Author: "Comotti, A." / Topic: chemistry - Searchworks@Jio Institute Digital Library Search Results

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1. Phosphine Oxide Porous Organic Polymers Incorporating Cobalt(II) Ions: Synthesis, Characterization, and Investigation of H2 Production

Author: Giulia Bonfant, Davide Balestri, Jacopo Perego, Angiolina Comotti, Silvia Bracco, Matthieu Koepf, Marcello Gennari, and Luciano Marchiò
Subjects: Chemistry, QD1-999
Published: 2022
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2. Ultrasound Elastography in the Evaluations of Tendon-Related Disorders—A Systematic Review

Author: Gianluca Rossetto, Emilia Scalona, Paolo Comotti, Lorenzo Gatti, Denise Di Maso, Massimiliano Gobbo, and Nicola Francesco Lopomo
Subjects: ultrasound elastography, strain elastography, shear wave elastography, tendon-related disorders, Technology, Engineering (General). Civil engineering (General), TA1-2040, Biology (General), QH301-705.5, Physics, QC1-999, Chemistry, QD1-999
Abstract: Tendon-related disorders are a common condition in both sports medicine and orthopedic clinical practice. Ultrasonography, power doppler, and magnetic resonance imaging (MRI) are the most widespread technologies, but the use of ultrasound elastography—including strain elastography and shear wave elastography—has been increasing in the last years. The aim of this paper is to evaluate the use of ultrasound elastography in tendon-related disorders. Research in PubMed, Scopus, and Web of Science databases is performed, and 364 papers are exported. After the study selection process, 38 papers are included in this systematic review. The risk of bias of each paper is evaluated using the RoBANS tool. Blinding, confounding variables, and measurement of exposure are the most affected items. From the included papers, tendinopathy is the most analyzed pathology, followed by tenosynovitis and rotator cuff disease. The Achilles tendon, patellar tendon, and common extensor tendon of the hand are the most analyzed tendons. Ultrasound elastography results in being the method providing good sensitivity and specificity (up to 100% and 100%, respectively, in tendinosis of the long head of the biceps tendon, in transverse plan examination) and accuracy (up to 97.8% in Achilles tendinopathy); furthermore, this technique is able to ensure real-time feedback on tissue elasticity and appears more sensitive than B-mode alone.
Published: 2023
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3. Cascade Dynamics of Multiple Molecular Rotors in a MOF: Benchmark Mobility at a Few Kelvins and Dynamics Control by CO2

Author: Silvia Bracco, J Perego, Pietro Carretta, Angiolina Comotti, Charl X. Bezuidenhout, Piero Sozzani, Giacomo Prando, M Negroni, Luciano Marchiò, Perego, J, Bezuidenhout, C, Bracco, S, Prando, G, Marchio, L, Negroni, M, Carretta, P, Sozzani, P, and Comotti, A
Subjects: molecular rotors, dynamics, Pillared-MOFs, 2H solid-echo NMR, T1(1H) relaxation time, CO2, business.industry, Spin–lattice relaxation, Rotation around a fixed axis, General Chemistry, CHIM/04 - CHIMICA INDUSTRIALE, Rotation, Biochemistry, Article, Catalysis, Mechanism (engineering), Bipyridine, chemistry.chemical_compound, Colloid and Surface Chemistry, chemistry, Chemical physics, Cascade, Benchmark (computing), business, Thermal energy
Abstract: Achieving sophisticated juxtaposition of geared molecular rotors with negligible energy-requirements in solids enables fast yet controllable and correlated rotary motion to construct switches and motors. Our endeavor was to realize multiple rotors operating in a MOF architecture capable of supporting fast motional regimes, even at extremely cold temperatures. Two distinct ligands, 4,4′-bipyridine (bipy) and bicyclo[1.1.1]pentanedicarboxylate (BCP), coordinated to Zn clusters fabricated a pillar-and-layer 3D array of orthogonal rotors. Variable temperature XRD, 2H solid-echo, and 1H T1 relaxation NMR, collected down to a temperature of 2 K revealed the hyperfast mobility of BCP and an unprecedented cascade mechanism modulated by distinct energy barriers starting from values as low as 100 J mol–1 (24 cal mol–1), a real benchmark for complex arrays of rotors. These rotors explored multiple configurations of conrotary and disrotary relationships, switched on and off by thermal energy, a scenario supported by DFT modeling. Furthermore, the collective bipy-ring rotation was concerted with the framework, which underwent controllable swinging between two arrangements in a dynamical structure. A second way to manipulate rotors by external stimuli was the use of CO2, which diffused through the open pores, dramatically changing the global rotation mechanism. Collectively, the intriguing gymnastics of multiple rotors, devised cooperatively and integrated into the same framework, gave the opportunity to engineer hypermobile rotors (107 Hz at 4 K) in machine-like double ligand MOF crystals.
Published: 2021

4. Anionic Polymerization in Porous Organic Frameworks: A Strategy to Fabricate Anchored Polymers and Copolymers

Author: Jacopo Perego, Silvia Bracco, Angiolina Comotti, Daniele Piga, Irene Bassanetti, Piero Sozzani, Perego, J, Bracco, S, Comotti, A, Piga, D, Bassanetti, I, and Sozzani, P
Subjects: chemistry.chemical_classification, Materials science, Chain propagation, materials science, 010405 organic chemistry, nanoparticle, porous framework, Nanoparticle, General Medicine, General Chemistry, Polymer, CHIM/04 - CHIMICA INDUSTRIALE, 010402 general chemistry, 01 natural sciences, Catalysis, 0104 chemical sciences, Anionic addition polymerization, Chemical engineering, Solid-state nuclear magnetic resonance, chemistry, Polymerization, Covalent bond, polymerization, Copolymer, solid-state NMR
Abstract: An anionic mechanism is used to create polymers and copolymers as confined to, or anchored to, high-surface-area porous nanoparticles. Linear polymers with soft and glassy chains, such as polyisoprene and polymethylmethacrylate, were produced by confined anionic polymerization in 3D networks of porous aromatic frameworks. Alternatively, multiple anions were generated on the designed frameworks which bear removal protons at selected positions, and initiate chain propagation, resulting in chains covalently connected to the 3D network. Such growth can continue outside the pores to produce polymer-matrix nanoparticles coated with anchored chains. Sequential reactions were promoted by the living character of this anionic propagation, yielding nanoparticles that were covered by a second polymer anchored by anionic block copolymerization. The intimacy of the matrix and the grown-in polymers was demonstrated by magnetization transfer across the interfaces in 2D 1 H-13 C-HETCOR NMR spectra.
Published: 2021

5. Fast motion of molecular rotors in metal–organic framework struts at very low temperatures

Author: Giacomo Prando, Charl X. Bezuidenhout, J Perego, Angiolina Comotti, M Negroni, Silvia Bracco, Piero Sozzani, Pietro Carretta, Perego, J, Bracco, S, Negroni, M, Bezuidenhout, C, Prando, G, Carretta, P, Comotti, A, and Sozzani, P
Subjects: Bicyclic molecule, 010405 organic chemistry, General Chemical Engineering, Supramolecular chemistry, General Chemistry, Cubic crystal system, CHIM/04 - CHIMICA INDUSTRIALE, 010402 general chemistry, Rotation, Crystal engineering, 01 natural sciences, Molecular machine, 0104 chemical sciences, CHIM/02 - CHIMICA FISICA, chemistry.chemical_compound, Crystallography, chemistry, molecular rotors, molecular dynamics, MOFs, solid state NMR, spin–lattice relaxation times, energy barrier, Metal-organic framework, Carboxylate
Abstract: The solid state is typically not well suited to sustaining fast molecular motion, but in recent years a variety of molecular machines, switches and rotors have been successfully engineered within porous crystals and on surfaces. Here we show a fast-rotating molecular rotor within the bicyclopentane–dicarboxylate struts of a zinc-based metal–organic framework—the carboxylate groups anchored to the metal clusters act as an axle while the bicyclic unit is free to rotate. The three-fold bipyramidal symmetry of the rotator conflicts with the four-fold symmetry of the struts within the cubic crystal cell of the zinc metal–organic framework. This frustrates the formation of stable conformations, allowing for the continuous, unidirectional, hyperfast rotation of the bicyclic units with an energy barrier of 6.2 cal mol−1 and a high frequency persistent for several turns even at very low temperatures (1010 Hz below 2 K). Using zirconium instead of zinc led to a different metal cluster–carboxylate coordination arrangement in the resulting metal–organic framework, and much slower rotation of the bicyclic units. Molecular rotors have been engineered within the bicyclopentane–dicarboxylate struts of a metal–organic framework—the bicyclic unit is the rotator and the carboxylate groups serve as the stator. In a zinc-based metal–organic framework, the crossed conformation of the strut–metal nodes enables fast rotation of the bicyclic moiety, but in the corresponding zirconium metal–organic framework a change in the conformation results in much slower rotation.
Published: 2020

6. Modulation of porosity in a solid material enabled by bulk photoisomerization of an overcrowded alkene

Author: Wojciech Danowski, Franco King Chi Leung, Angiolina Comotti, Piero Sozzani, Silvia Bracco, F Castiglioni, Ben L. Feringa, J Perego, Sander J. Wezenberg, Castiglioni, F, Danowski, W, Perego, J, Leung, F, Sozzani, P, Bracco, S, Wezenberg, S, Comotti, A, Feringa, B, and Synthetic Organic Chemistry
Subjects: chemistry.chemical_classification, Bistability, Photoisomerization, 010405 organic chemistry, Alkene, General Chemical Engineering, photoswitchable molecules, porosity, responsive materials, photoisomerization, ssNMR,gas adsorption, General Chemistry, CHIM/04 - CHIMICA INDUSTRIALE, 010402 general chemistry, Photochemistry, 01 natural sciences, 0104 chemical sciences, CHIM/02 - CHIMICA FISICA, chemistry.chemical_compound, symbols.namesake, Adsorption, chemistry, symbols, Molecule, Porosity, Raman spectroscopy, Tetraphenylmethane
Abstract: The incorporation of photoswitchable molecules into solid-state materials holds promise for the fabrication of responsive materials, the properties of which can be controlled on-demand. However, the possible applications of these materials are limited due to the restrictions imposed by the solid-state environment on the incorporated photoswitches, which render the photoisomerization inefficient. Here we present responsive porous switchable framework materials based on a bistable chiroptical overcrowded alkene incorporated in the backbone of a rigid aromatic framework. As a consequence of the high intrinsic porosity, the resulting framework readily responds to a light stimulus, as demonstrated by solid-state Raman and reflectance spectroscopies. Solid-state 13C NMR spectroscopy highlights an efficient and quantitative bulk photoisomerization of the incorporated light-responsive overcrowded olefins in the solid material. Taking advantage of the quantitative photoisomerization, the porosity of the framework and the consequent gas adsorption can be reversibly modulated in response to light and heat. Despite numerous potential applications, the development of light-responsive solid materials based on molecular photoswitches is impeded by the low efficiency of photoisomerization in the solid environment. Now a robust, solid porous material made from tetraphenylmethane and a photoswitchable overcrowded alkene exhibits nearly quantitative photoisomerization in the bulk and in photomodulation of gas uptake.
Published: 2020

7. Carbonization of single polyacrylonitrile chains in coordination nanospaces

Author: Xiyuan Zhang, Silvia Bracco, Takashi Uemura, D Piga, Angiolina Comotti, Takashi Kitao, Piero Sozzani, Ryoto Hongu, Zhang, X, Kitao, T, Piga, D, Hongu, R, Bracco, S, Comotti, A, Sozzani, P, and Uemura, T
Subjects: Materials science, Carbonization, Polyacrylonitrile, General Chemistry, Conjugated system, CHIM/04 - CHIMICA INDUSTRIALE, Structural evolution, Chemical reaction, Chemistry, chemistry.chemical_compound, chemistry, Chemical engineering, polyacrylonitrile, PAN, MOF, polymer confinement, carbonization, carbon fibers, ss-NMR, Ladder polymer, Bond cleavage
Abstract: It has been over half a century since polyacrylonitrile (PAN)-based carbon fibers were first developed. However, the mechanism of the carbonization reaction remains largely unknown. Structural evolution of PAN during the preoxidation reaction, a stabilization reaction, is one of the most complicated stages because many chemical reactions, including cyclization, dehydration, and cross-linking reactions, simultaneously take place. Here, we report the stabilization reaction of single PAN chains within the one-dimensional nanochannels of metal–organic frameworks (MOFs) to study an effect of interchain interactions on the stabilization process as well as the structure of the resulting ladder polymer (LP). The stabilization reaction of PAN within the MOFs could suppress the rapid generation of heat that initiates the self-catalyzed reaction and inevitably provokes many side-reactions and scission of PAN chains in the bulk state. Consequently, LP prepared within the MOFs had a more extended conjugated backbone than the bulk condition., Accommodation of polyacrylonitrile in MOFs facilitated and regulated the transformation to ladder polymer in the carbonization process.
Published: 2020

8. Reorientable fluorinated aryl rings in triangular channel Fe-MOFs: an investigation on CO2–matrix interactions

Author: Charl X. Bezuidenhout, J Perego, Silvia Bracco, Piero Sozzani, Angiolina Comotti, Alessandro Pedrini, M Negroni, Perego, J, Bezuidenhout, C, Pedrini, A, Bracco, S, Negroni, M, Comotti, A, and Sozzani, P
Subjects: Materials science, Renewable Energy, Sustainability and the Environment, Aryl, Fe-MOFs, CO2 adsorption, solid state NMR, 129Xe NMR, microcalorimetry, adsorption enthalpy, Supramolecular chemistry, chemistry.chemical_element, 02 engineering and technology, General Chemistry, CHIM/04 - CHIMICA INDUSTRIALE, 010402 general chemistry, 021001 nanoscience & nanotechnology, Ring (chemistry), 01 natural sciences, 0104 chemical sciences, Turn (biochemistry), CHIM/02 - CHIMICA FISICA, Paramagnetism, Crystallography, chemistry.chemical_compound, Adsorption, chemistry, Fluorine, Molecule, General Materials Science, 0210 nano-technology
Abstract: The realization of tunable and functionalized MOFs is a winning strategy for CO2 capture. Here we report on a series of robust Fe-MOFs with triangular channels constructed by rod-like fluorinated pyrazolate ligands, comprising an increasing number of fluorine atoms on the central p-phenylene core (F = 1, 2, and 4). This yielded a series of isoreticular frameworks, engineered with orientational flexibility of the fluorinated aryl rings pivoted on ethynyl groups with an sp2–sp soft rotary barrier, providing a stable axel, which supported reorientable C–F dipoles. A combined approach, including powder X-ray diffraction, multinuclear solid-state NMR (2D 1H–13C, 19F, hyperpolarized 129Xe NMR and distance measurements by paramagnetic shift), gas-adsorption and microcalorimetry, enabled the exhaustive description of the fluorinated ring arrangement and the organization of functionalized sites for accommodating CO2. In the tetrafluoro-aryl-derivative MOF, protrusion of perfluorinated rings towards the channel space plays a major role in CO2 capture. Partially fluorinated aryl rings of mono- and di-fluoro MOFs turn to retract into the channel-walls to form continuous ribbons of inter-strut supramolecular interactions, contributing to the robustness of the overall architecture. Detailed computational models obtained using GCMC and DFT of CO2 diffusion and interactions in MOFs showed how the gas molecules approach the channel walls. The highly occupied sites are aligned at the corners of the triangular channels, wherein fluorine atoms participate in host–CO2 interactions. A CO2–matrix adsorption enthalpy of 33 kJ mol−1, suitable for capture/delivery cycles, was accurately measured in situ by simultaneous acquisition of microcalorimetric and volumetric-isotherm data. Thus, the designed advantages of rotationally flexible fluorinated moieties were successfully explored.
Published: 2020

