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The Koum Basin is one of major intracontinental basins in northern Cameroon. It is part of the Upper Benue Trough and has genetic ties to the West and Central African Rift System. The main purpose of studying the Koum Basin sedimentary deposits was to re-examine the time of the deposition and constrain the palaeoenvironmental and paleoclimatic conditions during deposition. To accomplish this, we used a combination of sedimentologic, palynologic, mineralogic, and geochemical data. Claystone units interbedded with calcareous siltstones dominate sedimentary sequence, including few clay beds, fine to medium-grained sandstone, and rare marl layers. The palynomorph assemblage suggests a previously unknown Maastrichtian – Paleocene age in this basin. The sediments originated from intermediate igneous parent rocks with a relative contribution of felsic rocks. These rocks underwent low detritism (Si/Al: 2.51–4.43; K/Al: 0.11–0.36; Ti/Al: 0.05–0.10) and chemical weathering (CIA: 55–64; PIA: 56–68) in the source region. Consequently, deposits are immature (ICV values > 1) and weakly recycled (Si 2 O 3 /Al 2 O 3 ratios ≤5). The organic matter analysis and the palynoflora assemblage, reveal Type III kerogen with significant contributions of Type II-III and type II kerogens, as well as a continental paleo-depositional environment with open rainforest to savannah vegetation. The clay minerals distribution suggests moderate illitization and chloritization processes and thus moderate burial diagenesis at temperatures ranging from 70 to 90 °C, also attested by immature to mature Tmax values (≤436 °C) marginally. The low CIA values and very low kaolinite contents, indicate dry climatic conditions. In addition, two major-element-based discrimination diagrams show that the parent rocks of clastic sediments formed primarily in a continental arc system, with a moderate contribution from the rift system and a low contribution from the oceanic island arc, implying compressional conditions, which is consistent with previous studies on the tectonic background of the region during the late Maastrichtian to Paleocene period. • The first Maastrichtian – Paleocene record from the Koum Basin, Upper Benue Trough, northern Cameroon. • Illitization and chloritization processes point moderate burial diagenesis, and immature to marginally mature organic matter. • Pollen and spores, clay minerals, and CIA all hint to a semi-arid environment with open rainforest to savannah vegetation. • Compressional tectonic conditions were discovered in the Koum Basin at this period. [ABSTRACT FROM AUTHOR]