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Sulfonated Honeycomb Coral (HC-SOH), has been synthesized from the reaction of Honeycomb Coral with chlorosulfonic acid as sulfonating agent. The as-synthesized catalyst was characterized via XRF, FT-IR, TGA, SEM-EDS, XRD, BET and pH analysis. The superior catalytic activity of HC-SOH was investigated for the synthesis of 4,4′-(aryl methylene)bis(3-methyl-1 H-pyrazol-5-ol) derivatives through the one-pot pseudo-five component reactions. The main advantages of this protocol include simple procedure, excellent yields and short reaction times besides the non-toxicity, high stability and reusability of the catalyst. [ABSTRACT FROM AUTHOR]