9. Composite fast scintillators based on high-Z fluorescent metal–organic framework nanocrystals

Author: J Perego, Alessandro Pedrini, L. Gironi, Angelo Monguzzi, E. C. Padovani, Christophe Dujardin, Anna Vedda, Silvia Bracco, Etiennette Auffray, I Villa, Angiolina Comotti, Francesco Meinardi, M Beretta, Piero Sozzani, Matteo Salomoni, R Crapanzano, Charl X. Bezuidenhout, Stefan Gundacker, Nicolaus Kratochwil, Dipartimento di Scienza dei Materiali = Department of Materials Science [Milano-Bicocca], Università degli Studi di Milano-Bicocca [Milano] (UNIMIB), Luminescence (LUMINESCENCE), Institut Lumière Matière [Villeurbanne] (ILM), Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Centre National de la Recherche Scientifique (CNRS)-Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Centre National de la Recherche Scientifique (CNRS), Dipartimento di Fisica 'Giuseppe Occhialini' = Department of Physics 'Giuseppe Occhialini' [Milano-Bicocca], European Organization for Nuclear Research (CERN), University of Vienna [Vienna], Perego, J, Villa, I, Pedrini, A, Padovani, E, Crapanzano, R, Vedda, A, Dujardin, C, Bezuidenhout, C, Bracco, S, Sozzani, P, Comotti, A, Gironi, L, Beretta, M, Salomoni, M, Kratochwil, N, Gundacker, S, Auffray, E, Meinardi, F, and Monguzzi, A
Subjects: Materials science, Physics::Instrumentation and Detectors, sicintillator, fast emitter, Nanoparticle, Physics::Optics, 02 engineering and technology, Scintillator, 01 natural sciences, Particle detector, 010309 optics, [SPI]Engineering Sciences [physics], met-organic framework, 0103 physical sciences, X-rays, [CHIM]Chemical Sciences, MOF, chemistry.chemical_classification, [PHYS]Physics [physics], Scintillation, Nanoscale materials, business.industry, Photonic devices, Polymer, composite material, 021001 nanoscience & nanotechnology, Fluorescence, Atomic and Molecular Physics, and Optics, Electronic, Optical and Magnetic Materials, chemistry, Optics and photonics, nnocrystal, Picosecond, Optoelectronics, Nanoparticles, 0210 nano-technology, business, Ultrashort pulse
Abstract: Scintillators, materials that produce light pulses upon interaction with ionizing radiation, are widely employed in radiation detectors. In advanced medical-imaging technologies, fast scintillators enabling a time resolution of tens of picoseconds are required to achieve high-resolution imaging at the millimetre length scale. Here we demonstrate that composite materials based on fluorescent metal–organic framework (MOF) nanocrystals can work as fast scintillators. We present a prototype scintillator fabricated by embedding MOF nanocrystals in a polymer. The MOF comprises zirconium oxo-hydroxy clusters, high-Z linking nodes interacting with the ionizing radiation, arranged in an orderly fashion at a nanometric distance from 9,10-diphenylanthracene ligand emitters. Their incorporation in the framework enables fast sensitization of the ligand fluorescence, thus avoiding issues typically arising from the intimate mixing of complementary elements. This proof-of-concept prototype device shows an ultrafast scintillation rise time of ~50 ps, thus supporting the development of new scintillators based on engineered fluorescent MOF nanocrystals. Composites of fluorescent metal–organic framework nanocrystals in a polymer are exploited to create fast scintillators with a rise time of about 50 ps.
Published: 2021

10. Calixarene-based porous 3D polymers and copolymers with high capacity and binding energy for CO2, CH4 and Xe capture

Author: Angiolina Comotti, Piero Sozzani, Alessandro Pedrini, J Perego, Silvia Bracco, Charl X. Bezuidenhout, Pedrini, A, Perego, J, Bracco, S, Bezuidenhout, C, Sozzani, P, and Comotti, A
Subjects: chemistry.chemical_classification, Calixarene-based porous 3D polymers. Yamamoto coupling reaction, CO2, CH4, Xe, hierarchical porosity, gas selectivity, ssNMR, HP Xe NMR, Renewable Energy, Sustainability and the Environment, Hydrogen bond, Supramolecular chemistry, General Chemistry, Polymer, CHIM/04 - CHIMICA INDUSTRIALE, Combinatorial chemistry, chemistry.chemical_compound, Monomer, chemistry, Covalent bond, Calixarene, Copolymer, General Materials Science, Conformational isomerism
Abstract: The supramolecular capacity of calixarenes towards guests is largely consolidated; in contrast, the synthesis of porous calixarene-based frameworks by covalent bond formation is still a challenge. Our target was to yield 3D polymers and copolymers based on calixarenes for selective gas-capture, endowed with easy pore accessibility and specific sites, and built via a straightforward synthetic route. The covalent calixarene frameworks (CXFs) were prepared by the Yamamoto coupling reaction starting from tetrabromo calixarene propoxy- and methoxy-monomers of three stable calixarene (partial cone, effective cone, and 1,3-alternate) conformers and complete post-synthetic deprotection to achieve polar phenolic calixarene derivatives. Moreover, the copolymer of calixarene-based monomers with tetrabromo-tetraphenylmethane exhibited remarkable surface area up to about 3000 m2 g−1. Smart architectures endowed with hierarchical porosity from micro- to meso-porosity showed notable sponge-like swellability by CO2, which was captured effectively at room temperature, even in competition with N2, yielding CO2 removal in column breakthrough experiments. Indeed, CXFs displayed excellent CO2 and CH4 energy binding of 35 and 24 kJ mol−1, respectively. Ultramicropore sites were highlighted by Xe capture and in situ detection after a xenon diffusion time of a few milliseconds, by laser-assisted hyperpolarized 129Xe NMR, revealing the accessibility of calixarene capsules and the available space. This synthetic route demonstrated the possibility to modulate at will the pore capacity and selectivity, displaying porous frameworks with two distinct pore families, wherein calixarene moieties play the role of small and selective sites. A contractile behavior of the frameworks was observed upon deprotection which produced more polar sites, due to the formation of hydrogen bond networks.
Published: 2021

11. Synthesis, crystal structure, and optical properties of fluorinated poly(pyrazole) ligands and in silico assessment of their affinity for volatile organic compounds

Author: Alessandro Pedrini, Luciano Marchiò, Piero Sozzani, Simona Galli, Massimo Mella, Angiolina Comotti, Silvia Bracco, Luca Nardo, Andrea Penoni, Angelo Maspero, Luca Scapinello, Guglielmo Vesco, Pedrini, A, Maspero, A, Bracco, S, Comotti, A, Galli, S, Marchio, L, Nardo, L, Penoni, A, Scapinello, L, Sozzani, P, Vesco, G, and Mella, M
Subjects: Molecular model, Hydrogen bond, Chemistry, fluorinated bis(pyrazoles), Sonogashira, crystal structure, dielectric properties, hydrophobicity, Supramolecular chemistry, Sonogashira coupling, chemistry.chemical_element, General Chemistry, Crystal structure, CHIM/04 - CHIMICA INDUSTRIALE, Catalysis, Crystal, Crystallography, Materials Chemistry, Fluorine, Molecule
Abstract: Three new fluorinated bis(pyrazoles), namely: 1,4-bis(1H-pyrazol-4-ylethynyl)-2-fluorobenzene (H2BPEFB), 1,4-bis(1H-pyrazol-4-ylethynyl)-2,3-difluorobenzene (H2BPEF2B) and 1,4-bis(1H-pyrazol-4-ylethynyl)-tetrafluorobenzene (H2BPEF4B), have been synthesized taking advantage of Sonogashira coupling reactions, and characterized as per their crystal and molecular structure, spectroscopic and dielectric properties, and hydrophobicity. In the crystal structures, the three molecules, whose deviation from planarity increases on increasing the fluorination degree, interact by means of hydrogen bonds, forming 2D supramolecular layers. Notably, the absorption and fluorescence emission properties are only slightly affected by the fluorination degree in both the solid state and solution. Furthermore, the spectral line-shapes are weakly dependent on the environment when dissolved in a number of solvents of different polarity and hydrogen-bonding affinity. On the other hand, the dielectric constant monotonically increases on increasing the number of fluorine atoms. In silico molecular modeling with time-dependent density functional theory has offered a valuable means to rationalize the above mentioned behaviors and has shed some light on the ligand affinity towards representative gases – H2O and CO2 – and organic solvents – toluene.
Published: 2020

12. Multifunctional Organosulfonate Anions Self-Assembled with Organic Cations by Charge-Assisted Hydrogen Bonds and the Cooperation of Water

Author: Guolong Xing, Angiolina Comotti, Irene Bassanetti, Silvia Bracco, Luciano Marchiò, Piero Sozzani, Teng Ben, Xing, G, Bassanetti, I, Ben, T, Bracco, S, Sozzani, P, Marchiò, L, and Comotti, A
Subjects: 010405 organic chemistry, Hydrogen bond, Adamantane, Supramolecular chemistry, Supramolecular Structure, Self-assembly, General Chemistry, CHIM/04 - CHIMICA INDUSTRIALE, 010402 general chemistry, Condensed Matter Physics, 01 natural sciences, Acceptor, 0104 chemical sciences, Self assembled, CHIM/02 - CHIMICA FISICA, chemistry.chemical_compound, Crystallography, chemistry, Molecule, General Materials Science, Linker, Charge-Assisted Hydrogen Bond
Abstract: The present study focuses on the assembly of organo-cations with organo-anions in water. The anions, characterized by symmetric moieties (carbon-, adamantane-, or calixarene-based) functionalized with directional hydrogen bond (HB) acceptor functions (tetra-sulfonate moieties), are combined with planar guanidinium or terephtalimidamide cations as hydrogen bond donors, the purpose being to integrate water molecules into the lattice. The imbalance between the charge on the two components, and the considerable number of HB donor and acceptor sites, promotes the insertion of water into the structures. In the reported structures, a part of the water molecules serves as a structural linker between the anions and cations, while the remaining molecules cluster into channels and cavities in a loose association with the supramolecular matrix framework.
Published: 2018

13. Flexible porous molecular materials responsive to CO2, CH4 and Xe stimuli

Author: Angiolina Comotti, Stefano Canossa, Charl X. Bezuidenhout, M Negroni, Luciano Marchiò, Paolo Pio Mazzeo, Piero Sozzani, Irene Bassanetti, Silvia Bracco, Bassanetti, I, Bracco, S, Comotti, A, Negroni, M, Bezuidenhout, C, Canossa, S, Mazzeo, P, Marchió, L, and Sozzani, P
Subjects: Materials science, solid state NMR of CO2, Xe NMR, chemistry.chemical_element, 02 engineering and technology, CHIM/04 - CHIMICA INDUSTRIALE, 010402 general chemistry, 01 natural sciences, Crystal, Molecular dynamics, Xenon, molecular crystal, Molecule, General Materials Science, Anisotropy, hydrogen bond, Renewable Energy, Sustainability and the Environment, Hydrogen bond, General Chemistry, 021001 nanoscience & nanotechnology, 0104 chemical sciences, CHIM/02 - CHIMICA FISICA, chemistry, Chemical physics, flexible porous material, Density functional theory, Absorption (chemistry), 0210 nano-technology
Abstract: In the search for flexible molecular crystals endowed with porosity, we achieved the fabrication of expandable crystalline prototypal structures, which allow the absorption of gases, without modifying the crystal architecture. The design brings together highly symmetrical tetrahedral elements to construct swellable porous adamantoid frameworks through co-operation of eight surrounding hydrogen bonds mounted on conformationally flexible groups. The flexibility of the porous crystals manifests itself in response to stimuli of selected gases, which promote reversible conformational changes, inducing breathing in the molecular structure. The backbone of the reticular construction is based on the formation of the carboxylic dimers, which project outwards from the tetrahedral molecular core to consolidate the 3D framework. Contact with proper gases such as CO2, Xe and hexane triggers a 56-70% enlargement of the channel cross-section. The accommodation of CO2 and Xe in the channel chambers was revealed by synchrotron-light X-ray diffraction, combined with molecular dynamics and density functional theory (DFT) theoretical calculations. Rare experimental observations of xenon dynamics, in which Xe diffuses along the channels and experiences different chamber orientations in the crystal, were gathered by analysing 129Xe NMR chemical shift anisotropy profiles, which encode the shape and orientation of each visited cavity along the channel. The jump rate and activation energy experienced was uniquely established by exploring Xe atoms in their diffusional path. Nitrogen showed a low affinity to the matrix and was unable to enlarge the pores, thus it was excluded from the restrictive pores of the empty crystal. Given the properties of molecular crystals, it is possible to outline some advantageous aspects, such as simple design, easy self-assembly, solubility, reversible gas uptake and absence of metal ions, and they can thus be considered for eco-friendly gas capture and separation.
Published: 2018

14. Atomistic Model of Realistic Crystalline Mesoporous Organosilica Materials Including Nanochannels

Author: Angiolina Comotti, Antonio De Nicola, Giuseppe Milano, Piero Sozzani, Andrea Correa, De Nicola, Antonio, Correa, Andrea, Comotti, Angiolina, Sozzani, Piero, Milano, Giuseppe, De Nicola, A, Correa, A, Comotti, A, Sozzani, P, and Milano, G
Subjects: Materials science, Silicon, mesoporous organosilica materials (PMOs), crystalline crtucure, OPLS-AA force-field, DFT calculations, CO2 and H2O interaction, Hexagonal crystal system, Research areas, chemistry.chemical_element, Nanotechnology, 02 engineering and technology, 010402 general chemistry, 021001 nanoscience & nanotechnology, CHIM/04 - CHIMICA INDUSTRIALE, 01 natural sciences, Force field (chemistry), 0104 chemical sciences, Surfaces, Coatings and Films, Electronic, Optical and Magnetic Materials, PMOS logic, Mesoporous organosilica, CHIM/02 - CHIMICA FISICA, General Energy, chemistry, Physical and Theoretical Chemistry, 0210 nano-technology, Mesoporous material, Nanoscopic scale
Abstract: The new class of periodic mesoporous organosilica materials (PMOs), due to the peculiar features, has attracted growing interest from several research areas. We present an atomistic model of a p-phenylenesilica crystalline mesoporous structure with a hexagonal framework, explicitly including channels on nanoscale. OPLS-AA force-field optimization, to get a suitable PMO structure compared with the experimental one, is described. In particular, DFT calculations have been performed to calculate torsional energy barrier of phenyl rings connected to the silicon atoms belonging to inorganic layers and to improve the OPLS-AA force field performances for these materials. Finally, inclusion of small molecules and their interactions with PMO walls have been investigated for CO2 and H2O.
Published: 2018

15. Tight Xenon Confinement in a Crystalline Sandwich-like Hydrogen-Bonded Dimeric Capsule of a Cyclic Peptide

Author: Giancarlo Terraneo, Juan R. Granja, Nicola Demitri, Angiolina Comotti, Manuel Amorín, Silvia Bracco, Charl X. Bezuidenhout, Piero Sozzani, Pierangelo Metrangolo, Andrea Pizzi, Rebeca García-Fandiño, Martín Calvelo, Haxel Lionel Ozores, Pizzi, A, Ozores, H, Calvelo, M, Garcia-Fandino, R, Amorin, M, Demitri, N, Terraneo, G, Bracco, S, Comotti, A, Sozzani, P, Bezuidenhout, C, Metrangolo, P, and Granja, J
Subjects: Materials science, Dimer, Shell (structure), Supramolecular chemistry, chemistry.chemical_element, gas confinement, CHIM/04 - CHIMICA INDUSTRIALE, 010402 general chemistry, 01 natural sciences, Catalysis, cyclic peptide, chemistry.chemical_compound, Xenon, Atom, host––guest systems, chemistry.chemical_classification, 010405 organic chemistry, host––guest system, cyclic peptides, General Medicine, General Chemistry, Nuclear magnetic resonance spectroscopy, self-assembly, Cyclic peptide, 0104 chemical sciences, xenon, CHIM/02 - CHIMICA FISICA, Crystallography, chemistry, Self-assembly
Abstract: A cyclic hexapeptide with three pyridyl moieties connected to its backbone forms a hydrogen-bonded dimer, which tightly encapsulates a single xenon atom, like a pearl in its shell. The dimer imprints its shape and symmetry to the captured xenon atom, as demonstrated by 129 Xe NMR spectroscopy, single-crystal X-ray diffraction, and computational studies. The dimers self-assemble hierarchically into tubular structures to form a porous supramolecular architecture, whose cavities are filled by small molecules and gases.
Published: 2019

