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Soil moisture measurement is very important for soil system monitoring. Compared to the traditional thermo-gravimetric technique, which is time-consuming and can be only performed in labs, the optic-fiber technique has unique advantages, such as small size, remote application in fields, fast response time and immunity to electromagnetic fields. In this paper, the soil moisture is measured by using a polymer optical fiber Bragg grating (POFBG) probe with a packaged dimension of 40 mm × 15 mm × 8 mm. Due to the intrinsic water-absorbing property of poly (methyl methacrylate) (PMMA), optical fiber Bragg gratings based on PMMA have been widely investigated for humidity measurement. Taking advantage of this, a sensor based on the POFBG is investigated to verify the soil condition. The POFBG is protectively integrated inside a stainless-steel package. A window is opened with a thin polypropylene mat as a filter, which allows the air to go through but prevents the soil from going inside to pollute the POFBG. The sensor probe is embedded in soils with different gravimetric soil moisture contents (SMCs) ranging from 0% to 40% and, then, insulated by polyethylene films to minimize the impact from the external environment, showing an average temperature cross sensitivity of −0.080 nm/°C. For a constant temperature, an exponential relationship between the Bragg wavelength and the SMC is obtained. For the SMCs between 8% and 24%, linear relationships are presented showing a temperature-corresponded sensitivity between 0.011 nm/% and 0.018 nm/%. The maximal sensitivity is calculated to be 0.018 nm/% at 20 °C, which is 28 times as high as that in the previous work. For the SMC over 24%, the sensor becomes insensitive because of humidity saturation in the cavity of the sensor probe. Though temperature cross sensitivity is problematic for SMC measurement, the influence could be eliminated by integrating another humidity-insensitive temperature sensor, such as a silica FBG temperature sensor.

[EN] In this work, we obtained chirped Bragg gratings by post-coating uniform poly (methylmethacrylate) (PMMA) microstructured polymer optical fiber Bragg gratings (POFBGs) with an UV cure adhesive. The main advantage of the proposed method consists on being a cost-effective and simple solution, since no special phase mask, addi tional etching or gradient thermal annealing are required. A comparison between the fabricated chirped Bragg grating¿s performance and previous reported methods in the literature is presented. As a compact sensor with two different active areas (adhesive coated and uncoated sections of the POFBG), the developed sensing device can be used for multiparameter sensing, namely for strain, humidity and temperature monitoring. Allying the proposed flexible and low-cost fabrication technique with the intrinsic characteristics of POFs, one may conclude that the developed sensor has high potential for multiparameter sensing in possible future engineering and biomedical applications., National Natural Science Foundation of China (62003046) ; The Spanish Ministerio de Ciencia, Innovacion y Universidades RTI2018-101658-B-I00 FOCAL Project; Guangdong Basic and Applied Basic Research Foundation (2021A1515011997) ; Guangdong Recruitment Program of Foreign Experts (2020A1414010393) ; C. Marques ac-knowledges Fundacao para a Ciencia e a Tecnologia (FCT) through the CEECIND/00034/2018 (iFish project) and this work was developed within the scope of the project i3N, UIDB/50025/2020 &UIDP/50025/2020, financed by national funds through the FCT/MEC. Luis Pereira and Tiago Paixao also acknowledge FCT for the grant with references SFRH/BD/146295/2019 and PD/BD/128265/2016, respectively.

We experimentally report high reflectivity on the poly(methyl methacrylate) (PMMA)-based polymer optical fiber Bragg gratings by means of a 266 nm pulsed laser and phase mask technique. In the first recipe, fiber Bragg gratings (FBGs) were manufactured with a single pulse up to 3.7 mJ. After post-annealing, a stable refractive index change up to 4.2 × 10 − 4 was obtained. In the second recipe, FBGs were inscribed by 22 pulses with a lower pulse energy of 1.4 mJ, showing a stable refractive index change of 6.2 × 10 − 4 . Both behaviors may mainly be attributed to the movement of initiating radicals arising from benzyl dimethyl ketal (BDK) under UV irradiation. The high refractive index change in step-index fibers paves the way to tilted FBG manufacturing with large tilt angles potentially for biomedical applications.

