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Objective: To evaluate the effect of ethanol wet bonding technique on the immediate and long term bond strength of simplified etch and rinse adhesive systems to dentin., Study Design: 96 extracted human permanent molars were ground to expose the flat dentin surface. The teeth were divided into four groups (n=24) according to the adhesives used, either Tetric N Bond or Solobond M and bonding techniques i.e. water wet bonding or ethanol wet bonding (EWB). Composite cylinder was bonded to each specimen using the respective adhesive technique. Ten samples from each group were then tested immediately for shear bond strength evaluation and two samples for SEM analysis. The remaining samples (12) were tested after 6 month storage in distilled water., Results: Upon immediate testing, there was no significant difference in the mean shear bond strength of the groups regardless of the bonding technique or adhesive used. The bond strength fell dramatically in the water wet bonded specimens after 6 months water storage, while the bond strength of both the adhesives was maintained when EWB technique was used. SEM observation revealed good interfacial adaptation in EWB groups even after six months., Conclusion: For both simplified etch and rinse adhesives used, ethanol wet bonding technique led to significant preservation of the resin dentin bond over 6 months.

Aim: The aim of the present study was to determine the effect of ethylenediaminetetraacetic acid (EDTA) and NaOCl irrigation on the microleakage and interfacial morphology of adhesives bonded to pulp chamber dentin., Methods: The pulp chamber roof of 72 extracted permanent molars was removed. Samples were equally divided into six groups. Pulp chamber dentin was bonded with either Adper Easy One (group 1), Adper Prompt L-Pop (group 2), or Adper Single Bond 2 (Group 3), after irrigation with either normal saline (groups 1a, 2a, 3a) or 17% EDTA and 5.25% NaOCl (groups 1b, 2b, 3b). Composite resin restorations were placed in the pulp chamber. Ten samples per group were subjected to microleakage test and scanning electron microscopic analysis was done in two samples from each group. Data were statistically analyzed using Mann-Whitney and Kruskal Wallis tests at a significance level of P < 0.05., Results: EDTA and NaOCl irrigation of the pulp chamber significantly reduced microleakage in Adper Easy One. However, it had no significant effect on the microleakage of Adper Prompt L-Pop and Adper Single Bond 2., Conclusions: EDTA and NaOCl irrigation of the pulp chamber was not deleterious to the bonding of any of the adhesives tested. While this irrigation regimen had no significant effect on the microleakage of Adper Prompt L-Pop and Adper Single Bond 2, it significantly reduced the microleakage scores in Adper Easy One., (© 2014 Wiley Publishing Asia Pty Ltd.)

Aim: To evaluate the effect of additional enamel etching on the shear bond strength of three self-etch adhesives., Methods: Class II box type cavities were made on extracted human molars. Teeth were randomly divided into one control group of etch and rinse adhesive and three test groups of self-etch adhesives (Clearfil S3 Bond, Futurabond NR, Xeno V). The teeth in the control group (n = 10) were treated with Adper™ Single Bond 2. The three test groups were further divided into two subgroups (n = 10): (i) self-etch adhesive was applied as per the manufacturer's instructions; (ii) additional etching of enamel surfaces was done prior to the application of self-etch adhesives. All cavities were restored with Filtek Z250. After thermocycling, shear bond strength was evaluated using a Universal testing machine. Data were analyzed using anova independent sample's 't' test and Dunnett's test. The failure modes were evaluated with a stereomicroscope at a magnification of 10×., Results: Additional phosphoric acid etching of the enamel surface prior to the application of the adhesive system significantly increased the shear bond strength of all the examined self-etch adhesives., Conclusions: Additional phosphoric acid etching of enamel surface significantly improved the shear bond strength., (© 2013 Wiley Publishing Asia Pty Ltd.)

