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[Display omitted] • An exploratory routine was carried out for a novel NSP-rich ingredient. • Interactions with water and exposure to high and low temperatures were studied. • Sorption isotherms of ripe bananas non-starch polysaccharides samples were Type III. • State diagrams of non-starch polysaccharides NSP from ripe bananas were built. • The stability criterion between water activity and glass transition was studied. In this work, an ingredient containing non-starch polysaccharides (NSP), obtained from overripe bananas, was characterized using differential scanning calorimetry (DSC) and vapor sorption isotherms. Soluble sugars from overripe bananas were extracted using ethanol, resulting in a solid NSP-rich fraction. The physical properties of this new ingredient and its response to temperature and water interactions are needed for its application as a fiber flour aggregate in food preparations. Results from thermal analyses, including gelatinization, glass transition and fusion, allowed building state diagrams, then compared to vapor sorption isotherms which resulted similar to a Brunauer–Emmet–Teller (BET) type III isotherm at 25 °C, for NSP and standards samples as arabinoxylan and polygalacturonic acid. A good fit was obtained for the glass transition curves using the Kwei model. This approach enabled us to explore the stability of the material, regarding safety limits for microbial deterioration and structural changes due to glass transition. [ABSTRACT FROM AUTHOR]

Unripe acerola powders obtained from freeze-drying without (AV) and with polydextrose (AP) were characterized by using differential scanning calorimetry (DSC) and vapor sorption isotherms at (25, 35, and 45) °C in water activity (a w) range of 0.10–0.90. State diagrams built from DSC results, such as the glass transition (T g) and freezing (T m) points, were compared with those of the sorption isotherms. The Gordon-Taylor equation presented a good fit for T g , in which the solids glass transition increased and the k parameter decreased in the presence of polydextrose. The isotherms obtained were Brunauer-Emmett-Teller (BET) type III, and the Guggenheim-Anderson-de Boer (GAB) equation fitted to the experimental data showed slightly higher monolayer water content for AP, and not affected by temperature. Although there was a divergence in the stability when comparing the criteria of a w and T g , polydextrose increased the a w and T g of freeze-dried unripe acerola and conferred a stabler powder. • The stability criterion between water activity and glass transition was studied. • State diagrams of unripe acerola with polydextrose were built. • Polydextrose used as a drying aid increased the glass transition temperature. • Sorption isotherms of unripe acerola powders were BET Type III. [ABSTRACT FROM AUTHOR]