We demonstrate a dual-core fiber-based Mach–Zehnder interferometer that could be used for precise detection of variations in refractive indices of gaseous samples. The fiber used here have a solid germanium-doped silica core and an air core that allows gases to flow through. Coherent laser beams are coupled to the two cores, respectively, and thus excite guiding modes thereby. Interferogram would be produced as the light transmitted from the dual cores interferes. Variations in refractive index of the hollow core lead to variations in phase difference between the modes in the two cores, thus shifting the interference fringes. The fringe shifts can be then interrogated by a photodiode together with a narrow slit in front. The resolution of the sensor was found to be ~1 × 10−8 RIU, that is comparable to the highest resolution obtained by other fiber sensors reported in previous literatures. Other advantages of our sensor include very low cost, high sensitivity, straightforward sensing mechanism, and ease of fabrication.

In this paper, an endlessly single mode microstructured polymer optical fiber (mPOF) in a Mach–Zehnder (M–Z) interferometer configuration is demonstrated for temperature and strain measurement. Because there is no commercial splicer applied for POF-silica optical fiber (SOF) connectorization, prior to the M–Z interferometric sensing, we introduce an imaging projecting method to align a polycarbonate mPOF to a SOF and then the splice is cured permanently using ultraviolet (UV) glue. A He-Ne laser beam at 632.8 nm coupled in a SOF is divided by a 1 × 2 fiber coupler to propagate in two fiber arms. A piece of mPOF is inserted in one arm for sensing implementation and the interference fringes are monitored by a camera. For non-annealed fiber, the temperature sensitivity is found to be 25.5 fringes/◦ C for increasing temperature and 20.6 fringes/◦ C for decreasing temperature. The converted sensitivity per unit length is 135.6 fringes/◦ C/m for increasing temperature, which is twice as much as the silica fiber, or 852.2 rad/◦ C/m (optical phase change versus fiber temperature), which is more than four times as much as that for the PMMA fiber. To solve the sensitivity disagreement, the fiber was annealed at 125◦ C for 36 h. Just after the thermal treatment, the temperature measurement was conducted with sensitivities of 16.8 fringes/◦ C and 21.3 fringes/◦ C for increasing and decreasing process, respectively. One month after annealing, the linear response was improved showing a temperature sensitivity of ~20.7 fringes/◦ C in forward and reverse temperature measurement. For the strain measurement based on non-annealed fiber, the sensitivity was found to be ~1463 fringes/%ε showing repeatable linear response for forward and reverse strain. The fiber axial force sensitivity was calculated to be ~2886 fringes/N, showing a force measurement resolution of ~3.47 × 10−4 N. The sensing methodology adopted in this work shows several advantages, such as very low cost, high sensitivity, a straightforward sensing mechanism, and ease of fabrication.

In this paper, we report a capillary-based Mach&ndash, Zehnder (M&ndash, Z) interferometer that could be used for precise detection of variations in refractive indices of gaseous samples. The sensing mechanism is quite straightforward. Cladding and core modes of a capillary are simultaneously excited by coupling coherent laser beams to the capillary cladding and core, respectively. An interferogram would be generated as the light transmitted from the core interferes with the light transmitted from the cladding. Variations in the refractive index of the air filling the core lead to variations in the phase difference between the core and cladding modes, thus shifting the interference fringes. Using a photodiode together with a narrow slit, we could interrogate the fringe shifts. The resolution of the sensor was found to be ~5.7 &times, 10&minus, 8 RIU (refractive index unit), which is comparable to the highest resolution obtained by other interferometric sensors reported in previous studies. Finally, we also analyze the temperature cross sensitivity of the sensor. The main goal of this paper is to demonstrate that the ultra-sensitive sensing of gas refractive index could be realized by simply using a single capillary fiber rather than some complex fiber-optic devices such as photonic crystal fibers or other fiber-optic devices fabricated via tricky fiber processing techniques. This capillary sensor, while featuring an ultrahigh resolution, has many other advantages such as simple structure, ease of fabrication, straightforward sensing principle, and low cost.

The monitoring of human physiological signs and body functions, such as respiration rate, heart rate, foot pressure, and joint movement, plays an important role in medical advances and life quality improvements. Polymer optical fibers are made of polymer materials with attractive characteristics compared with silica fibers, such as low Young’s modulus, high failure strain levels, high flexibility, and bio-compatibility. These advantages are well-aligned with the instrumentation requirements for monitoring human physiological and body functions. In this perspective, this paper provides a comprehensive review about polymer optical fiber for human physiological and body functions monitoring, namely mechanisms, materials, and applications, which makes it possible to envisage a widespread implementation of such sensors in this research field in the next few years.