16. A double helix of opposite charges to form channels with unique CO2 selectivity and dynamics

Author: Irene Bassanetti, Angiolina Comotti, Teng Ben, Piero Sozzani, Guolong Xing, Silvia Bracco, M Negroni, Charl X. Bezuidenhout, Xing, G, Bassanetti, I, Bracco, S, Negroni, M, Bezuidenhout, C, Ben, T, Sozzani, P, and Comotti, A
Subjects: Materials science, 010405 organic chemistry, Hydrogen bond, General Chemistry, 010402 general chemistry, Electrostatics, CHIM/04 - CHIMICA INDUSTRIALE, 01 natural sciences, 0104 chemical sciences, Crystal, Dipole, chemistry.chemical_compound, CHIM/02 - CHIMICA FISICA, chemistry, Chemical physics, Helix, Molecule, Thermal stability, Bifunctional, molecular crystals, pororsity, CO2 dynamics, host-guest interactions, solid state NMR
Abstract: Porous molecular materials represent a new front in the endeavor to achieve high-performance sorptive properties and gas transport. Self-assembly of polyfunctional molecules containing multiple charges, namely, tetrahedral tetra-sulfonate anions and bifunctional linear cations, resulted in a permanently porous crystalline material exhibiting tailored sub-nanometer channels with double helices of electrostatic charges that governed the association and transport of CO2 molecules. The charged channels were consolidated by robust hydrogen bonds. Guest recognition by electrostatic interactions remind us of the role played by the dipolar helical channels in regulatory biological membranes. The systematic electrostatic sites provided the perfectly fitting loci of complementary charges in the channels that proved to be extremely selective with respect to N2 (S = 690), a benchmark in the field of porous molecular materials. The unique screwing dynamics of CO2 travelling along the ultramicropores with a step-wise reorientation mechanism was driven by specific host–guest interactions encountered along the helical track. The unusual dynamics with a single-file transport rate of more than 106 steps per second and an energy barrier for the jump to the next site as low as 2.9 kcal mol−1 was revealed unconventionally by complementing in situ13C NMR anisotropic line-shape analysis with DFT modelling of CO2 diffusing in the crystal channels. The peculiar sorption performances and the extraordinary thermal stability up to 450 °C, combined with the ease of preparation and regeneration, highlight the perspective of applying these materials for selective removal of CO2 from other gases.
Published: 2019

17. A double helix of opposite charges to form channels with unique CO2 selectivity and dynamics† †Electronic supplementary information (ESI) available. CCDC 1865475 and 1865476. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c8sc04376k

Author: Xing, Guolong, Bassanetti, Irene, Bracco, Silvia, Negroni, Mattia, Bezuidenhout, Charl, Ben, Teng, Sozzani, Piero, and Comotti, Angiolina
Subjects: Chemistry
Abstract: Electrostatic charges patterning along crystalline channels recognize CO2 with high selectivity and promote its fast screwing dynamics through the crystal at one million steps per second, strongly reminiscent of trans-membrane transport in biological channels., Porous molecular materials represent a new front in the endeavor to achieve high-performance sorptive properties and gas transport. Self-assembly of polyfunctional molecules containing multiple charges, namely, tetrahedral tetra-sulfonate anions and bifunctional linear cations, resulted in a permanently porous crystalline material exhibiting tailored sub-nanometer channels with double helices of electrostatic charges that governed the association and transport of CO2 molecules. The charged channels were consolidated by robust hydrogen bonds. Guest recognition by electrostatic interactions remind us of the role played by the dipolar helical channels in regulatory biological membranes. The systematic electrostatic sites provided the perfectly fitting loci of complementary charges in the channels that proved to be extremely selective with respect to N2 (S = 690), a benchmark in the field of porous molecular materials. The unique screwing dynamics of CO2 travelling along the ultramicropores with a step-wise reorientation mechanism was driven by specific host–guest interactions encountered along the helical track. The unusual dynamics with a single-file transport rate of more than 106 steps per second and an energy barrier for the jump to the next site as low as 2.9 kcal mol–1 was revealed unconventionally by complementing in situ13C NMR anisotropic line-shape analysis with DFT modelling of CO2 diffusing in the crystal channels. The peculiar sorption performances and the extraordinary thermal stability up to 450 °C, combined with the ease of preparation and regeneration, highlight the perspective of applying these materials for selective removal of CO2 from other gases.
Published: 2018

18. Support effect in high activity gold catalysts for CO oxidation

Author: Comotti, Massimiliano, Schuth, Ferdi, and Spliethoff, Bernd
Subjects: Oxidation-reduction reaction -- Analysis, Gold compounds -- Chemical properties, Carbon monoxide -- Chemical properties, Chemistry
Abstract: The study concerning the evaluation of the metal-support interaction in high activity gold catalysts for CO oxidation is presented. Using the preparation route, the catalysts show high-temperature stability, size dependent activity, and a very good long-term stability.
Published: 2006

19. Stoichiometric compounds of magnesium dichloride with ethanol for the supported Ziegler-Natta catalysis: first recognition and multidimensional MAS NMR study

Author: Sozzani, Piero, Bracco, Silvia, Comotti, Angiolina, Simonutti, Roberto, and Camurati, Isabella
Subjects: Spectrum analysis -- Usage, Magnesium compounds -- Research, Magnesium compounds -- Chemical properties, Alcohol -- Research, Alcohol -- Chemical properties, Alcohol, Denatured -- Research, Alcohol, Denatured -- Chemical properties, Chemistry
Abstract: A deeper understanding and a greater control of the structure of MgCl2/EtOH crystalline adducts that takes part in the catalytic system of Ziegler-Natta polymerization is presented by applying suitable NMR techniques. Study indicates that the MgCl2/EtOH ratios of 2.8 and 1.5 represent stoichiometric values of defined and stable MgCl2.nEtOH complexes.
Published: 2003

