF up to 670 °C. • Microplasticity mainly in softmode colonies: parallel to lamellae, near interfaces. • Poor strain transfer across colony boundaries at both temperatures. • At 25 °C, maximum stress influenced the slip band count more than did the cycle count. Microplasticity in a lamellar TiAl alloy upon high cycle tensile fatigue was measured by high resolution digital image correlation strain mapping at several stress and cycle increments, at 25 °C and 670 °C, for two lamellar thicknesses. Plastic deformation occurred primarily in soft-mode colonies at both temperatures, operating by slip parallel to the lamellae, and near lamellar interfaces. Plastic strains generally decreased to zero by the colony boundary; strain transfer across such boundaries was rare at both temperatures. At 25 °C, the maximum applied stress influenced the number of slip bands more so than did the number of loading cycles. [ABSTRACT FROM AUTHOR]

The strain rate (ε ˙) and temperature (T) dependent mechanical response of single crystal magnesium (Mg) micropillars compressed along the [ 2 ¯ 110 ] direction (a -axis) is investigated from room temperature to 573 K and from 10-3 to 100 s-1. The loading direction was chosen to disfavour basal slip activation by a low Schmid factor, allowing the investigation of the rate-sensitivities of extension twinning and prismatic slip. For T ≤ 423 K, the plasticity was governed by extension twinning for the entire range of the applied strain rates. At T > 423 K and for ε ˙ ≤ 10 s-1, extension twinning did not occur and a continuous plastic flow induced by prismatic dislocation mediated plasticity was observed: the twin to slip transition takes place due to the decrease of the critical resolved shear stress of non-basal slip. For ε ˙ > 10 s-1, however, the accommodation of the plastic deformation by activation of prismatic slip is not enough to match the applied deformation rate, favouring again deformation twinning. The first part of this work provides a complete overview of the mutual effects of T and ε ˙ on the transition points of deformation modes in Mg at the microscale. In a second stage, the influence of thermal and kinetic contributions on the evolution of the flow stress leading to the slip to twin transition at 573 K has been assessed in more detail. Within the slip-dominated plasticity regime, this work provides a quantitative assessment of the increases in the saturation stress (stage III) with ε ˙ at high temperature, showing how the strain rate dependency of the dislocation generation rate in the pillar and escape rate at the free surfaces of the structure controls the stress evolution in Mg microcrystals. [Display omitted] [ABSTRACT FROM AUTHOR]