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Objectives: The aim of our in vitro study was to quantitatively evaluate dentin microleakage by means of the impedance technique., Methods: Forty-five 2 mm thick dentin disks were embedded in a hollow polyurethane resin cylinder. The system used was a 'like' permeation cell. Standard cylindrical cavities (1.5 mm deep, 3.5 mm diameter) were prepared on the occlusal side of the disk. The current passing through the dentin was measured to calculate impedance and to establish resistance of the sample. The doses were then randomly divided into nine groups (n = 5). Each group was bounded with a different adhesive system and filled with microhybrid composite resin (Filtek P60). The initial measurement with the empty cavity and the record measurement (t = 0) were performed to evaluate initial resistance after filling. Samples were then thermocycled., Results: At t = 0, the highest value was obtained with EP (550%), the lowest with PLP (115%). The values of other adhesives ranged in a group (350-450%) without statistical difference. After thermocycling, all groups exhibited no significant difference (350-230%) except PLP (50%). The lower joint degradation rate (5%) was obtained with OS with a significant difference for all systems, the higher with PLP (35%). The results for other adhesives ranged from 20 to 27% without significant difference., Significance: Dentin microleakage may be quantified with the impedance technique and this has shown that, except for PLP, the differences between the two families of adhesives are slight. This methodology is able to prove the influence of thermocycling in terms of joint degradation., (Copyright 2003 Academy of Dental Materials)

Purpose: To evaluate quantitatively the effect of six contemporary self-etching systems on dentin permeability by means of the electrochemical impedance technique and to correlate these results with their acidity. Methods: 36 1.1 mm thick dentin disks were embedded in a hollow polyurethane resin cylinder. The system used was a "like" permeation cell: two electrodes immersed in a 10-1 KCl solution were attached to a potentiostat. It was connected to a microcomputer controlled frequency response analyzer, and a 10 mV sinusoidal voltage signal over a frequency range of 1 Hz to 65 kHz was applied between the electrodes. The current passing through the dentin was measured to enable a calculation of impedance expressed in a complex number. To establish an evaluation of permeability variation, the resistance was noted for all specimens before and after the application of self-etching adhesive. A pH meter used with a combined glass-electrode measured the pH of all the systems. Results: The higher decrease of the resistance of dentin samples was obtained with Experimental (EXP), which presented no significant difference with Touch and Bond (TB), Etch and Prime 3.0 (EP), and Etch Free Tenure (RF). These acidic monomers improved the dentin permeability respectively to 6.7, 5.1, 5.0 and 5.0%. The lowest values were obtained with Clearfil EE Bond (SEB) (2.0%), which showed significant difference with all the other systems. Prompt L-Pop (PLP) with 4.3% showed significant difference with EXP and SEB and no significant difference with the three other systems. The pH and permeability variation were not systematically correlated. [ABSTRACT FROM AUTHOR]