20. Mechanical stability of the CMS strip tracker measured with a laser alignment system

Author: Sirunyan, A. M., Tumasyan, A., Adam, W., Asilar, E., Bergauer, T., Brandstetter, J., Brondolin, E., Dragicevic, M., Eroe, J., Flechl, M., Friedl, M., Fruehwirth, R., Ghete, V. M., Hoch, M., Hartl, C., Hoermann, N., Hrubec, J., Jeitler, M., Koenig, A., Kraetschmer, I., Liko, D., Matsushita, T., Mikulec, I., Rabady, D., Rad, N., Rahbaran, B., Rohringer, H., Schieck, J., Strauss, J., Waltenberger, W., Wulz, C. -. E., Dvornikov, O., Makarenko, V., Mossolov, V., Gonzalez, J. Suarez, Zykunov, V., Shumeiko, N., Alderweireldt, S., De Wolf, E. A., Janssen, X., Lauwers, J., De Klundert, M. Van, Van Haevermaet, H., Van Mechelen, P., Van Remortel, N., Van Spilbeeck, A., Abu Zeid, S., Blekman, F., D'Hondt, J., Daci, N., De Bruyn, I., Deroover, K., Lowette, S., Moortgat, S., Moreels, L., Olbrechts, A., Python, Q., Skovpen, K., Tavernier, S., Van Doninck, W., Van Mulders, P., Van Parijs, I., Brun, H., Clerbaux, B., De Lentdecker, G., Delannoy, H., Fasanella, G., Favart, L., Goldouzian, R., Grebenyuk, A., Karapostoli, G., Lenzi, T., Leonard, A., Luetic, J., Maerschalk, T., Marinov, A., Randle-conde, A., Seva, T., Velde, C. Vander, Vanlaer, P., Vannerom, D., Yonamine, R., Zenoni, F., Zhang, F., Cimmino, A., Cornelis, T., Dobur, D., Fagot, A., Gul, M., Khvastunov, I., Poyraz, D., Salva, S., Schofbeck, R., Tytgat, M., Van Driessche, W., Yazgan, E., Zaganidis, N., Bakhshiansohi, H., Beluffi, C., Bondu, O., Brochet, S., Bruno, G., Caudron, A., De Visscher, S., Delaere, C., Delcourt, M., Francois, B., Giammanco, A., Jafari, A., Komm, M., Krintiras, G., Lemaitre, V., Magitteri, A., Mertens, A., Musich, M., Piotrzkowski, K., Quertenmont, L., Selvaggi, M., Marono, M. Vidal, Wertz, S., Beliy, N., Alda Junior, W. L., Alves, F. L., Alves, G. A., Brito, L., Hensel, C., Moraes, A., Pol, M. E., Rebello Teles, P., Belchior Batista Das Chagas, E., Carvalho, W., Chinellato, J., Custodio, A., Da Costa, E. M., Da Silveira, G. G., De Jesus Damiao, D., De Oliveira Martins, C., Fonseca De Souza, S., Huertas Guativa, L. M., Malbouisson, H., Matos Figueiredo, D., Mora Herrera, C., Mundim, L., Nogima, H., Prado Da Silva, W. 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H., Taylor, D., Woods, N., Department of Physics, Helsinki Institute of Physics, Institut de Recherches sur les lois Fondamentales de l'Univers (IRFU), Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Université Paris-Saclay, Laboratoire Leprince-Ringuet (LLR), Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-École polytechnique (X)-Centre National de la Recherche Scientifique (CNRS), Département Recherches Subatomiques (DRS-IPHC), Institut Pluridisciplinaire Hubert Curien (IPHC), Université de Strasbourg (UNISTRA)-Université de Haute-Alsace (UHA) Mulhouse - Colmar (Université de Haute-Alsace (UHA))-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS)-Université de Strasbourg (UNISTRA)-Université de Haute-Alsace (UHA) Mulhouse - Colmar (Université de Haute-Alsace (UHA))-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), Centre de Calcul de l'IN2P3 (CC-IN2P3), Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), Institut de Physique Nucléaire de Lyon (IPNL), Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), CMS, UCL - 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Mathematics, Belforte, S., Candelise, V., Casarsa, M., Cossutti, F., DELLA RICCA, G., Zanetti, A., ET AL (the CMS, Collaboration), Skovpen, Y., Sirunyan, A. M., Tumasyan, A., Adam, W., Asilar, E., Bergauer, T., Brandstetter, J., Brondolin, E., Dragicevic, M., Erö, J., Flechl, M., Friedl, M., Frühwirth, R., Ghete, V. M., Hoch, M., Hartl, C., Hörmann, N., Hrubec, J., Jeitler, M., König, A., Krätschmer, I., Liko, D., Matsushita, T., Mikulec, I., Rabady, D., Rad, N., Rahbaran, B., Rohringer, H., Schieck, J., Strauss, J., Waltenberger, W., Wulz, C. E., Dvornikov, O., Makarenko, V., Mossolov, V., Gonzalez, J. S., Zykunov, V., Shumeiko, N., Alderweireldt, S., De Wolf, E. A., Janssen, X., Lauwers, J., Van De Klundert, M., Van Haevermaet, H., Van Mechelen, P., Van Remortel, N., Van Spilbeeck, A., Zeid, S. A., Blekman, F., D'Hondt, J., Daci, N., De Bruyn, I., Deroover, K., Lowette, S., Moortgat, S., Moreels, L., Olbrechts, A., Python, Q., Skovpen, K., Tavernier, S., Van Doninck, W., Van Mulders, P., Van Parijs, I., Brun, H., Clerbaux, B., De Lentdecker, G., Delannoy, H., Fasanella, G., Favart, L., Goldouzian, R., Grebenyuk, A., Karapostoli, G., Lenzi, T., Léonard, A., Luetic, J., Maerschalk, T., Marinov, A., Randle Conde, A., Seva, T., Velde, C. V., Vanlaer, P., Vannerom, D., Yonamine, R., Zenoni, F., Zhang, F., Cimmino, A., Cornelis, T., Dobur, D., Fagot, A., Gul, M., Khvastunov, I., Poyraz, D., Salva, S., Schöfbeck, R., Tytgat, M., Van Driessche, W., Yazgan, E., Zaganidis, N., Bakhshiansohi, H., Beluffi, C., Bondu, O., Brochet, S., Bruno, G., Caudron, A., De Visscher, S., Delaere, C., Delcourt, M., Francois, B., Giammanco, A., Jafari, A., Komm, M., Krintiras, G., Lemaitre, V., Magitteri, A., Mertens, A., Musich, M., Piotrzkowski, K., Quertenmont, L., Selvaggi, M., Marono, M. 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A., Radi, A., Kadastik, M., Perrini, L., Raidal, M., Tiko, A., Veelken, C., Eerola, P., Pekkanen, J., Voutilainen, M., Härkönen, J., Järvinen, T., Karimäki, V., Kinnunen, R., Lampén, T., Lassila Perini, K., Lehti, S., Lindén, T., Luukka, P., Tuominiemi, J., Tuovinen, E., Wendland, L., Talvitie, J., Tuuva, T., Besancon, M., Couderc, F., Dejardin, M., Denegri, D., Fabbro, B., Faure, J. L., Favaro, C., Ferri, F., Ganjour, S., Ghosh, S., Givernaud, A., Gras, P., De Monchenault, G. H., Jarry, P., Kucher, I., Locci, E., Machet, M., Malcles, J., Rander, J., Rosowsky, A., Titov, M., Abdulsalam, A., Antropov, I., Baffioni, S., Beaudette, F., Busson, P., Cadamuro, L., Chapon, E., Charlot, C., Davignon, O., De Cassagnac, R. G., Jo, M., Lisniak, S., Miné, P., Nguyen, M., Ochando, C., Ortona, G., Paganini, P., Pigard, P., Regnard, S., Salerno, R., Sirois, Y., Strebler, T., Yilmaz, Y., Zabi, A., Zghiche, A., Agram, J. L., Andrea, J., Aubin, A., Bloch, D., Brom, J. M., Buttignol, M., Chabert, E. C., Chanon, N., Collard, C., Conte, E., Coubez, X., Fontaine, J. C., Gelé, D., Goerlach, U., Hosselet, J., Le Bihan, A. C., Tromson, D., Van Hove, P., Gadrat, S., Beauceron, S., Bernet, C., Boudoul, G., Montoya, C. A. C., Chierici, R., Combaret, C., Contardo, D., Courbon, B., Depasse, P., El Mamouni, H., Fay, J., Galbit, G., Gascon, S., Gouzevitch, M., Grenier, G., Ille, B., Lagarde, F., Laktineh, I. B., Lethuillier, M., Mirabito, L., Pequegnot, A. L., Perries, S., Popov, A., Sabes, D., Sordini, V., Donckt, M. V., Verdier, P., Viret, S., Zoccarato, Y., Toriashvili, T., Lomidze, D., Adolphi, R., Autermann, C., Beranek, S., Feld, L., Kiesel, M. K., Klein, K., Lipinski, M., Ostapchuk, A., Preuten, M., Rauch, M., Raupach, F., Schael, S., Schomakers, C., Schulz, J., Von Dratzig, A. 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M., Stöver, M., Tholen, H., Troendle, D., Usai, E., Vanelderen, L., Vanhoefer, A., Vormwald, B., Wellhausen, J., Abbas, M., Akbiyik, M., Amstutz, C., Barth, C., Baur, S., Baus, C., Berger, J., Butz, E., Casele, M., Caspart, R., Chwalek, T., Colombo, F., De Boer, W., Dierlamm, A., Fink, S., Freund, B., Friese, R., Giffels, M., Gilbert, A., Goldenzweig, P., Haitz, D., Hartmann, F., Heindl, S. M., Husemann, U., Katkov, I., Kornmeyer, A., Kudella, S., Mildner, H., Mozer, M. U., Müller, T. h., Plagge, M., Quast, G., Rabbertz, K., Röcker, S., Roscher, F., Schröder, M., Shvetsov, I., Sieber, G., Simonis, H. J., Ulrich, R., Wayand, S., Weber, M., Weiler, T., Williamson, S., Wöhrmann, C., Wolf, R., Anagnostou, G., Daskalakis, G., Geralis, T., Giakoumopoulou, V. A., Kyriakis, A., Loukas, D., Topsis Giotis, I., Kesisoglou, S., Panagiotou, A., Saoulidou, N., Tziaferi, E., Evangelou, I., Flouris, G., Foudas, C., Kokkas, P., Loukas, N., Manthos, N., Papadopoulos, I., Paradas, E., Filipovic, N., Pasztor, G., Bencze, G., Hajdu, C., Horvath, D., Sikler, F., Veszpremi, V., Vesztergombi, G., Zsigmond, A. J., Beni, N., Czellar, S., Karancsi, J., Makovec, A., Molnar, J., Szillasi, Z., Bartók, M., Raics, P., Trocsanyi, Z. L., Ujvari, B., Komaragiri, J. R., Bahinipati, S., Bhowmik, S., Choudhury, S., Mal, P., Mandal, K., Nayak, A., Sahoo, D. K., Sahoo, N., Swain, S. K., Bansal, S., Beri, S. B., Bhatnagar, V., Chawla, R., Bhawandeep, U., Kalsi, A. K., Kaur, A., Kaur, M., Kumar, R., Kumari, P., Mehta, A., Mittal, M., Singh, J. B., Walia, G., Kumar, A., Bhardwaj, A., Choudhary, B. C., Garg, R. B., Keshri, S., Malhotra, S., Naimuddin, M., Ranjan, K., Sharma, R., Sharma, V., Bhattacharya, R., Bhattacharya, S., Chatterjee, K., Dey, S., Dutt, S., Dutta, S., Majumdar, N., Modak, A., Mondal, K., Mukhopadhyay, S., Nandan, S., Purohit, A., Roy, A., Roy, D., Chowdhury, S. R., Sarkar, S., Sharan, M., Thakur, S., Behera, P. K., Chudasama, R., Dutta, D., Jha, V., Kumar, V., Mohanty, A. K., Netrakanti, P. K., Pant, L. M., Shukla, P., Topkar, A., Aziz, T., Dugad, S., Kole, G., Mahakud, B., Mitra, S., Mohanty, G. B., Parida, B., Sur, N., Sutar, B., Banerjee, S., Dewanjee, R. K., Ganguly, S., Guchait, M., Jain, S. a., Kumar, S., Maity, M., Majumder, G., Mazumdar, K., Sarkar, T., Wickramage, N., Chauhan, S., Dube, S., Hegde, V., Kapoor, A., Kothekar, K., Pandey, S., Rane, A., Sharma, S., Bakhshiansohl, H., Chenarani, S., Tadavani, E. E., Etesami, S. M., Khakzad, M., Najafabadi, M. M., Naseri, M., Mehdiabadi, S. P., Hosseinabadi, F. R., Safarzadeh, B., Zeinali, M., Felcini, M., Grunewald, M., Abbrescia, M., Calabria, C., Caputo, C., Cariola, P., Colaleo, A., Creanza, D., Cristella, L., De Filippis, N., De Palma, M., Fiore, L., Iaselli, G., Maggi, G., Maggi, M., Miniello, G., My, S., Nuzzo, S., Pompili, A., Pugliese, G., Radogna, R., Ranieri, A., Selvaggi, G., Sharma, A., Silvestris, L., Venditti, R., Verwilligen, P., Abbiendi, G., Battilana, C., Bonacorsi, D., Braibant Giacomelli, S., Brigliadori, L., Campanini, R., Capiluppi, P., Castro, A., Cavallo, F. R., Chhibra, S. S., Codispoti, G., Cuffiani, M., Dallavalle, G. M., Fabbri, F., Fanfani, A., Fasanella, D., Giacomelli, P., Grandi, C., Guiducci, L., Marcellini, S., Masetti, G., Montanari, A., Navarria, F. L., Perrotta, A., Rossi, A. M., Rovelli, T., Siroli, G. 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Gomez, Innocenti, G.M., Lai, Y.S., Lee, Y.-J., Luckey, P.D., Marini, A.C., McGinn, C., Salfeld-Nebgen, J., Stephans, G.S.F., Wang, T.W., Benvenuti, A.C., Chatterjee, R.M., Kao, S.C., Acosta, J.G., Claes, D.R., Suarez, R. Gonzalez, Rodrigues, A. Malta, Siado, J.E., Snow, G.R., Morse, D.M., De Lima, R. Teixeira, Wang, R.-J., Hahn, K.A., Schmitt, M.H., Anampa, K. Hurtado, Karmgard, D.J., Durkin, L.S., Winer, B.L., Wulsin, H.W., Barnes, V.E., Jha, M.K., Jung, A.W., Miller, D.H., Schulte, J.F., Ecklund, K.M., Geurts, F.J.M., Padley, B.P., Duh, Y.T., Garcia-Bellido, A., Lo, K.H., Chou, J.P., Espinosa, T.A. Gómez, Elayavalli, R. Kunnawalkam, Delannoy, A.G., Ulmer, K.A., Dudero, P.R., Arenton, M.W., Karchin, P.E., Belknap, D.A., Pierro, G.A., Smith, W.H., Elementary Particle Physics, Physics, Faculty of Sciences and Bioengineering Sciences, Vriendenkring VUB, Centre National de la Recherche Scientifique (CNRS)-École polytechnique (X)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3), Université de Strasbourg (UNISTRA)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS)-Université de Strasbourg (UNISTRA)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), Centre National de la Recherche Scientifique (CNRS)-Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3), Çukurova Üniversitesi, Fen-Edebiyat 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Elvira, V, Fisk, I, Freeman, J, Gingu, C, Gottschalk, E, Gray, L, Green, D, Grünendahl, S, Gutsche, O, Hare, D, Harris, R, Hasegawa, S, Hirschauer, J, Hoff, J, Hrycyk, M, Hu, Z, Jayatilaka, B, Jindariani, S, Johnson, M, Joshi, U, Kahlid, F, Klima, B, Kreis, B, Lammel, S, Linacre, J, Lincoln, D, Lipton, R, Liu, M, Liu, T, De Sá, R, Lykken, J, Maeshima, K, Magini, N, Marraffino, J, Maruyama, S, Mason, D, Matulik, M, Mcbride, P, Merkel, P, Mrenna, S, Nahn, S, O'Dell, V, Pedro, K, Prokofyev, O, Rakness, G, Ristori, L, Sexton-Kennedy, E, Shenai, A, Soha, A, Spalding, W, Spiegel, L, Stoynev, S, Strait, J, Strobbe, N, Taylor, L, Tkaczyk, S, Tran, N, Uplegger, L, Vaandering, E, Vernieri, C, Verzocchi, M, Vidal, R, Wang, M, Weber, H, Whitbeck, A, Wu, Y, Zimmerman, T, Acosta, D, Avery, P, Bortignon, P, Bourilkov, D, Brinkerhoff, A, Carnes, A, Carver, M, Curry, D, Das, S, Field, R, Furic, I, Konigsberg, J, Korytov, A, Low, J, Ma, P, Matchev, K, Mei, H, Mitselmakher, G, Rank, D, Shchutska, L, Sperka, D, Thomas, L, Wang, J, Wang, S, Yelton, J, Linn, S, Markowitz, P, Martinez, G, Rodriguez, J, Ackert, A, Adams, T, Askew, A, Bein, S, Hagopian, S, Hagopian, V, Johnson, K, Prosper, H, Santra, A, Yohay, R, Baarmand, M, Bhopatkar, V, Colafranceschi, S, Hohlmann, M, Noonan, D, Roy, T, Yumiceva, F, Adams, M, Apanasevich, L, Berry, D, Betts, R, Bucinskaite, I, Cavanaugh, R, Ennesser, L, Evdokimov, A, Evdokimov, O, Gauthier, L, Gerber, C, Hofman, D, Jung, K, Makauda, S, Gonzalez, I, Varelas, N, Wang, H, Wu, Z, Zakaria, M, Zhang, J, Bilki, B, Clarida, W, Dilsiz, K, Durgut, S, Gandrajula, R, Haytmyradov, M, Khristenko, V, Merlo, J, Mermerkaya, H, Mestvirishvili, A, Moeller, A, Nachtman, J, Ogul, H, Onel, Y, Ozok, F, Penzo, A, Snyder, C, Tiras, E, Wetzel, J, Yi, K, Anderson, I, Blumenfeld, B, Cocoros, A, Eminizer, N, Fehling, D, Feng, L, Gritsan, A, Maksimovic, P, Roskes, J, Sarica, U, Swartz, M, Xiao, M, Xin, Y, You, C, Al-Bataineh, A, Baringer, P, Bean, A, Boren, S, Bowen, J, Castle, J, Forthomme, L, Iii, R, Khalil, S, Kropivnitskaya, A, Majumder, D, Mcbrayer, W, Murray, M, Sanders, S, Stringer, R, Takaki, J, Wang, Q, Wilson, G, Ivanov, A, Kaadze, K, Maravin, Y, Mohammadi, A, Saini, L, Skhirtladze, N, Toda, S, Rebassoo, F, Wright, D, Anelli, C, Baden, A, Baron, O, Belloni, A, Calvert, B, Eno, S, Ferraioli, C, Hadley, N, Jabeen, S, Jeng, G, Kellogg, R, Kolberg, T, Kunkle, J, Mignerey, A, Ricci-Tam, F, Shin, Y, Skuja, A, Tonjes, M, Tonwar, S, Abercrombie, D, Allen, B, Apyan, A, Azzolini, V, Barbieri, R, Baty, A, Bi, R, Bierwagen, K, Brandt, S, Busza, W, Cali, I, D'Alfonso, M, Demiragli, Z, Di Matteo, L, Ceballos, G, Goncharov, M, Hsu, D, Iiyama, Y, Innocenti, G, Klute, M, Kovalskyi, D, Krajczar, K, Lai, Y, Lee, Y, Levin, A, Luckey, P, Maier, B, Marini, A, Mcginn, C, Mironov, C, Narayanan, S, Niu, X, Paus, C, Roland, C, Roland, G, Salfeld-Nebgen, J, Stephans, G, Tatar, K, Varma, M, Velicanu, D, Veverka, J, Wang, T, Wyslouch, B, Yang, M, Benvenuti, A, Chatterjee, R, Evans, A, Hansen, P, Kalafut, S, Kao, S, Kubota, Y, Lesko, Z, Mans, J, Nourbakhsh, S, Ruckstuhl, N, Rusack, R, Tambe, N, Turkewitz, J, Acosta, J, Oliveros, S, Avdeeva, E, Bloom, K, Claes, D, Fangmeier, C, Suarez, R, Kamalieddin, R, Kravchenko, I, Rodrigues, A, Monroy, J, Siado, J, Snow, G, Stieger, B, Alyari, M, Dolen, J, Godshalk, A, Harrington, C, Iashvili, I, Kaisen, J, Nguyen, D, Parker, A, Rappoccio, S, Roozbahani, B, Alverson, G, Barberis, E, Hortiangtham, A, Massironi, A, Morse, D, Nash, D, Orimoto, T, De Lima, R, Trocino, D, Wang, R, Wood, D, Charaf, O, Hahn, K, Mucia, N, Odell, N, Pollack, B, Schmitt, M, Sung, K, Trovato, M, Velasco, M, Dev, N, Hildreth, M, Anampa, K, Jessop, C, Karmgard, D, Kellams, N, Lannon, K, Marinelli, N, Meng, F, Mueller, C, Musienko, Y, Planer, M, Reinsvold, A, Ruchti, R, Rupprecht, N, Smith, G, Taroni, S, Wayne, M, Wolf, M, Woodard, A, Alimena, J, Antonelli, L, Bylsma, B, Durkin, L, Flowers, S, Francis, B, Hart, A, Hill, C, Hughes, R, Ji, W, Liu, B, Luo, W, Puigh, D, Winer, B, Wulsin, H, Cooperstein, S, Driga, O, Elmer, P, Hardenbrook, J, Hebda, P, Lange, D, Luo, J, Marlow, D, Medvedeva, T, Mei, K, Ojalvo, I, Olsen, J, Palmer, C, Piroué, P, Stickland, D, Svyatkovskiy, A, Tully, C, Barker, A, Barnes, V, Folgueras, S, Gutay, L, Hinton, N, Jha, M, Jones, M, Jung, A, Khatiwada, A, Miller, D, Neumeister, N, Schulte, J, Shi, X, Sun, J, Wang, F, Xie, W, Parashar, N, Stupak, J, Adair, A, Akgun, B, Chen, Z, Ecklund, K, Geurts, F, Guilbaud, M, Kilpatrick, M, Li, W, Michlin, B, Northup, M, Nussbaum, T, Padley, B, Roberts, J, Rorie, J, Tu, Z, Zabel, J, Betchart, B, Bodek, A, De Barbaro, P, Demina, R, Duh, Y, Ferbel, T, Galanti, M, Garcia-Bellido, A, Han, J, Hindrichs, O, Khukhunaishvili, A, Lo, K, Tan, P, Verzetti, M, Agapitos, A, Chou, J, Gershtein, Y, Espinosa, T, Halkiadakis, E, Heindl, M, Hughes, E, Kaplan, S, Elayavalli, R, Kyriacou, S, Lath, A, Nash, K, Osherson, M, Park, M, Saka, H, Salur, S, Schnetzer, S, Sheffield, D, Somalwar, S, Stone, R, Thomas, S, Thomassen, P, Walker, M, Delannoy, A, Foerster, M, Heideman, J, Riley, G, Rose, K, Spanier, S, Thapa, K, Bouhali, O, Celik, A, Dalchenko, M, De Mattia, M, Delgado, A, Dildick, S, Eusebi, R, Gilmore, J, Huang, T, Juska, E, Kamon, T, Mueller, R, Pakhotin, Y, Patel, R, Perloff, A, Perniè, L, Rathjens, D, Safonov, A, Tatarinov, A, Ulmer, K, Akchurin, N, Cowden, C, Damgov, J, De Guio, F, Dragoiu, C, Dudero, P, Faulkner, J, Gurpinar, E, Kunori, S, Lamichhane, K, Libeiro, T, Peltola, T, Undleeb, S, Volobouev, I, Greene, S, Gurrola, A, Janjam, R, Johns, W, Maguire, C, Melo, A, Ni, H, Sheldon, P, Tuo, S, Velkovska, J, Xu, Q, Arenton, M, Barria, P, Cox, B, Goodell, J, Hirosky, R, Ledovskoy, A, Li, H, Neu, C, Sinthuprasith, T, Sun, X, Wang, Y, Wolfe, E, Xia, F, Clarke, C, Harr, R, Karchin, P, Sturdy, J, Belknap, D, Buchanan, J, Caillol, C, Dasu, S, Dodd, L, Duric, S, Gomber, B, Grothe, M, Herndon, M, Hervé, A, Klabbers, P, Lanaro, A, Levine, A, Long, K, Loveless, R, Perry, T, Pierro, G, Polese, G, Ruggles, T, Savin, A, Smith, N, Smith, W, Taylor, D, Woods, N, Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Université de Strasbourg (UNISTRA)-Centre National de la Recherche Scientifique (CNRS)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Université de Strasbourg (UNISTRA)-Centre National de la Recherche Scientifique (CNRS), Lista, Luca, Iorio, Alberto O M, Fienga, Francesco, And, Others., and CMS Collaboration
Subjects: Technology, Physics - Instrumentation and Detectors, Compact Muon Solenoid, Physics::Instrumentation and Detectors, measurement methods, Detector alignment and calibration methods (lasers, sources, particle-beams), Detector alignment, 7. Clean energy, 01 natural sciences, law.invention, High Energy Physics - Experiment, fibre [carbon], High Energy Physics - Experiment (hep-ex), law, Particle tracking detectors, [PHYS.HEXP]Physics [physics]/High Energy Physics - Experiment [hep-ex], Large detector systems, tracking detector, Large detector systems for particle and astroparticle physics, Particle tracking detectors (Solid-state detectors), Detectors and Experimental Techniques, Image resolution, Instruments & Instrumentation, Instrumentation, physics.ins-det, Mathematical Physics, Physics, Large Hadron Collider, CMS, Detector, Settore FIS/01 - Fisica Sperimentale, Electrical engineering, microstrip [semiconductor detector], alignment, particle-beams), Instrumentation and Detectors (physics.ins-det), Nuclear & Particles Physics, Semiconductor detector, ComputingMethodologies_DOCUMENTANDTEXTPROCESSING, High energy physics, Experimental particle physics, LHC, CMS, Standard Model, semiconductor detector: microstrip, PARTICLE PHYSICS, CMS collaboration, particle tracking detectors, large detector-system performance, physics, Particle Physics - Experiment, sources, Silicon, education, chemistry.chemical_element, FOS: Physical sciences, temperature dependence [stability], 114 Physical sciences, Optics, Detector alignment and calibration methods (lasers, sources, Large detector systems for particle and astroparticle, (Solid-state detectors), DETECTOR, 0103 physical sciences, ddc:530, ddc:610, Detector alignment and calibration methods (lasers, sources, particle-beams), Large detector systems for particle and astroparticle physics, Particle tracking detectors, Particle tracking detectors (Solid-state detectors), Instrumentation, Mathematical Physics, 010306 general physics, spatial resolution, mechanics: stability, stability: temperature dependence, Science & Technology, 010308 nuclear & particles physics, business.industry, LARGE HADRON COLLIDER, hep-ex, stability [mechanics], Atmospheric temperature range, Laser, Particle tracking detector, laser, Detector alignment and calibration methods (lasers, Physics and Astronomy, chemistry, Large detector systems for particle and astroparticle physic, carbon: fibre, business
Abstract: Journal of Instrumentation 12(04), P04023(2017). doi:10.1088/1748-0221/12/04/P04023, The CMS tracker consists of 206 m$^2$ of silicon strip sensors assembled on carbon fibre composite structures and is designed for operation in the temperature range from −25 to +25°C. The mechanical stability of tracker components during physics operation was monitored with a few μm resolution using a dedicated laser alignment system as well as particle tracks from cosmic rays and hadron-hadron collisions. During the LHC operational period of 2011–2013 at stable temperatures, the components of the tracker were observed to experience relative movements of less than 30μm. In addition, temperature variations were found to cause displacements of tracker structures of about 2μm°C, which largely revert to their initial positions when the temperature is restored to its original value., Published by IOP, London
Published: 2017
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21. Solid-State NMR of Supramolecular Materials

