1. Effect of the addition of t-ZrO2 on the material properties of β-TCP/PCL composites
- Author
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Ho-Yeon Song, Do Van Quang, Byong-Taek Lee, and Young-Ki Min
- Subjects
Materials science ,Scanning electron microscope ,Mechanical Engineering ,Methacrylate ,Ceramic matrix composite ,chemistry.chemical_compound ,Flexural strength ,chemistry ,Mechanics of Materials ,Polycaprolactone ,Relative density ,General Materials Science ,Composite material ,Porosity ,Elastic modulus - Abstract
Using poly-methyl methacrylate as a pore-forming agent, porous β-tricalcium phosphate (β-TCP)/t-ZrO2 composites were fabricated depending on the volume percentages (vol.%) of t-ZrO2 powder. In the porous sintered bodies, hybrid pores, about 20 and 200 μm in diameter, were homogenously dispersed in the β-TCP/t-ZrO2 matrix and showed good interconnection. On the other hand, β-TCP-(t-ZrO2)/polycaprolactone (PCL) composites were fabricated by the melt infiltration process using porous β-TCP/t-ZrO2 bodies. The relative density of the β-TCP-(t-ZrO2)/PCL composites increased as the vol.% of t-ZrO2 increased and its maximum value was about 98.6%. However, the hardness, bending strength and elastic modulus of β-TCP-(t-ZrO2)/PCL composites decreased due to the low densification of porous β-TCP/t-ZrO2 bodies as the volume percentages of t-ZrO2 content increased. The values (using 20 vol.% of t-ZrO2) were 11.4 Hv, 25.5 MPa and 17.2 GPa, respectively.
- Published
- 2008