1. Transformation of graphene oxide in supercritical media.
- Author
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Groshkova, Yu. A., Buslaeva, E. Yu., and Gubin, S. P.
- Subjects
- *
GRAPHENE oxide , *SUPERCRITICAL water , *ISOPROPYL alcohol , *SCANNING electron microscopy , *REDUCING agents , *GRAPHITE oxide - Abstract
Graphene oxide (GO) synthesized according to the modified Hummers method was reduced by supercritical isopropyl alcohol (SCI), supercritical acetone (SCA), and supercritical water (SCW). Methods free of toxic reducing agents were developed for the graphene production. The composition, morphology, and structure of synthesized graphene were determined using CHN analysis, XRD, Raman spectroscopy, and scanning electron microscopy. The best results were acquired in the case of GO reduction in SCA and SCI at high parameters. [ABSTRACT FROM AUTHOR]
- Published
- 2019
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