Author: Piero Sozzani, Silvia Bracco, Angiolina Comotti, Comotti, A., Bracco, S., Sozzani, P., Editor-in-Chiefs: Jerry Atwood Editors: George W. Gokel Len Barbour, Comotti, A, Bracco, S, and Sozzani, P
Subjects: Deuterium NMR, Chemistry, supramolecular material, technology, industry, and agriculture, Supramolecular chemistry, self-assembly, macromolecular substances, Nuclear magnetic resonance spectroscopy, Nuclear magnetic resonance crystallography, CHIM/04 - CHIMICA INDUSTRIALE, Characterization (materials science), Amorphous solid, CHIM/02 - CHIMICA FISICA, host-guest interaction, Solid-state nuclear magnetic resonance, Computational chemistry, Organic chemistry, Molecule, solid-state NMR spectroscopy
Abstract: Supramolecular chemistry finds in solid-state NMR spectroscopy a privileged characterization method, especially in a variety of multidimensional experiments. Several applications of solid-state NMR to inclusion compounds, host–guest systems, cocrystals, polymeric self-assembly, and porous materials have been realized. Gases and volatile molecules were detected in supramolecular adducts by NMR as well, providing accurate information about their interaction with the solid transport properties and anisotropic behavior. In ordered systems, the results are complementary to XRD and, thus, NMR is regarded as a structural method, but it is also sensitive to amorphous phases, complex molecular aggregates, interfaces, and overall dynamics.
Published: 2017

22. Expandable porous organic frameworks with built-in amino and hydroxyl functions for CO2 and CH4 capture

Author: D Piga, Silvia Bracco, Piero Sozzani, Angiolina Comotti, J Perego, Perego, J, Piga, D, Bracco, S, Sozzani, P, and Comotti, A
Subjects: Materials science, Metals and Alloys, chemistry.chemical_element, 02 engineering and technology, General Chemistry, Porous Organic Frameworks (POFs), CO2 adsorption, CH4 adsorption, interaction energies, 2D MAS NMR, 010402 general chemistry, 021001 nanoscience & nanotechnology, CHIM/04 - CHIMICA INDUSTRIALE, 01 natural sciences, Catalysis, 0104 chemical sciences, Surfaces, Coatings and Films, Electronic, Optical and Magnetic Materials, CHIM/02 - CHIMICA FISICA, chemistry, Chemical engineering, Materials Chemistry, Ceramics and Composites, Amine gas treating, 0210 nano-technology, Porosity, Carbon
Abstract: The synthesis of porous organic 3D frameworks, wherein amine, hydroxyl and Li-alkoxide functions were built directly on the monomer-unit carbon core, realizes improved interactions with target gases. CO2 was retained by the amine group with a remarkable energy of 54 kJ mol-1, while 2D MAS NMR provided rare evidence of amine-to-gas short-distance interactions. Frameworks containing hydroxyl and Li-alkoxide functions show optimal interaction energies with CH4 of up to 25 kJ mol-1. The light network of 3-branch building units ensures the expandability of the nano-sponges.
Published: 2018

23. Changing the Dress to a MOF through Fluorination and Transmetalation. Structural and Gas-Sorption Effects

Author: Davide Balestri, Silvia Bracco, Angiolina Comotti, Irene Bassanetti, Cristina Gazzurelli, Paolo Pelagatti, Alessia Bacchi, Stefano Canossa, Balestri, D, Bassanetti, I, Canossa, S, Gazzurelli, C, Bacchi, A, Bracco, S, Comotti, A, and Pelagatti, P
Subjects: chemistry.chemical_classification, MOFs, permanent porosity, gas adsorption, selectivity, 010405 organic chemistry, Ligand, General Chemistry, Microporous material, 010402 general chemistry, Condensed Matter Physics, CHIM/04 - CHIMICA INDUSTRIALE, 01 natural sciences, 0104 chemical sciences, chemistry.chemical_compound, Transmetalation, CHIM/02 - CHIMICA FISICA, Dicarboxylic acid, Adsorption, chemistry, Selective adsorption, Amide, Polymer chemistry, General Materials Science, Metal-organic framework
Abstract: Two novel pillared Zn(II)-based Metal–Organic Frameworks were de novo synthesized exploiting N,N′-(1,1′-biphenyl)-4,4′-diylbis-4-pyridinecarboxamide (bpba) and its fluorinated analogous N,N′-(perfluoro-1,1′-biphenyl-4,4′-diyl)diisonicotinamide (F-bpba) as suitable pillar linkers and 2,6-naphthalene dicarboxylic acid as carboxylic ligand. The resulting heteroleptic MOFs, namely, PUM210, [Zn4(bpba)1.5·(ndc)4·(H2O)]n and PUM210F, [Zn3(F-bpba)1·(ndc)3·(DMF)]n, feature an uncommon truncation of the Zn(II) paddle-wheel nodes along the pillaring direction. PUM210 and PUM210F exhibit a polycatenated architecture, resulting in microporous channels decorated by amide moieties. The activated forms show a permanent porosity and a selective adsorption of CO2 over N2. Moreover, the partially transmetalated Cu-PUM210 and Cu-PUM210F were obtained by convenient transmetalation protocol and their adsorption propriety toward CO2 were subsequently investigated.
Published: 2018

24. Microporous Molecular Materials from Dipeptides Containing Non‐proteinogenic Residues

Author: Piero Sozzani, Angiolina Comotti, Vitthal N. Yadav, Martin Hennum, Carl Henrik Görbitz, Silvia Bracco, Tore Bonge-Hansen, Yadav, V, Comotti, A, Sozzani, P, Bracco, S, Bonge Hansen, T, Hennum, M, and Görbitz, C
Subjects: Peptide, CHIM/04 - CHIMICA INDUSTRIALE, Crystallography, X-Ray, Crystal engineering, Catalysis, microporous material, Adsorption, Side chain, Molecule, Bioorganic chemistry, bioorganic chemistry, solid state NMR, chemistry.chemical_classification, Hydrogen Bonding, General Medicine, Dipeptides, General Chemistry, Microporous material, Combinatorial chemistry, peptide, X-ray diffraction, CHIM/02 - CHIMICA FISICA, chemistry, crystal engineering, X-ray crystallography, Porosity
Abstract: Dipeptides with two hydrophobic side chains have proved to be an exceptional source of microporous organic materials, but since previous structures were limited to the incorporation of only proteinogenic residues, their full potential as adsorbents has remained unexplored. Single-crystal XRD data for ten new compounds with non-proteinogenic L-2-aminobutanoic acid and/or L-2-amino-pentanoic acid are presented. The gas-phase accessibility of their crystal pores, with cross-sections of 2.3 to 5.1 Å, was monitored by CO2 and CH4 adsorption isotherms. Included CO2 was also detected spectroscopically by 2D MAS NMR. An extensive conformational analysis reveals that the use of linear rather than branched side chains (such as L-valine and L-isoleucine) affords peptides with a greater degree of conformational freedom and yields more-flexible channel surfaces that may easily adapt to a series of potential guest molecules.
Published: 2015