[EN] We demonstrate the Bragg gratings inscription in the 850-nm spectral region by using trans-4-stilbenemethanol-doped poly methyl methacrylate step-index optical fiber and a 248-nm krypton fluoride (KrF) excimer laser system. The gratings inscription only takes 0.4 s. A detailed study of the grating fabrication process using different pulse repetition rates is also reported. In addition, temperature, humidity, and strain sensitivities are measured to demonstrate the potentiality of these components for different sensing applications., The research leading to these results has received funding from the Fundacao para a Ciencia e Tecnologia (FCT)/MEC national funds and when applicable co-funded by FEDER-PT2020 Partnership Agreement under Project UID/EEA/50008/2013. This work was also supported in part by the Research Excellence Award Programme GVA Prometeo 2017/103 Future Microwave Photonics Technologies and Applications, and in part by the Fundamental Research Funds for the Heilongjiang Provincial Universities under Grant KJCXZD201703. The work of C. Marques was supported by FCT through the Fellowship SFRH/BPD/109458/2015.

This article discusses recent advances in biocompatible and biodegradable polymer optical fiber (POF) for medical applications. First, the POF material and its optical properties are summarized. Then, several common optical fiber fabrication methods are thoroughly discussed. Following that, clinical applications of biocompatible and biodegradable POFs are discussed, including optogenetics, biosensing, drug delivery, and neural recording. Following that, biomedical applications expanded the specific functionalization of the material or fiber design. Different research or clinical applications necessitate the use of different equipment to achieve the desired results. Finally, the difficulty of implanting flexible fiber varies with its flexibility. We present our article in a clear and logical manner that will be useful to researchers seeking a broad perspective on the proposed topic. Overall, the content provides a comprehensive overview of biocompatible and biodegradable POFs, including previous breakthroughs, as well as recent advancements. Biodegradable optical fibers have numerous applications, opening up new avenues in biomedicine.

[EN] We demonstrate a largely tunable dispersion fiber Bragg grating (FBG) inscribed in a microstructured polymer optical fiber (mPOF). The bandwidth of the chirped FBG (CFBG) was achieved from 0.11 to 4.86 nm, which corresponds to a tunable dispersion range from 513.6 to 11.15 ps/nm. Furthermore, thermal sensitivity is used to compensate for the wavelength shift due to the applied strain. These results demonstrate that a CFBG in a POF is a promising technology for future optical systems. (C) 2018 Optical Society of America, Fundacao para a Ciencia e a Tecnologia (FCT) (SFRH/BPD/109458/2015, UID/EEA/50008/2013); Research Excellence Award Programme GVA (PROMETEO 2017/103); Oak Ridge Associated Universities (ORAU) (LIFESTART (2017-2019)); Natural Science Foundation of Heilongjiang Province (F2018026).

We report the inscription of fiber Bragg gratings (FBGs) and Fabry-Perot (FP) cavities in a gradient index cyclized transparent optical polymer (CYTOP) polymer optical fiber (POF) using a femtosecond laser. Through careful control of the inscription parameters, the coupling between the grating and the fiber’s higher order propagation modes is reduced, allowing for single peak grating spectra. Furthermore, we inscribe a 10-nm chirped grating and an FBG FP cavity with a free spectral range of 240 pm. We measure the group delay of the chirped grating and characterize the fiber FP cavity for strain and temperature.

[EN] In this work, a linearly chirped fiber Bragg grating (CFBG) inscribed in a microstructured polymer optical fiber (mPOF) has been demonstrated for detecting temperature pro- files during thermal treatments. A CFBG of 10 mm length and 0.98 nm bandwidth has been inscribed in a mPOF fiber by means of a KrF laser and uniform phase mask. The CFBG has a high temperature sensitivity of -191.4 pm/°C). The CFBG has been used as a semi-distributed temperature sensor, capable of detecting the temperature profile along the grating length, for scenarios that account minimally invasive biomedical treatments. Two experiments have been designed to validate the CFBG tem- perature reconstruction, using a linear gradient, and a research- grade radiofrequency ablation (RFA) setup to apply Gaussian- shaped temperature spatial profiles. The result is that the higher sensitivity of the CFBG supports the detection of spatially non- uniform temperature fields by means of spectral reconstruction., This work was supported in part by Nazarbayev University, Research Council (ORAU project LIFESTART), in part by Fundacao para a Ciencia e Tecnologia (FCT)/MEC through National funds and when applicable co-funded by FEDER PT2020 partnership agreement under the project UID/EEA/50008/2013, and in part by the Research Excellence Award Programme GVA PROMETEO 2017/103 FUTURE MICROWAVE PHOTONIC TECHNOLOGIES AND APPLICATIONS. The work of C. Marques was supported by FCT through the fellowship SFRH/BPD/109458/2015.