Objective: To analyze the effect of proanthocyanidin (PA) treatment of the pulp chamber dentin after NaOCl and EDTA irrigation on the microleakage and interfacial morphology of adhesive restorations., Study Design: Pulp chambers of 66 extracted permanent molars were exposed. In half of the samples, pulp chamber dentin was bonded with Clearfil S3 after irrigation with normal saline (Group1a); 1% NaOCl and 17% EDTA (Group1b) or 1% NaOCl, 17% EDTA and 30% PA (Group1c) and in other half samples, pulp chamber dentin was bonded with Futurabond NR after irrigation with normal saline (Group 2a); 1% NaOCl and 17% EDTA (Group 2b) or 1% NaOCl, 17% EDTA and 30% PA (Group 2c). After adhesive procedures, Filtek Z 250 restorations were placed in the pulp chambers. Microleakage assessment was done in ten samples from each group and scanning electron microscopic examination was done in one sample from each group. Statistical analysis was done using Mann-Whitney and Kruskal Wallis tests at a significance level of P<0.05., Results: Both the adhesives showed extensive microleakage. NaOCl and EDTA irrigation had no significant effect on the microleakage of both the adhesives. PA treatment of the pulp chamber dentin after NaOCl and EDTA irrigation significantly reduced microleakage in both the adhesives., Conclusion: It was concluded that 1 minute application of 30% proanthocyanidin solution in the pulp chamber after NaOCl and EDTA irrigation improved the subsequent bonding of self-etch adhesives to pulp chamber dentin.

Contemporary dental adhesives show favorable immediate results in terms of bonding effectiveness. However, the durability of resin-dentin bonds is their major problem. It appears that simplification of adhesive techniques is rather detrimental to the long-term stability of resin-tooth interface. The hydrostatic pulpal pressure, the dentinal fluid flow and the increased dentinal wetness in vital dentin can affect the intimate interaction of certain dentin adhesives with dentinal tissue. Bond degradation occurs via water sorption, hydrolysis of ester linkages of methacrylate resins, and activation of endogenous dentin matrix metalloproteinases. The three-step etch-and-rinse adhesives still remain the gold standard in terms of durability. This review discusses the fundamental process of adhesion to enamel and dentin with different adhesive techniques, factors affecting the long-term bonding performance of modern adhesives and addresses the current perspectives for improving bond durability.

Purpose: The purpose of this study was to analyze the effect of additional enamel etching and hydrophobic layer application on microleakage of 1-step self-etch adhesives., Methods: Class V cavities were made on the buccal surfaces of 80 extracted human premolars. The teeth were divided into 2 test groups according to the 1-step self-etch adhesive used: Clearfil S(3) Bond and Xeno III. Each test group was subdivided into 4 groups (n=10) according to application mode of the adhesive: (1) Group 1=adhesive applied following manufacturer's directions; (2) Group 2=enamel etching prior to adhesive application; (3) Group 3=same as Group 1, plus application of an additional coat of hydrophobic resin layer; (4) Group 4=same as Group 2, plus application of an additional coat of hydrophobic resin layer. The adhesives were light cured, and the cavities were filled with resin composite. Specimens were thermocycled and analyzed for leakage using Kruskal-Wallis and Mann-Whitney U test at a significance level of P=.05., Results: Enamel etching significantly reduced leakage in both the adhesives. Hydrophobic resin layer application significantly reduced leakage in Xeno III., Conclusions: An additional acid etching step and hydrophobic resin layer application can improve the bonding of 1-step self-etched adhesives to enamel and dentin, respectively.

Aim: To comparatively evaluate the shear bond strength of recent tooth-colored restorative materials to dentin., Materials and Methods: Flat dentinal surface were prepared from 60 caries free, extracted human permanent molars and were mounted in acrylic rings. These were randomly divided into four groups - Group A to Group D, according to the restorative material used i.e. Glass ionomer cement (Fuji IX), Giomer (Beautifil), an Ormocer-based composite (Admira) and Nano Ceramic restorative material (Ceram X). These restorative materials were applied on dentinal surface of all the specimens using nylon cylinders. The mounted samples were stored in distilled water for 24 hours and thermocycled. They were then subjected to shear bond strength test using universal testing machine. Data was analyzed using a one-way analysis of variance (ANOVA) and student's 't'-test., Results: Ceram X (16.63 ± 0.94 MPa) and Admira (17.31 ± 0.95 MPa) were comparable in their bond strength values, but depicted significantly higher bond strength when compared to Beautifil (12.39 ± 1.05 MPa) and Fuji IX (7.76 ± 1.07 MPa)., Conclusion: Nano-ceramic and ormocer-based restorative materials showed better bonding potential to dentin as compared to GIC and Giomer.