25. Trapping in proton irradiated p + -n-n + silicon sensors at fluences anticipated at the HL-LHC outer tracker

Author: Adam, W, Bergauer, T, Dragicevic, M, Friedl, M, Fruehwirth, R, Hoch, M, Hrubec, J, Krammer, M, Treberspurg, W, Waltenberger, W, Alderweireldt, S, Beaumont, W, Janssen, X, Luyckx, S, Van Mechelen, P, Van Remortel, N, Van Spilbeeck, A, Barria, P, Caillol, C, Clerbaux, B, De Lentdecker, G, Dobur, D, Favart, L, Grebenyuk, A, Lenzi, T, Leonard, A, Maerschalk, T, Mohammadi, A, Pernie, L, Randle-Conde, A, Reis, T, Seva, T, Thomas, L, Velde, CV, Vanlaer, P, Wang, J, Zenoni, F, Abu Zeid, S, Blekman, F, De Bruyn, I, D'Hondt, J, Daci, N, Deroover, K, Heracleous, N, Keaveney, J, Lowette, S, Moreels, L, Olbrechts, A, Python, Q, Tavernier, S, Van Mulders, P, Van Onsem, G, Van Parijs, I, Strom, DA, Basegmez, S, Bruno, G, Castello, R, Caudron, A, Ceard, L, De Callatay, B, Delaere, C, Du Pree, T, Forthomme, L, Giammanco, A, Hollar, J, Jez, P, Michotte, D, Nuttens, C, Perrini, L, Pagano, D, Quertenmont, L, Selvaggi, M, Marono, MV, Beliy, N, Caebergs, T, Daubie, E, Hammad, GH, Harkonen, J, Lampen, T, Luukka, P-R, Maenpaa, T, Peltola, T, Tuominen, E, Tuovinen, E, Eerola, P, Tuuva, T, Beaulieu, G, Boudoul, G, Combaret, C, Contardo, D, Gallbit, G, Lumb, N, Mathez, H, Mirabito, L, Perries, S, Sabes, D, Donckt, MV, Verdier, P, Viret, S, Zoccarato, Y, Agram, J-L, Conte, E, Fontaine, J-C, Andrea, J, Bloch, D, Bonnin, C, Brom, J-M, Chabert, E, Charles, L, Goetzmann, C, Gross, L, Hosselet, J, Mathieu, C, Richer, M, Skovpen, K, Pistone, C, Fluegge, G, Kuensken, A, Geisler, M, Pooth, O, Stahl, A, Autermann, C, Edelhoff, M, Esser, H, Feld, L, Karpinski, W, Klein, K, Lipinski, M, Ostapchuk, A, Pierschel, G, Preuten, M, Raupach, F, Sammet, J, Schael, S, Schwering, G, Wittmer, B, Wlochal, M, Zhukov, V, Bartosik, N, Behr, J, Burgmeier, A, Calligaris, L, Dolinska, G, Eckerlin, G, Eckstein, D, Eichhorn, T, Fluke, G, Garcia, JG, Gizhko, A, Hansen, K, Harb, A, Hauk, J, Kalogeropoulos, A, Kleinwort, C, Korol, I, Lange, W, Lohmann, W, Mankel, R, Maser, H, Mittag, G, Muhl, C, Mussgiller, A, Nayak, A, Ntomari, E, Perrey, H, Pitzl, D, Schroeder, M, Seitz, C, Spannagel, S, Zuber, A, Biskop, H, Blobel, V, Buhmann, P, Centis-Vignali, M, Draeger, A-R, Erfle, J, Garutti, E, Haller, J, Hoffmann, M, Junkes, A, Lapsien, T, Maettig, S, Matysek, M, Perieanu, A, Poehlsen, J, Poehlsen, T, Scharf, C, Schleper, P, Schmidt, A, Sola, V, Steinbrueck, G, Wellhausen, J, Barvich, T, Barth, C, Boegelspacher, F, De Boer, W, Butz, E, Casele, M, Colombo, F, Dierlamm, A, Eber, R, Freund, B, Hartmann, F, Hauth, T, Heindl, S, Hoffmann, K-H, Husemann, U, Kornmeyer, A, Mallows, S, Muller, T, Nuernberg, A, Printz, M, Simonis, HJ, Steck, P, Weber, M, Weiler, T, Bhardwaj, A, Kumar, A, Ranjan, K, Bakhshiansohl, H, Behnamian, H, Khakzad, M, Naseri, M, Cariola, P, De Robertis, G, Fiore, L, Franco, M, Loddo, F, Sala, G, Silvestris, L, Creanza, D, De Palma, M, Maggi, G, My, S, Selvaggi, G, Albergo, S, Cappello, G, Chiorboli, M, Costa, S, Giordano, F, Di Mattia, A, Potenza, R, Saizu, MA, Tricomi, A, Tuve, C, 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Teodorescu, L, Bainbridge, R, Dauncey, P, Fulcher, J, Hall, G, Magnan, A-M, Pesaresi, M, Raymond, DM, Uchida, K, Coughlan, JA, Harder, K, Ilic, J, Tomalin, IR, Garabedian, A, Heintz, U, Narain, M, Nelson, J, Sagir, S, Speer, T, Swanson, J, Tersegno, D, Watson-Daniels, J, Chertok, M, Conway, J, Conway, R, Flores, C, Lander, R, Pellett, D, Ricci-Tam, F, Squires, M, Thomson, J, Yohay, R, Burt, K, Ellison, J, Hanson, G, Malberti, M, Olmedo, M, Cerati, G, Sharma, V, Vartak, A, Yagil, A, Della Porta, GZ, Dutta, V, Gouskos, L, Incandela, J, Kyre, S, McColl, N, Mullin, S, White, D, Cumalat, JP, Ford, WT, Gaz, A, Krohn, M, Stenson, K, Wagner, SR, Baldin, B, Bolla, G, Burkett, K, Butler, J, Cheung, H, Chramowicz, J, Christian, D, Cooper, WE, Deptuch, G, Derylo, G, Gingu, C, Gruenendahl, S, Hasegawa, S, Hoff, J, Howell, J, Hrycyk, M, Jindariani, S, Johnson, M, Jung, A, Joshi, U, Kahlid, F, Lei, CM, Lipton, R, Liu, T, Los, S, Matulik, M, Merkel, P, Nahn, S, Prosser, A, Rivera, R, Shenai, A, Spiegel, L, Tran, N, Uplegger, L, Voirin, E, Yin, H, Adams, MR, Berry, DR, Evdokimov, A, Evdokimov, O, Gerber, CE, Hofman, DJ, Kapustka, BK, O'Brien, C, Gonzalez, DIS, Trauger, H, Turner, P, Parashar, N, Stupak, J, Bortoletto, D, Bubna, M, Hinton, N, Jones, M, Miller, DH, Shi, X, Tan, P, Baringer, P, Bean, A, Benelli, G, Gray, J, Majumder, D, Noonan, D, Sanders, S, Stringer, R, Ivanov, A, Makouski, M, Skhirtladze, N, Taylor, R, Anderson, I, Fehling, D, Gritsan, A, Maksimovic, P, Martin, C, Nash, K, Osherson, M, Swartz, M, Xiao, M, Acosta, JG, Cremaldi, LM, Oliveros, S, Perera, L, Summers, D, Bloom, K, Bose, S, Claes, DR, Dominguez, A, Fangmeier, C, Suarez, RG, Meier, F, Monroy, J, Hahn, K, Sevova, S, Sung, K, Trovato, M, Bartz, E, Duggan, D, Halkiadakis, E, Lath, A, Park, M, Schnetzer, S, Stone, R, Walker, M, Malik, S, Mendez, H, Vargas, JER, Alyari, M, Dolen, J, George, J, Godshalk, A, Iashvili, I, Kaisen, J, Kharchilava, A, Rappoccio, S, Alexander, J, Chaves, J, Chu, J, Dittmer, S, 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A., Basegmez, S., Bruno, G., Castello, R., Caudron, A., Ceard, L., De Callatay, B., Delaere, C., Du Pree, T., Forthomme, L., Giammanco, A., Hollar, J., Jez, P., Michotte, D., Nuttens, C., Perrini, L., Pagano, D., Quertenmont, L., Selvaggi, M., Vidal Marono, M., Beliy, N., Caebergs, T., Daubie, E., Hammad, G. H., Härkönen, J., Lampén, T., Luukka, P. -R., Mäenpää, T., Peltola, T., Tuominen, E., Tuovinen, E., Eerola, P., Tuuva, T., Beaulieu, G., Boudoul, G., Combaret, C., Contardo, D., Gallbit, G., Lumb, N., Mathez, H., Mirabito, L., Perries, S., Sabes, D., Vander Donckt, M., Verdier, P., Viret, S., Zoccarato, Y., Agram, J. -L., Conte, E., Fontaine, J. -Ch., Andrea, J., Bloch, D., Bonnin, C., Brom, J. -M., Chabert, E., Charles, L., Goetzmann, Ch., Gross, L., Hosselet, J., Mathieu, C., Richer, M., Skovpen, K., Pistone, C., Fluegge, G., Kuensken, A., Geisler, M., Pooth, O., Stahl, A., Autermann, C., Edelhoff, M., Esser, H., Feld, L., Karpinski, W., Klein, K., Lipinski, M., Ostapchuk, A., Pierschel, G., Preuten, M., Raupach, F., Sammet, J., Schael, S., Schwering, G., Wittmer, B., Wlochal, M., Zhukov, V., Bartosik, N., Behr, J., Burgmeier, A., Calligaris, L., Dolinska, G., Eckerlin, G., Eckstein, D., Eichhorn, T., Fluke, G., Garay Garcia, J., Gizhko, A., Hansen, K., Harb, A., Hauk, J., Kalogeropoulos, A., Kleinwort, C., Korol, I., Lange, W., Lohmann, W., Mankel, R., Maser, H., Mittag, G., Muhl, C., Mussgiller, A., Nayak, A., Ntomari, E., Perrey, H., Pitzl, D., Schroeder, M., Seitz, C., Spannagel, S., Zuber, A., Biskop, H., Blobel, V., Buhmann, P., Centis-Vignali, M., Draeger, A. -R., Erfle, J., Garutti, E., Haller, J., Hoffmann, M., Junkes, A., Lapsien, T., Mättig, S., Matysek, M., Perieanu, A., Poehlsen, J., Poehlsen, T., Scharf, Ch., Schleper, P., Schmidt, A., Sola, V., Steinbrück, G., Wellhausen, J., Barvich, T., Barth, Ch., Boegelspacher, F., De Boer, W., Butz, E., Casele, M., Colombo, F., Dierlamm, A., Eber, R., Freund, B., Hartmann, F., Hauth, Th., Heindl, S., Hoffmann, K. -H., Husemann, U., Kornmeyer, A., Mallows, S., Muller, Th., Nuernberg, A., Printz, M., Simonis, H. J., Steck, P., Weber, M., Weiler, Th., Bhardwaj, A., Kumar, A., Ranjan, K., Bakhshiansohl, H., Behnamian, H., Khakzad, M., Naseri, M., Cariola, P., De Robertis, G., Fiore, L., Franco, M., Loddo, F., Sala, G., Silvestris, L., Creanza, D., De Palma, M., Maggi, G., My, S., Selvaggi, G., Albergo, S., Cappello, G., Chiorboli, M., Costa, S., Giordano, F., Di Mattia, A., Potenza, R., Saizu, M. A., Tricomi, A., Tuvè, C., Barbagli, G., Brianzi, M., Ciaranfi, R., Civinini, C., Gallo, E., Meschini, M., Paoletti, S., Sguazzoni, G., Ciulli, V., D'Alessandro, R., Gonzi, S., Gori, V., Focardi, E., Lenzi, P., Scarlini, E., Tropiano, A., Viliani, L., Ferro, F., Robutti, E., Lo Vetere, M., Gennai, S., Malvezzi, S., Menasce, D., Moroni, L., Pedrini, D., Dinardo, M., Fiorendi, S., Manzoni, R. A., Azzi, P., Bacchetta, N., Bisello, D., Dall'Osso, M., Dorigo, T., Giubilato, P., Pozzobon, N., Tosi, M., Zucchetta, A., De Canio, F., Gaioni, L., Manghisoni, M., Nodari, B., Re, V., Traversi, G., Comotti, D., Ratti, L., Bilei, G. M., Bissi, L., Checcucci, B., Magalotti, D., Menichelli, M., Saha, A., Servoli, L., Storchi, L., Biasini, M., Conti, E., Ciangottini, D., Fanò, L., Lariccia, P., Mantovani, G., Passeri, D., Placidi, P., Salvatore, M., Santocchia, A., Solestizi, L. A., Spiezia, A., Androsov, K., Azzurri, P., Arezzini, S., Bagliesi, G., Basti, A., Boccali, T., Bosi, F., Castaldi, R., Ciampa, A., Ciocci, M. A., Dell'Orso, R., Fedi, G., Giassi, A., Grippo, M. T., Lomtadze, T., Magazzu, G., Mazzoni, E., Minuti, M., Moggi, A., Moon, C. S., Morsani, F., Palla, F., Palmonari, F., Raffaelli, F., Savoy-Navarro, A., Serban, A. T., Spagnolo, P., Tenchini, R., Venturi, A., Verdini, P. G., Martini, L., Messineo, A., Rizzi, A., Tonelli, G., Calzolari, F., Donato, S., Fiori, F., Ligabue, F., Vernieri, C., Demaria, N., Rivetti, A., Bellan, R., Casasso, S., Costa, M., Covarelli, R., Migliore, E., Monteil, E., Musich, M., Pacher, L., Ravera, F., Romero, A., Solano, A., Trapani, P., Jaramillo Echeverria, R., Fernandez, M., Gomez, G., Moya, D., Gonzalez Sanchez, F. J., Munoz Sanchez, F. J., Vila, I., Virto, A. 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D., Teodorescu, L., Bainbridge, R., Dauncey, P., Fulcher, J., Hall, G., Magnan, A. -M., Pesaresi, M., Raymond, D. M., Uchida, K., Coughlan, J. A., Harder, K., Ilic, J., Tomalin, I. R., Garabedian, A., Heintz, U., Narain, M., Nelson, J., Sagir, S., Speer, T., Swanson, J., Tersegno, D., Watson-Daniels, J., Chertok, M., Conway, J., Conway, R., Flores, C., Lander, R., Pellett, D., Ricci-Tam, F., Squires, M., Thomson, J., Yohay, R., Burt, K., Ellison, J., Hanson, G., Malberti, M., Olmedo, M., Cerati, G., Sharma, V., Vartak, A., Yagil, A., Zevi Della Porta, G., Dutta, V., Gouskos, L., Incandela, J., Kyre, S., Mccoll, N., Mullin, S., White, D., Cumalat, J. P., Ford, W. T., Gaz, A., Krohn, M., Stenson, K., Wagner, S. R., Baldin, B., Bolla, G., Burkett, K., Butler, J., Cheung, H., Chramowicz, J., Christian, D., Cooper, W. E., Deptuch, G., Derylo, G., Gingu, C., Gruenendahl, S., Hasegawa, S., Hoff, J., Howell, J., Hrycyk, M., Jindariani, S., Johnson, M., Jung, A., Joshi, U., Kahlid, F., Lei, C. M., Lipton, R., Liu, T., Los, S., Matulik, M., Merkel, P., Nahn, S., Prosser, A., Rivera, R., Shenai, A., Spiegel, L., Tran, N., Uplegger, L., Voirin, E., Yin, H., Adams, M. R., Berry, D. R., Evdokimov, A., Evdokimov, O., Gerber, C. E., Hofman, D. J., Kapustka, B. K., O'Brien, C., Sandoval Gonzalez, D. I., Trauger, H., Turner, P., Parashar, N., Stupak, J., Bortoletto, D., Bubna, M., Hinton, N., Jones, M., Miller, D. H., Shi, X., Tan, P., Baringer, P., Bean, A., Benelli, G., Gray, J., Majumder, D., Noonan, D., Sanders, S., Stringer, R., Ivanov, A., Makouski, M., Skhirtladze, N., Taylor, R., Anderson, I., Fehling, D., Gritsan, A., Maksimovic, P., Martin, C., Nash, K., Osherson, M., Swartz, M., Xiao, M., Acosta, J. G., Cremaldi, L. M., Oliveros, S., Perera, L., Summers, D., Bloom, K., Bose, S., Claes, D. R., Dominguez, A., Fangmeier, C., Gonzalez Suarez, R., Meier, F., Monroy, J., Hahn, K., Sevova, S., Sung, K., Trovato, M., Bartz, E., Duggan, D., Halkiadakis, E., Lath, A., Park, M., Schnetzer, S., Stone, R., Walker, M., Malik, S., Mendez, H., Ramirez Vargas, J. E., Alyari, M., Dolen, J., George, J., Godshalk, A., Iashvili, I., Kaisen, J., Kharchilava, A., Rappoccio, S., Alexander, J., Chaves, J., Chu, J., Dittmer, S., Kaufman, G., Mirman, N., Ryd, A., Salvati, E., Skinnari, L., Thom, J., Thompson, J., Tucker, J., Winstrom, L., Akgün, B., Ecklund, K. M., Nussbaum, T., Zabel, J., Betchart, B., Demina, R., Hindrichs, O., Petrillo, G., Eusebi, R., Osipenkov, I., Perloff, A., Ulmer, K. A., Delannoy, A. G., D'Angelo, P., Johns, W., Adam, W, Bergauer, T, Dragicevic, M, Friedl, M, Fruehwirth, R, Hoch, M, Hrubec, J, Krammer, M, Treberspurg, W, Waltenberger, W, Alderweireldt, S, Beaumont, W, Janssen, X, Luyckx, S, Van Mechelen, P, Van Remortel, N, Van Spilbeeck, A, Barria, P, Caillol, C, Clerbaux, B, De Lentdecker, G, Dobur, D, Favart, L, Grebenyuk, A, Lenzi, T, Leonard, A, Maerschalk, T, Mohammadi, A, Pernie, L, Randle-Conde, A, Reis, T, Seva, T, Thomas, L, Vander Velde, C, Vanlaer, P, Wang, J, Zenoni, F, Abu Zeid, S, Blekman, F, De Bruyn, I, D'Hondt, J, Daci, N, Deroover, K, Heracleous, N, Keaveney, J, Lowette, S, Moreels, L, Olbrechts, A, Python, Q, Tavernier, S, Van Mulders, P, Van Onsem, G, Van Parijs, I, Strom, D, Basegmez, S, Bruno, G, Castello, R, Caudron, A, Ceard, L, De Callatay, B, Delaere, C, Du Pree, T, Forthomme, L, Giammanco, A, Hollar, J, Jez, P, Michotte, D, Nuttens, C, Perrini, L, Pagano, D, Quertenmont, L, Selvaggi, M, Vidal Marono, M, Beliy, N, Caebergs, T, Daubie, E, Hammad, G, Harkonen, J, Lampen, T, Luukka, P, Maenpaa, T, Peltola, T, Tuominen, E, Tuovinen, E, Eerola, P, Tuuva, T, Beaulieu, G, Boudoul, G, Combaret, C, Contardo, D, Gallbit, G, Lumb, N, Mathez, H, Mirabito, L, Perries, S, Sabes, D, Vander Donckt, M, Verdier, P, Viret, S, Zoccarato, Y, Agram, J, Conte, E, Fontaine, J, Andrea, J, Bloch, D, Bonnin, C, Brom, J, Chabert, E, Charles, L, Goetzmann, C, Gross, L, Hosselet, J, Mathieu, C, Richer, M, Skovpen, K, Pistone, C, Fluegge, G, Kuensken, A, Geisler, M, Pooth, O, Stahl, A, Autermann, C, Edelhoff, M, Esser, H, Feld, L, Karpinski, W, Klein, K, Lipinski, M, Ostapchuk, A, Pierschel, G, Preuten, M, Raupach, F, Sammet, J, Schael, S, Schwering, G, Wittmer, B, Wlochal, M, Zhukov, V, Bartosik, N, Behr, J, Burgmeier, A, Calligaris, L, Dolinska, G, Eckerlin, G, Eckstein, D, Eichhorn, T, Fluke, G, Garay Garcia, J, Gizhko, A, Hansen, K, Harb, A, Hauk, J, Kalogeropoulos, A, Kleinwort, C, Korol, I, Lange, W, Lohmann, W, Mankel, R, Maser, H, Mittag, G, Muhl, C, Mussgiller, A, Nayak, A, Ntomari, E, Perrey, H, Pitzl, D, Schroeder, M, Seitz, C, Spannagel, S, Zuber, A, Biskop, H, Blobel, V, Buhmann, P, Centis-Vignali, M, Draeger, A, Erfle, J, Garutti, E, Haller, J, Hoffmann, M, Junkes, A, Lapsien, T, Mattig, S, Matysek, M, Perieanu, A, Poehlsen, J, Poehlsen, T, Scharf, C, Schleper, P, Schmidt, A, Sola, V, Steinbruck, G, Wellhausen, J, Barvich, T, Barth, C, Boegelspacher, F, De Boer, W, Butz, E, Casele, M, Colombo, F, Dierlamm, A, Eber, R, Freund, B, Hartmann, F, Hauth, T, Heindl, S, Hoffmann, K, Husemann, U, Kornmeyer, A, Mallows, S, Muller, T, Nuernberg, A, Printz, M, Simonis, H, Steck, P, Weber, M, Weiler, T, Bhardwaj, A, Kumar, A, Ranjan, K, Bakhshiansohl, H, Behnamian, H, Khakzad, M, Naseri, M, Cariola, P, De Robertis, G, Fiore, L, Franco, M, Loddo, F, Sala, G, Silvestris, L, Creanza, D, De Palma, M, Maggi, G, My, S, Selvaggi, G, Albergo, S, Cappello, G, Chiorboli, M, Costa, S, Giordano, F, Di Mattia, A, Potenza, R, Saizu, M, Tricomi, A, Tuve, C, Barbagli, G, Brianzi, M, Ciaranfi, R, Civinini, C, Gallo, E, Meschini, M, Paoletti, S, Sguazzoni, G, Ciulli, V, D'Alessandro, R, Gonzi, S, Gori, V, Focardi, E, Lenzi, P, Scarlini, E, Tropiano, A, Viliani, L, Ferro, F, Robutti, E, Lo Vetere, M, Gennai, S, Malvezzi, S, Menasce, D, Moroni, L, Pedrini, D, Dinardo, M, Fiorendi, S, Manzoni, R, Azzi, P, Bacchetta, N, Bisello, D, Dall'Osso, M, Dorigo, T, Giubilato, P, Pozzobon, N, Tosi, M, Zucchetta, A, De Canio, F, Gaioni, L, Manghisoni, M, Nodari, B, Re, V, Traversi, G, Comotti, D, Ratti, L, Bilei, G, Bissi, L, Checcucci, B, Magalotti, D, Menichelli, M, Saha, A, Servoli, L, Storchi, L, Biasini, M, Conti, E, Ciangottini, D, Fano, L, Lariccia, P, Mantovani, G, Passeri, D, Placidi, P, Salvatore, M, Santocchia, A, Solestizi, L, Spiezia, A, Androsov, K, Azzurri, P, Arezzini, S, Bagliesi, G, Basti, A, Boccali, T, Bosi, F, Castaldi, R, Ciampa, A, Ciocci, M, Dell'Orso, R, Fedi, G, Giassi, A, Grippo, M, Lomtadze, T, Magazzu, G, Mazzoni, E, Minuti, M, Moggi, A, Moon, C, Morsani, F, Palla, F, Palmonari, F, Raffaelli, F, Savoy-Navarro, A, Serban, A, Spagnolo, P, Tenchini, R, Venturi, A, Verdini, P, Martini, L, Messineo, A, Rizzi, A, Tonelli, G, Calzolari, F, Donato, S, Fiori, F, Ligabue, F, Vernieri, C, Demaria, N, Rivetti, A, Bellan, R, Casasso, S, Costa, M, Covarelli, R, Migliore, E, Monteil, E, Musich, M, Pacher, L, Ravera, F, Romero, A, Solano, A, Trapani, P, Jaramillo Echeverria, R, Fernandez, M, Gomez, G, Moya, D, Gonzalez Sanchez, F, Munoz Sanchez, F, Vila, I, Virto, A, Abbaneo, D, Ahmed, I, Albert, E, Auzinger, G, Berruti, G, Bianchi, G, Blanchot, G, Breuker, H, Ceresa, D, Christiansen, J, Cichy, K, Daguin, J, D'Alfonso, M, D'Auria, A, Detraz, S, De Visscher, S, Deyrail, D, Faccio, F, Felici, D, Frank, N, Gill, K, Giordano, D, Harris, P, Honma, A, Kaplon, J, Kornmayer, A, Kottelat, L, Kovacs, M, Mannelli, M, Marchioro, A, Marconi, S, Martina, S, Mersi, S, Michelis, S, Moll, M, Onnela, A, Pakulski, T, Pavis, S, Peisert, A, Pernot, J, Petagna, P, Petrucciani, G, Postema, H, Rose, P, Rzonca, M, Stoye, M, Tropea, P, Troska, J, Tsirou, A, Vasey, F, Vichoudis, P, Verlaat, B, Zwalinski, L, Bachmair, F, Becker, R, Bani, L, Di Calafiori, D, Casal, B, Djambazov, L, Donega, M, Dunser, M, Eller, P, Grab, C, Hits, D, Horisberger, U, Hoss, J, Kasieczka, G, Lustermann, W, Mangano, B, Marionneau, M, Martinez Ruiz Del Arbol, P, Masciovecchio, M, Perrozzi, L, Roeser, U, Rossini, M, Starodumov, A, Takahashi, M, Wallny, R, Amsler, C, Bosiger, K, Caminada, L, Canelli, F, Chiochia, V, De Cosa, A, Galloni, C, Hreus, T, Kilminster, B, Lange, C, Maier, R, Ngadiuba, J, Pinna, D, Robmann, P, Taroni, S, Yang, Y, Bertl, W, Deiters, K, Erdmann, W, Horisberger, R, Kaestli, H, Kotlinski, D, Langenegger, U, Meier, B, Rohe, T, Streuli, S, Chen, P, Dietz, C, Grundler, U, Hou, W, Lu, R, Moya, M, Wilken, R, Cussans, D, Flacher, H, Goldstein, J, Grimes, M, Jacob, J, Seif El Nasr-Storey, S, Cole, J, Hobson, P, Leggat, D, Reid, I, Teodorescu, L, Bainbridge, R, Dauncey, P, Fulcher, J, Hall, G, Magnan, A, Pesaresi, M, Raymond, D, Uchida, K, Coughlan, J, Harder, K, Ilic, J, Tomalin, I, Garabedian, A, Heintz, U, Narain, M, Nelson, J, Sagir, S, Speer, T, Swanson, J, Tersegno, D, Watson-Daniels, J, Chertok, M, Conway, J, Conway, R, Flores, C, Lander, R, Pellett, D, Ricci-Tam, F, Squires, M, Thomson, J, Yohay, R, Burt, K, Ellison, J, Hanson, G, Malberti, M, Olmedo, M, Cerati, G, Sharma, V, Vartak, A, Yagil, A, Zevi Della Porta, G, Dutta, V, Gouskos, L, Incandela, J, Kyre, S, Mccoll, N, Mullin, S, White, D, Cumalat, J, Ford, W, Gaz, A, Krohn, M, Stenson, K, Wagner, S, Baldin, B, Bolla, G, Burkett, K, Butler, J, Cheung, H, Chramowicz, J, Christian, D, Cooper, W, Deptuch, G, Derylo, G, Gingu, C, Gruenendahl, S, Hasegawa, S, Hoff, J, Howell, J, Hrycyk, M, Jindariani, S, Johnson, M, Jung, A, Joshi, U, Kahlid, F, Lei, C, Lipton, R, Liu, T, Los, S, Matulik, M, Merkel, P, Nahn, S, Prosser, A, Rivera, R, Shenai, A, Spiegel, L, Tran, N, Uplegger, L, Voirin, E, Yin, H, Adams, M, Berry, D, Evdokimov, A, Evdokimov, O, Gerber, C, Hofman, D, Kapustka, B, O'Brien, C, Sandoval Gonzalez, D, Trauger, H, Turner, P, Parashar, N, Stupak, J, Bortoletto, D, Bubna, M, Hinton, N, Jones, M, Miller, D, Shi, X, Tan, P, Baringer, P, Bean, A, Benelli, G, Gray, J, Majumder, D, Noonan, D, Sanders, S, Stringer, R, Ivanov, A, Makouski, M, Skhirtladze, N, Taylor, R, Anderson, I, Fehling, D, Gritsan, A, Maksimovic, P, Martin, C, Nash, K, Osherson, M, Swartz, M, Xiao, M, Acosta, J, Cremaldi, L, Oliveros, S, Perera, L, Summers, D, Bloom, K, Bose, S, Claes, D, Dominguez, A, Fangmeier, C, Gonzalez Suarez, R, Meier, F, Monroy, J, Hahn, K, Sevova, S, Sung, K, Trovato, M, Bartz, E, Duggan, D, Halkiadakis, E, Lath, A, Park, M, Schnetzer, S, Stone, R, Walker, M, Malik, S, Mendez, H, Ramirez Vargas, J, Alyari, M, Dolen, J, George, J, Godshalk, A, Iashvili, I, Kaisen, J, Kharchilava, A, Rappoccio, S, Alexander, J, Chaves, J, Chu, J, Dittmer, S, Kaufman, G, Mirman, N, Ryd, A, Salvati, E, Skinnari, L, Thom, J, Thompson, J, Tucker, J, Winstrom, L, Akgun, B, Ecklund, K, Nussbaum, T, Zabel, J, Betchart, B, Demina, R, Hindrichs, O, Petrillo, G, Eusebi, R, Osipenkov, I, Perloff, A, Ulmer, K, Delannoy, A, D'Angelo, P, Johns, W, Elementary Particle Physics, Physics, Faculty of Sciences and Bioengineering Sciences, Vriendenkring VUB, UCL - SST/IRMP - Institut de recherche en mathématique et physique, Institut de Physique Nucléaire de Lyon (IPNL), Centre National de la Recherche Scientifique (CNRS)-Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3), CMS Tracker Group, CMS Collaboration, Helsinki Institute of Physics, and Department of Physics
Subjects: electron, Technology, Physics - Instrumentation and Detectors, Detector modelling and simulations II (electric field, Physics::Instrumentation and Detectors, Detector modelling and simulations II (electric fields, Detector modelling and simulations II (electric fields, charge transport, multiplication and induction, pulse formation, electron emission, etc), Radiation damage to detector materials (solid state), Radiation-hard detectors, Si microstrip and pad detectors, Electron, Settore ING-INF/01 - Elettronica, 01 natural sciences, Etc), charge, transport, multiplication and induction, pulse formation, emission, etc), DETECTORS, ELECTRONS, HOLES, Electron emission, capture [charged particle], Detectors and Experimental Techniques, Instrumentation, Instruments & Instrumentation, physics.ins-det, Si microstrip and pad detector, Mathematical Physics, Large Hadron Collider, CMS, Physics, Instrumentation and Detectors (physics.ins-det), Nuclear & Particles Physics, Wavelength, performance [tracking detector], Physique des particules élémentaires, Charge carrier, Atomic physics, Materials science, Silicon, education, chemistry.chemical_element, FOS: Physical sciences, Trapping, irradiation [p], Charge transport, 114 Physical sciences, Radiation-hard detector, Electric field, 0103 physical sciences, Irradiation, [PHYS.PHYS.PHYS-INS-DET]Physics [physics]/Physics [physics]/Instrumentation and Detectors [physics.ins-det], ddc:610, 010306 general physics, numerical calculations, Multiplication and induction, Science & Technology, 010308 nuclear & particles physics, hep-ex, FISICA DELLE PARTICELLE, Detector modelling and simulations II (electric fields), Pulse formation, charge transport, chemistry, Physics and Astronomy, efficiency, electron emission, semiconductor detector, Detector modelling and simulations II (electric fields, charge, transport, multiplication and induction, pulse formation, electron, emission, etc)
Abstract: The degradation of signal in silicon sensors is studied under conditions expected at the CERN High-Luminosity LHC. 200μm thick n-type silicon sensors are irradiated with protons of different energies to fluences of up to 3 · 1015 neq/cm2. Pulsed red laser light with a wavelength of 672 nm is used to generate electron-hole pairs in the sensors. The induced signals are used to determine the charge collection efficiencies separately for electrons and holes drifting through the sensor. The effective trapping rates are extracted by comparing the results to simulation. The electric field is simulated using Synopsys device simulation assuming two effective defects. The generation and drift of charge carriers are simulated in an independent simulation based on PixelAV. The effective trapping rates are determined from the measured charge collection efficiencies and the simulated and measured time-resolved current pulses are compared. The effective trapping rates determined for both electrons and holes are about 50% smaller than those obtained using standard extrapolations of studies at low fluences and suggest an improved tracker performance over initial expectations., 0, info:eu-repo/semantics/published
Published: 2016
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26. Ultrafast Molecular Rotors and Their CO2 Tuning in MOFs with Rod-Like Ligands

Author: Angiolina Comotti, Piero Sozzani, F Castiglioni, Angelo Maspero, Silvia Bracco, Simona Galli, M Negroni, Bracco, S, Castiglioni, F, Comotti, A, Galli, S, Negroni, M, Maspero, A, and Sozzani, P
Subjects: CO2 adsorption, solid state NMR spectroscopy, dynamics, molecular rotors, porous materials, solid state NMR spectroscopy, supramolecular chemistry, Diffusion, Supramolecular chemistry, 02 engineering and technology, CHIM/04 - CHIMICA INDUSTRIALE, 010402 general chemistry, 01 natural sciences, Catalysis, law.invention, molecular rotor, Computational chemistry, law, Molecule, porous material, Spinning, MOF, dynamic, Chemistry, Rotor (electric), Organic Chemistry, Rotation around a fixed axis, General Chemistry, Nuclear magnetic resonance spectroscopy, 021001 nanoscience & nanotechnology, 0104 chemical sciences, CHIM/02 - CHIMICA FISICA, Chemical physics, 0210 nano-technology, Porous medium
Abstract: A metal organic framework (MOF) engineered to contain in its scaffold rod-like struts featuring ultrafast molecular rotors showed extremely rapid 180 Â° flip reorientation with rotational rates of 1011 Hz at 150 K. Crystal-pore accessibility of the MOF allowed the CO2 molecules to enter the cavities and control the rotor spinning speed down to 105 Hz at 150 K. Rotor dynamics, as modulated by CO2 loading/unloading in the porous crystals, was described by proton T1 and 2H NMR spectroscopy. This strategy enabled the regulation of rotary motion by the diffusion of the gas within the channels and the determination of the energetics of rotary dynamics in the presence of CO2
Published: 2017

27. Porous 3D polymers for high pressure methane storage and carbon dioxide capture

Author: Piero Sozzani, J Perego, Silvia Bracco, D Piga, Angiolina Comotti, Irene Bassanetti, Bracco, S, Piga, D, Bassanetti, I, Perego, J, Comotti, A, and Sozzani, P
Subjects: Materials science, porous polymers, CO2, methane, gas storage, solid state nmr, Yamamoto cross-coupling, Friedel-Crafts alkylation, Nanotechnology, 02 engineering and technology, 010402 general chemistry, CHIM/04 - CHIMICA INDUSTRIALE, 01 natural sciences, Methane, chemistry.chemical_compound, Adsorption, Desorption, General Materials Science, Porosity, chemistry.chemical_classification, Renewable Energy, Sustainability and the Environment, Condensation, General Chemistry, Polymer, 021001 nanoscience & nanotechnology, 0104 chemical sciences, CHIM/02 - CHIMICA FISICA, chemistry, Chemical engineering, 0210 nano-technology, Porous medium, Bar (unit)
Abstract: High surface area 3D polymers represent one of the most promising classes of porous materials because of their high gas uptake and stability to thermal and chemical degradation. A series of porous organic polymers with aromatic building units have been synthesized and compared to explore their high-pressure performance as adsorbents of gases of relevant importance for energy and the environment. Particular attention was paid to methane storage up to pressures as high as 180 bar at ambient temperature. Porous polymers were prepared starting from a wide choice of spatially expanded aromatic monomers: a systematic change in the number of rings, variable size and shape was taken under consideration. The high number of rings (up to 6), which act as multiple reactive sites and form a number of connections between the multi-dentate nodes, result in an extensive cross-linked framework. Condensation was obtained by two alternative synthetic routes, viz., Yamamoto cross-coupling and Friedel–Crafts alkylation reactions. The structural characteristics and high stability of the porous polymers, even to mechanical compression, were carefully determined by several methods, including 1D and 2D solid state NMR, FT IR and thermal analyses. The CH4 uptake in the porous polymers allowed an understanding of the incremental response to pressure, up to extremely high values, and the exploitation of the extensive pressure range to customize the gas adsorption/desorption cycles for storage and transportation. Owing to the notable presence of large mesopores and network flexibility, combined with high surface area, a remarkable gain at high pressure was achieved, ensuring a highly competitive uptake/delivery efficiency. At 180 bar, adsorption values up to 445 cm3 STP g−1 were measured for porous organic polymers such as carbazolyl- and triptycene-based materials. The benchmark of these materials PAF1 reaches the value of 916 cm3 STP g−1 of adsorbed CH4, exceeding the performance of most of the best performing MOFs, COFs and activated carbons. CO2 and N2 adsorption isotherms collected at room temperature enabled the assessment of the suitability of such polymer networks for CO2 selective separation and capture. In summary, the in-depth and extensive comparative screening within this class of materials up to high pressures provides the necessary parameters for further synthetic and applicative work.
Published: 2017

28. Porous dipeptide crystals as volatile-drug vessels

Author: Piero Sozzani, Angiolina Comotti, D Asnaghi, Silvia Bracco, M Negroni, Bracco, S, Asnaghi, D, Negroni, M, Sozzani, P, and Comotti, A
Subjects: Magnetic Resonance Spectroscopy, Materials science, Hydrocarbons, Fluorinated, Surface Properties, Vapor pressure, Molecular Conformation, Ab initio, 02 engineering and technology, 010402 general chemistry, 01 natural sciences, Catalysis, law.invention, chemistry.chemical_compound, law, absorption of fluorinated ether, Materials Chemistry, GCMC simulation, Particle Size, Crystallization, solid state NMR spectroscopy, ab initio conformational analysi, Porosity, porous crystalline dipeptide, Anesthetics, Drug Carriers, Dipeptide, Metals and Alloys, Sorption, Dipeptides, General Chemistry, Nuclear magnetic resonance spectroscopy, 021001 nanoscience & nanotechnology, 0104 chemical sciences, Surfaces, Coatings and Films, Electronic, Optical and Magnetic Materials, chemistry, Chemical engineering, anesthetic, Ceramics and Composites, Quantum Theory, 0210 nano-technology, Drug carrier, Monte Carlo Method
Abstract: Porous crystalline dipeptides absorb, reversibly from the gas phase, a series of volatile fluorinated ethers in use as anesthetics. Their vapor pressure was considerably reduced, with favorable guest capture and release. Variable channel sizes were customized for selective sorption and pressure thresholds were observed in the narrowest pores. 1H, 13C and 19F MAS NMR coupled with ab initio conformational analysis and grand canonical Monte Carlo simulations highlight the guest loading and arrangement adopted in the congruent nanochannels, suggesting how the anesthetics can accommodate in biochemical receptors.
Published: 2017

29. Porous Molecular Crystals by Macrocyclic Coordination Supramolecules

Author: Angiolina Comotti, Gianluca Calestani, Piero Sozzani, Irene Bassanetti, Francesco Mezzadri, Luciano Marchiò, Silvia Bracco, Bassanetti, I, Comotti, A, Sozzani, P, Bracco, S, Calestani, G, Mezzadri, F, and Marchiò, L
Subjects: Stereochemistry, Metal ions in aqueous solution, Supramolecular chemistry, General Chemistry, CHIM/04 - CHIMICA INDUSTRIALE, Biochemistry, porous molecular crystals, metallacycles, gas adsorption, CO2, solid state NMR, Catalysis, CHIM/02 - CHIMICA FISICA, chemistry.chemical_compound, Crystallography, Colloid and Surface Chemistry, Thioether, chemistry, Tetrahedron, Moiety, Porosity
Abstract: In this study, we show how the combination of metal ions, counter-anions and opportunely functionalized and preorganized ligands gives rise to two distinct supramolecular isomers, coordination polymeric chains and hexameric macrocycles. The hexamers then aggregate to form a cubic structure exhibiting permanent microporosity. The supramolecular assemblies are formed with Ag(+), thioether functionalized bis(pirazolyl)methane ligands and CF3SO3(-)/PF6(-) as the counter-anions. Five different ligands were prepared by modifying the peripheral thioether moiety with naphthyl, methoxy, m-Me, p-Me and F groups (L(SNf), L(SPhOMe), L(SPhm-Me), L(SPhp-Me), and L(SPhF)). Helicoidal coordination polymeric chains are formed with CF3SO3(-) (general formula [Ag(L)]n(CF3SO3)n), whereas macrocyclic hexamers are formed with PF6(-) (general formula [Ag(L)]6(PF6)6). The macrocycles self-assemble into ordered capsules with the shape of a tetrahedron, and the overall framework is sustained by Ag(+)···(PF6(-))···Ag(+) contacts. The capsules generate a highly symmetric structural arrangement, which is characterized by permanent microporosity arising from two distinct types of microporous chambers in the structure. The gas absorption isotherms show that the materials can selectively adsorb CO2 and N2O over CH4 and N2. The modulation of the microporosity of the materials is achieved by the different thioether functionalization of the ligands L(SNf), L(SPhOMe), L(SPhm-Me), and L(SPhF). The diffusion and localization of the gas molecules within the cavities were investigated by 2D (1)H-(13)C solid state NMR on samples loaded with enriched (13)CO2, showing that both types of cavities are accessible to guest molecules from the gas phase.
Published: 2014

30. Molecular Rotors in Porous Organic Frameworks

Author: Shilun Qiu, Angiolina Comotti, Teng Ben, Piero Sozzani, Silvia Bracco, Comotti, A, Bracco, S, Ben, T, Qiu, S, and Sozzani, P
Subjects: Diffusion (acoustics), iodine, Chemistry, molecular dynamic, Rotation around a fixed axis, Nanotechnology, General Chemistry, Molecular rotors, General Medicine, CHIM/04 - CHIMICA INDUSTRIALE, Ferroelectricity, Catalysis, microporous material, CHIM/02 - CHIMICA FISICA, Molecular dynamics, NMR spectroscopy, adsorption, Actuator, Porosity
Abstract: Porous organic frameworks perform a variety of functions, owing to their extremely large surface areas, but the dynamics of the structural elements have never been explored. Our discovery of ultra-fast molecular rotors (10(6) Hz at 225 K) in their architectures allows us to look at them from a new perspective. The constructive elements are robust struts and rapid rotors, resulting in a dynamic material whose motion can be frozen or released at will. The rotational motion can be actively regulated in response to guests. As the temperature is increased, the rotors spin ever faster, approaching free-rotational diffusion at 550 K. The unusual combination of remarkable nanoporosity with fast dynamics is intriguing for engineering oscillating dipoles and producing responsive materials with switchable ferroelectricity, and for applications spanning from sensors to actuators, which capture and release chemicals on command.
Published: 2014

31. A computational study of the 1,4-addition of lithium enolates to conjugated carbonyl compounds

Author: Bernardi, Anna, Capelli, Anna Maria, Cassinari, Andrea, Comotti, Angiolina, Gennari, Cesare, and Scolastico, Carlo
Subjects: Chemical reactions -- Research, Biological sciences, Chemistry
Abstract: A study of the MNDO potential energy of the 1,4-addition of acetaldehyde lithium enolate to acrolein is presented. Computation of stationary points' relative energies reveal the existence of four cyclic intermediates consisting of eight atoms. This affords a qualitative explanation of the stereoselective trends observed. Optimization of the intermediate structures through molecular orbital calculations reveal that these structures bears remarkable similaruty with MNDO-optimized geometries.
Published: 1992

32. The rational design of highly stereoselective boron enolates using transition-state computer modeling: a novel, asymmetric anti aldol reaction for ketones

Author: Gennari, Cesare, Hewkin, Cheryl T., Molinari, Francesco, Bernardi, Anna, Comotti, Angiolina, Goodman, Jonathan M., and Patterson, Ian
Subjects: Organic compounds -- Synthesis, Organoboron compounds -- Usage, Aldehydes -- Research, Ketones -- Research, Stereochemistry -- Research, Rearrangements (Chemistry) -- Research, Biological sciences, Chemistry
Abstract: Computer-aided transition-state modeling enables the design and development of highly enantioselective anti aldol reactions using a new chiral boron ligand. The ligand design allows effective control of conformations and minimizes double gauche interactions. The boron reagent needed for the synthesis of the target ligand-derived E enolates is prepared from optically pure (-)-menthone. Enolization of cyclic and acyclic ketones with the reagent in dichloromethane/ether in the presence of acetonitrile, which ensures subsequent preferential attack on the aldehyde's re face, yields anti aldols with 86:14-100:0 anti/syn ratios and 56-85% enantiomeric purity.
Published: 1992

33. Photoinduced reversible switching of porosity in molecular crystals based on star-shaped azobenzene tetramers

Author: Simone d'Agostino, Serena Silvi, Paola Ceroni, Piero Sozzani, Fabrizia Grepioni, Angiolina Comotti, Margherita Venturi, Giacomo Bergamini, Irene Bassanetti, Taylor Hernandez, Alberto Credi, Massimo Baroncini, Baroncini, M., D'Agostino, S., Bergamini, G., Ceroni, P., Comotti, A., Sozzani, P., Bassanetti, I., Grepioni, F., Hernandez, T.M., Silvi, S., Venturi, M., Credi, A., Baroncini, M, D'Agostino, S, Bergamini, G, Ceroni, P, Comotti, A, Sozzani, P, Bassanetti, I, Grepioni, F, Hernandez, T, Silvi, S, Venturi, M, and Credi, A
Subjects: photochemistry, Birefringence, Photoisomerization, General Chemical Engineering, Crystal engineering, Optical materials, Photochemistry, Structural properties, Gas adsorption, Porous molecular crystal, solid state, General Chemistry, gas adsorption, photochromism, Photochemistry, CHIM/04 - CHIMICA INDUSTRIALE, Amorphous solid, chemistry.chemical_compound, Crystallinity, CHIM/02 - CHIMICA FISICA, azobenzene, Azobenzene, chemistry, Porosity, Photoisomerization, CO2 capture, X-ray diffraction, Single crystals, Azobenzene tetramers, Solid materials, Birefringence, Phase (matter), Porosity, porous materials, Isomerization
Abstract: The development of solid materials that can be reversibly interconverted by light between forms with different physicochemical properties is of great interest for separation, catalysis, optoelectronics, holography, mechanical actuation and solar energy conversion. Here, we describe a series of shape-persistent azobenzene tetramers that form porous molecular crystals in their E-configuration, the porosity of which can be tuned by changing the peripheral substituents on the molecule. Efficient E -> Z photoisomerization of the azobenzene units takes place in the solid state and converts the crystals into a non-porous amorphous melt phase. Crystallinity and porosity are restored upon Z -> E isomerization promoted by visible light irradiation or heating. We demonstrate that the photoisomerization enables reversible on/off switching of optical properties such as birefringence as well as the capture of CO2 from the gas phase. The linear design, structural versatility and synthetic accessibility make this new family of materials potentially interesting for technological applications.
Published: 2015

34. Highly ordered alignment of a vinyl polymer by host–guest cross-polymerization

Author: Piero Sozzani, Masahiko Tsujimoto, Gaetano Distefano, Silvia Bracco, Angiolina Comotti, Hirohito Suzuki, Seiji Isoda, Susumu Kitagawa, Takashi Uemura, Distefano, G, Suzuki, H, Tsujimoto, M, Isoda, S, Bracco, S, Comotti, A, Sozzani, P, Uemura, T, and Kitagawa, S
Subjects: Solid-state chemistry, Surface Properties, Coordination polymer, General Chemical Engineering, CHIM/04 - CHIMICA INDUSTRIALE, NANOCOMPOSITE, NANOSTRUCTURES, Polymerization, Styrene, METAL-ORGANIC FRAMEWORKS, chemistry.chemical_compound, Microscopy, Electron, Transmission, X-Ray Diffraction, Polymer chemistry, POROUS COORDINATION POLYMERS, chemistry.chemical_classification, Molecular Structure, Stereoisomerism, General Chemistry, Polymer, Vinyl polymer, POLYMER MORPHOLOGY, CHIM/02 - CHIMICA FISICA, Cross-Linking Reagents, Monomer, chemistry, Chemical engineering, POLYSTYRENE, FUNCTIONALIZATION, Polyvinyls, Polystyrene, Porosity, Powder Diffraction
Abstract: Chain alignment can significantly influence the macroscopic properties of a polymeric material, but no general and versatile methodology has yet been reported to obtain highly ordered crystalline packing of polymer chains, with high stability. Here, we disclose a strategy that relies on 'ordered crosslinks' to produce polymeric materials that exhibit a crystalline arrangement. Divinyl crosslinkers (2,5-divinyl-terephthalate) were first embedded, as substitutional ligands, into the structure of a porous coordination polymer (PCP), [Cu(terephthalate)triethylenediamine0.5]n. A representative vinyl monomer, styrene, was subsequently polymerized inside the channels of the host PCP. The polystyrene chains that form within the PCP channels also crosslink with the divinyl species. This bridges together the polymer chains of adjacent channels and ensures that, on selective removal of the PCP, the polymer chains remain aligned. Indeed, the resulting material exhibits long-range order and is stable to thermal and solvent treatments, as demonstrated by X-ray powder diffraction and transmission electron microscopy.
Published: 2013

35. Porous dipeptide crystals as selective CO2adsorbents: experimental isotherms vs. grand canonical Monte Carlo simulations and MAS NMR spectroscopy

Author: Gaetano Distefano, Silvia Bracco, Alberto Fraccarollo, Angiolina Comotti, Maurizio Cossi, Cristina Riccardi, M Beretta, Leonardo Marchese, Piero Sozzani, Comotti, A, Fraccarollo, A, Bracco, S, Beretta, M, Distefano, G, Cossi, M, Marchese, L, Riccardi, C, and Sozzani, P
Subjects: dipeptides, porosity, CO2, CH4, adsorption isotherms, Grand Canonical Monte Carlo simulations, MAS NMR, chemistry.chemical_classification, Mas nmr spectroscopy, Dipeptide, Direct observation, Analytical chemistry, Peptide, General Chemistry, CHIM/04 - CHIMICA INDUSTRIALE, Condensed Matter Physics, Methane, CHIM/02 - CHIMICA FISICA, chemistry.chemical_compound, Adsorption, chemistry, General Materials Science, Porosity, Grand canonical monte carlo
Abstract: Molecular crystals of dipeptides containing open channels can selectively absorb CO2 over N2 and CH4, as shown by experimental and simulated isotherms. The efficient CO2 capture enabled separation from methane and allowed the direct observation by 2D MAS NMR of CO2 sequestered in the peptide-based biozeolites. © 2013 The Royal Society of Chemistry
Published: 2013

36. Ammonia Decomposition over Iron Phthalocyanine-Based Materials

Author: Klaus Müllen, Massimiliano Comotti, Ferdi Schüth, Linjie Zhi, and Harun Tüysüz
Subjects: Organic Chemistry, Inorganic chemistry, chemistry.chemical_element, Carbon nanotube, Decomposition, Catalysis, law.invention, Inorganic Chemistry, chemistry.chemical_compound, Nickel, chemistry, law, Phthalocyanine, Physical and Theoretical Chemistry, Carbon, Pyrolysis, Chemical decomposition
Abstract: Iron phthalocyanine-based materials have been used herein as efficient catalysts for the ammonia decomposition reaction. These materials showed high activity, even superior to that showed by the commercial nickel-based catalyst and iron-doped carbon nanotubes, which were used as benchmarks in this study. Catalyst stability under reaction conditions appeared satisfactory, because no deactivation phenomena were observed. The type of the phthalocyanine precursor did not affect the catalytic performance; however, the preparation method had a strong effect. If the resulting material was exposed to the reaction conditions, some structural modification occurred. No clear correlation between phase composition and activity could be established because similar nitrogen content and similar crystalline domains in the sample led to different behaviors. However, the results of extensive characterization suggested that catalytic activities and conversion profiles were most likely dependent on material textural properties and thus on the preparation method used. The accessibility of iron species seems to be limited for catalysts prepared under vacuum. These phenomena are most likely responsible for the activation profile and for the low catalytic activity typical of these materials. In contrast, higher accessibility of iron species, typical of materials prepared under argon, would lead to improved and stable catalytic performance.
Published: 2015

37. P-Type Silicon Strip Sensors for the new CMS Tracker at HL-LHC

Author: Adam, W., Bergauer, T., Brondolin, E., Dragicevic, M., Friedl, M., Fruehwirth, R., Hoch, M., Hrubec, J., Koenig, A., Steininger, H., Waltenberger, W., Alderweireldt, S., Beaumont, W., Janssen, X., Lauwers, J., Van Mechelen, P., Van Remortel, N., Van Spilbeeck, A., Beghin, D., Brun, H., Clerbaux, B., Delannoy, H., De Lentdecker, G., Fasanella, G., Favart, L., Goldouzian, R., Grebenyuk, A., Karapostoli, G., Lenzi, Th., Leonard, A., Luetic, J., Postiau, N., Seva, T., Vanlaer, P., Vannerom, D., Wang, Q., Zhang, F., Abu Zeid, S., Blekman, F., De Bruyn, I., De Clercq, J., D'Hondt, J., Deroover, K., Lowette, S., Moortgat, S., Moreels, L., Python, Q., Skovpen, K., Van Mulders, P., Van Parijs, I., Bakhshiansohi, H., Bondu, O., Brochet, S., Bruno, G., Caudron, A., Delaere, C., Delcourt, M., De Visscher, S., Francois, B., Giammanco, A., Jafari, A., Komm, M., Krintiras, G., Lemaitre, V., Magitteri, A., Mertens, A., Michotte, D., Musich, M., Piotrzkowski, K., Quertenmont, L., Szilasi, N., Marono, M. Vidal, Wertz, S., Belly, N., Caebergs, T., Daubie, E., Hammad, G. H., