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Start Over Author "Song, Xiao-Nan" Topic dimethylformamide
1 results on '"Song, Xiao-Nan"'

1. Copper(I)-Mediated Direct Trifluoromethylthiolation of Allylic Halides with Elemental Sulfur and (Trifluoromethyl)trimethylsilane.

Author

Li, Jue, Wang, Peiqiang, Xie, Fei‐Fei, Yang, Xi‐Gang, Song, Xiao‐Nan, Chen, Wei‐Dong, Ren, Jiangmeng, and Zeng, Bu‐Bing

Subjects
HALIDES, POTASSIUM fluoride, DIMETHYLFORMAMIDE, TRIFLUOROMETHYL compounds, SULFIDES
Abstract

A new method has been developed for the copper-mediated trifluoromethylthiolation of allylic halides by using potassium fluoride, elemental sulfur, and (trifluoromethyl)trimethylsilane in anhydrous N, N-dimethylformamide. This protocol provides facile access to a variety of allylic trifluoromethyl thioethers in moderate to good yields under mild, ligand-free reaction conditions. [ABSTRACT FROM AUTHOR]

Published
2015
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