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The indigenous populations of La Palma (Canary Islands), who arrived on the island from Northwest Africa ca. 2000 years B.P., were predominantly pastoralists. Yet, many aspects of their subsistence economy such as the procurement, management, and use of wild plant resources remain largely unknown. To explore this, we studied the 600–1100‐year‐old archaeological site of Belmaco Cave, which comprises a stratified sedimentary deposit representative of a fumier. Here, we present a high‐resolution, multiproxy geoarchaeological study combining soil micromorphology, lipid biomarker analysis, X‐ray diffraction, μ‐X‐ray diffraction, μ‐X‐ray fluorescence, Fourier transform infrared spectroscopy, and μ‐Fourier transform infrared spectroscopy, to characterize formation processes and explore plant sources. Recurrent goat/sheep habitation and maintenance activities are represented by interstratified layers of unburned dung, charcoal‐rich sediment, and dung ash. Lipid biomarker data show a herd diet mainly composed of herbaceous plants, which is key to understanding the mobility of indigenous shepherds. Our results also revealed an unusual suite of authigenic minerals including hazenite, aragonite, and sylvite, possibly formed through diagenetic processes involving interaction between ash, dung, urine, volcanogenic components, and bacterial activity, coupled with arid and alkaline conditions. Our study shows the potential of a multiproxy approach to a fumier deposit in a volcanogenic sedimentary context. [ABSTRACT FROM AUTHOR]

Middle Paleolithic lithic and faunal assemblages throughout Eurasia reflect short-term Neanderthal occupations, which suggest high group mobility. However, the timing of these short-term occupations, a key factor to assess group mobility and territorial range, remains unresolved. Anthropogenic combustion structures are prominent in the Middle Paleolithic record and conceal information on the timing and intensity and natural setting of their associated human occupations. This paper examines a concentration of eleven combustion structures from unit Xb of El Salt, a Middle Paleolithic site in Spain through a geoarchaeological approach, in search of temporal, human impact and paleoenvironmental indicators to assess the timing, intensity and natural setting of the associated human occupations. The study was conducted using micromorphology, lipid biomarker analysis and compound specific isotope analysis. Results show in situ hearths built on different diachronic topsoils rich in herbivore excrements and angiosperm plant residues with rare anthropogenic remains. These data are suggestive of low impact, short-term human occupations separated by relatively long periods of time, with possible indicators of seasonality. Results also show an absence of conifer biomarkers in the mentioned topsoils and presence of conifer charcoal among the fuel residues (ash), indicating that fire wood was brought to the site from elsewhere. A microscopic and molecular approach in the study of combustion structures allows us to narrow down the timescale of archaeological analysis and contributes valuable information towards an understanding of Neanderthal group mobility and settlement patterns. [ABSTRACT FROM AUTHOR]

Leaf waxes have been assumed to be the dominant source of wax delivered to sediment. However, wooden branches and twigs have not been widely considered in this context and could be a potential source of wax lipids in fire places or combustion structures. Black sedimentary layers are the main material of open-air archaeological combustion structures and represent either carbonized fuel (wood) or the charred ground beneath the fire (mainly leaves) and it is difficult to discern between the two sources. To identify different plant parts as components of combustion residues, fresh and charred leaves, branches and twigs (bark and xylem) of the Celtis australis tree were analyzed for aliphatic and aromatic hydrocarbons and fatty acid concentrations, as well as the carbon isotopic composition of n -alkanes (δ 13 C alkane ). Charred biomass was produced under limited oxygen conditions at 150, 250 (3 and 5 h), 350 and 450 °C for 1 h. The n -alkyl profiles in different parts of C. australis are sufficiently distinct to allow their identification as components of combustion structures under low combustion temperature conditions. Average chain lengths and carbon preference index ratios decrease with increasing temperature and vary among plant parts. The δ 13 C alkane values remained slightly unaltered up to 350 °C and changed by 3–4‰ at 450 °C. Our results provide new information on the molecular and isotopic changes that occur upon burning different plant parts, which in turn show potential for good preservation of organic matter in archaeological black layers and for positive identification of burned leaf and wood residues in them. [ABSTRACT FROM AUTHOR]

Molecular and isotopic approaches offer the chance to identify combustion residues and substrate components of archaeological combustion features to infer past fire-related activities. Analysis of fatty acid methyl esters by gas chromatography-combustion-isotope ratio mass spectrometry have been successfully used to distinguish among different animal fat groups. However, plant oils from different tissues have not been widely investigated even though organic residues from leaf, root, and wood tissues are preserved in sediments from archaeological combustion structures. Our analyses of plant residues from controlled laboratory heating sequences and experimental hearths involving wood and animal residues, provide references to discern anatomical parts of fresh and charred plants and to differentiate contributions of terrestrial plants and animal sources in open air hearths. This information is compared with charred organic residues from combustion structures from three Middle Palaeolithic sites: El Salt (Spain), Abric del Pastor (Spain) and Crvena Stijena (Montenegro). The occurrence of n -alkyl nitriles in our samples corroborates their potential as combustion temperature biomarkers and the δ13C 16:0 and δ13C 18:0 values allow us differentiate between charred and fresh plant anatomical parts and between fresh plant oils and animal fats. • δ13C 16:0 and δ13C 18:0 values from modern fresh and charred plant plants were obtained. • Animal fat residues are enriched in 13C (≈4‰) compared to plant residues. • n -Alkyl nitriles are preserved in sediments from Neanderthal combustion structures. • n -Alkyl nitriles have potential as combustion temperature biomarkers. [ABSTRACT FROM AUTHOR]

The Northern Iberian Plateau during the Early Iron Age witnessed the proliferation of villages, showcasing well-preserved earthen architectural remains that offer valuable insights into past daily life practices. However, the application of high-resolution geoarchaeological approaches to these contexts has been largely overlooked, despite their significance in assessing complex sedimentary sequences predominantly composed of earth-based construction materials. This paper presents the outcomes of a microcontextual geoarchaeological study conducted on earthen dwellings from the Early Iron Age village of Cerro de San Vicente (Salamanca, Northern Iberia). Our study employed soil micromorphology, lipid biomarker analysis, XRD, and XRF analyses to investigate site formation processes, characterize construction materials and techniques, and explore aspects of daily life practices, functionality, and dwelling life histories. Our results have enabled the identification of three distinct construction layers within the dwellings, shedding light on recurrent events of floor use, maintenance, and repaving. Additionally, we have detected periods of abandonment and decay of the earth-based construction material that inform on the dynamics of abandonment and reuse within the village. Furthermore, our analysis has revealed the presence of well-preserved lipid biomarkers throughout the sequences, possibly associated with the past functionality of the dwellings. Ongoing and future analyses will further contribute to our understanding of ancient construction practices and the utilization of domestic spaces at Cerro de San Vicente. This study significantly enhances the limited availability of high-resolution, microcontextual data sets concerning Iron Age contexts in Iberia, underscoring the potential of our approach for future consolidation and advancement. By combining different geoarchaeological methodologies, we demonstrate the importance of integrating diverse analytical techniques to gain comprehensive insights into the socio-cultural dynamics of the Early Iron Age settlements. • Early Iron Age village in Northern Iberia, with numerous earthen dwellings. • Integrated application of soil micromorphology, lipid biomarkers, XRD, and XRF analyses to investigate floor sequences. • Lipid biomarkers are abundant and well-preserved throughout the earthen floor sequences of the dwellings. • Recurrent cycles of use, maintenance and decay are documented within the dwellings. • Relevant microcontextualized data can be obtained from the geoarchaeological characterization of construction layers. [ABSTRACT FROM AUTHOR]

By studying combustion structures, which conceal information about anthropogenic activity, we might learn about their makers. This is especially important for remote time periods like the Middle Paleolithic, whose archaeological record comprises numerous combustion structures. The majority of these are simple, flat, open hearths, although a small number of features situated in pit-like depressions have been recorded. Given that hearths built on a flat surface can result in pit-like color alteration of the underlying sediment, accurate identification of pit hearths is a crucial step prior to behavioral interpretation. Here we present a comprehensive study of a possible pit hearth from the Middle Paleolithic site of El Salt, Spain, using a microcontextual approach combining micromorphology, lipid biomarker analysis, archaeomagnetism and zooarchaeology. This pit hearth involves a true depression containing a thick plant ash deposit. It reached very high temperatures, possibly multiple burning events and long combustion times. Morphologically distinct combustion structures in a single archaeological context may indicate different functions and thus a diverse fire technology, pointing to Neanderthal behavioral variability. • Studying combustion structures informs about their makers. • Microcontextual and multidisciplinary approach is used to study a pit hearth. • Morphologically distinct combustion structures may indicate different functions. • Different hearth functions point to Neanderthal behavioral variability. [ABSTRACT FROM AUTHOR]