In this Letter, we report the fast growth of high quality uniform Bragg gratings in trans-4-stilbenemethanol (TS)-doped poly(methyl methacrylate) (PMMA) step-index optical fibers. Grating manufacturing was obtained using a 400 nm femtosecond pulsed laser and a 1060-nm-period uniform phase mask. For 20 mW mean laser beam power, the grating reflectivity reaches 98% in ∼60 s.

In this paper, we report photo-inscription of uniform Bragg gratings in trans-4-stilbenemethanol-doped photosensitive step-index polymer optical fiber. Gratings were produced at ~1575 nm by the phase mask technique with a femtosecond laser emitting at 400 nm with different average optical powers (8 mW, 13 mW and 20 mW). The grating growth dynamics in transmission were monitored during the manufacturing process, showing that the grating grows faster with higher power. Using 20 mW laser beam power, the reflectivity reaches 94 % (8 dB transmission loss) in 70 seconds. Finally, the gratings were characterized in temperature in the range 20 - 45 °C. The thermal sensitivity has been computed equal to – 86.6 pm/°C.

In this paper, both non-annealed and annealed trans-4-stilbenemethanol-doped step-index polymer optical fibers were photo-inscribed using a 325 nm HeCd laser with two different beam power densities reaching the fiber core. In the high density regime where 637 mW/mm2 are used, the grating reflectivity is stable over time after the photo-writing process but the reflected spectrum is of limited quality, as the grating physical length is limited to 1.2 mm. To produce longer gratings exhibiting more interesting spectral features, the beam is enlarged to 6 mm, decreasing the power density to 127 mW/mm2. In this second regime, the grating reflectivity is not stable after the inscription process but tends to decay for both kinds of fibers. A fortunate property in this case results from the possibility to fully recover the initial reflectivity using a post-inscription thermal annealing, where the gratings are annealed at 80 °C during 2 days. The observed evolutions for both regimes are attributed to the behavior of the excited intermediate states between the excited singlet and the ground singlet state of trans- and cis-isomers as well as the temperature-dependent glassy polymer matrix.

Bragg gratings photo-inscribed in polymer optical fibers (POFs) are more sensitive to temperature and pressure than their silica counterparts, because of their larger thermo-optic coefficient and smaller Young's modulus. Polymer optical fiber Bragg gratings (POFBGs) are most often photo-written in poly(methylmethacrylate) (PMMA) based materials using a continuous-wave 325 nm HeCd laser. In this work, we present the first study about birefringence effects in POFBGs manufactured in different types of fiber. To achieve this, highly reflective (> 90%) gratings were produced with the phase mask technique. Their spectral response was then monitored in transmission with polarized light. Polarization dependent loss (PDL) and differential group delay (DGD) were computed from the Jones matrix eigenanalysis using an optical vector analyzer. Maximum values exceeding several dB and a few picoseconds were obtained for the PDL and DGD, respectively. An inverse scattering technique applied to the experimental data provided an estimate of the photo-induced birefringence value arising from the side fabrication process. The response to lateral force was finally investigated for various incident directions using the PDL response of FBGs manufactured in step-index POFs. As the force induced birefringence adds to the photo-induced one, a force dependent evolution of the PDL maximum value was noticed, with a good temperature-insensitivity. (C) 2015 Optical Society of America

An endlessly single-mode doped microstructured poly(methyl methacrylate) (PMMA) optical fiber is produced for effective fiber Bragg grating (FBG) photo-inscription by means of a 400 nm femtosecond pulsed laser and the phase mask technique. The fiber presents a uniform benzyl dimethyl ketal (BDK) distribution in its core without drastic loss increase. It was produced using the selected center hole doping technique, and the BDK dopant acts as a photoinitiator. In this Letter, we report a rapidly growing process of the grating reflection band. For an 11 mW mean laser power, the FBG reflectivity reaches 83% in only 40 s.

During the past few years, a strong progress has been made in the photo-writing of fiber Bragg gratings (FBGs) in polymer optical fibers (POFs), animated by the constant wish to enhance the grating reflectivity and improve the sensing performances. In this paper, we report the photo-inscription of highly reflective gratings in step-index POFs, obtained thanks to a slight etching of the cladding. We demonstrate that a cladding diameter decrease of ~12% is an ideal trade-off to produce highly reflective gratings with enhanced axial strain sensitivity, while keeping almost intact their mechanical resistance. For this, we make use of Trans-4-stilbenemethanol-doped photosensitive step-index poly(methyl methacrylate) (PMMA) POFs. FBGs are inscribed at ~1550 nm by the scanning phase mask technique in POFs of different external diameters. Reflectivity reaching 97% is achieved for 6 mm long FBGs, compared to 25% for non-etched POFs. We also report that a cladding decrease enhances the FBG axial tension while keeping unchanged temperature and surrounding refractive index sensitivities. Finally and for the first time, a measurement is conducted in transmission with polarized light, showing that a photo-induced birefringence of 7 × 10(-6) is generated (one order of magnitude higher than the intrinsic fiber birefringence), which is similar to the one generated in silica fiber using ultra-violet laser.

Step-index polymer optical fiber Bragg gratings (POFBGs) and microstructured polymer optical fiber Bragg gratings (mPOFBGs) present several attractive features, especially for sensing purposes. In comparison to FBGs written in silica fibers, they are more sensitive to temperature and pressure because of the larger thermo-optic coefficient and smaller Young's modulus of polymer materials. (M)POFBGs are most often photowritten in poly(methylmethacrylate) (PMMA) materials using a continuous-wave 325 nm HeCd laser. For the first time to the best of our knowledge, we study photoinduced birefringence effects in (m)POFBGs. To achieve this, highly reflective gratings were inscribed with the phase mask technique. They were then monitored in transmission with polarized light. For this, (m)POF sections a few cm in length containing the gratings were glued to angled silica fibers. Polarization dependent loss (PDL) and differential group delay (DGD) were computed from the Jones matrix eigenanalysis using an optical vector analyser. Maximum values exceeding several dB and a few picoseconds were obtained for the PDL and DGD, respectively. The response to lateral force was finally investigated. As it induces birefringence in addition to the photo-induced one, an increase of the PDL and DGD values were noticed. © 2014 Copyright SPIE.

In this paper, we report photo-inscription of uniform Bragg gratings in Trans-4-stilbenemethanol-doped photosensitive step-index polymer optical fiber characterized by a core diameter of 8.2 μm. Single-mode gratings were produced at ~1550 nm by the phase mask technique with a Helium-Cadmium emitting at 325 nm with an average power of 30 mW. The grating growth was monitored during the manufacturing process, showing that the reflected band is blue shifted by a few hundreds of picometers. Finally, the gratings were characterized in temperature in the range 25 − 50 °C. Their sensitivity has been computed equal to − 47 pm/°C.

Bragg gratings are photo-inscribed in trans-4-stilbenemethanol doped PMMA fibers using a 325 nm He-Cd laser and a phase mask. Two distinct behaviors are reported depending on the laser power density. In the high-density regime with 637 mW/mm2, the grating reflectivity is stable over time after the writing process, but the reflected spectrum is of limited quality, as the grating length is limited to the laser width (1.2 mm). The beam is then enlarged to 6 mm, decreasing the power density to 127 mW/mm2. In this case, the grating reflectivity strongly decays after the writing process. A fortunate property here results from the recovery of the initial reflectivity using a post-inscription thermal annealing. Both behaviors are attributed to the evolution between trans- and cis-isomers.

We report the first excitation of surface plasmon waves at near-infrared telecommunication wavelengths using polymer optical fibers (POFs) made of poly(methyl methacrylate) (PMMA). For this, weakly tilted fiber-Bragg gratings (TFBGs) have been photo-inscribed in the core of step-index POFs and the fiber coated with a thin gold layer. Surface plasmon resonance is excited with radially polarized modes and is spectrally observed as a singular extinction of some cladding-mode resonances in the transmitted amplitude spectrum of gold-coated TFBGs. The refractometric sensitivity can reach ∼550 nm/RIU (refractive index unit) with a figure of merit of more than 2000 and intrinsic temperature self-compensation. This kind of sensor is particularly relevant to in situ operation.

We report the first slightly tilted Bragg gratings photo-inscription in polymer optical fiber (POF). For this, we make use of trans-4-stilbenemethanol-doped photosensitive step-index poly(methyl methacrylate) (PMMA) POFs. Tilted fiber Bragg gratings (TFBGs) are inscribed in the near-infrared wavelength range using the scanning phase mask technique with a tilted phase mask in the plane perpendicular to the laser beam direction. The transmitted amplitude spectrum evolution of a 3° TFBG is analyzed as a function of the surrounding refractive index. A maximum sensitivity close to 13 nm/RIU (refractive index unit) is obtained in the range 1.42-1.49.

We report on a pioneer thermal stability study of polymer optical fiber Bragg gratings (POFBGs) inscribed with a single laser pulse. The POFBG thermal decay follows a typical power-law function, which allowed us to simulate and predict POFBG lifetime for a maximum working temperature of 70 °C, for a working period up-to 1000 years.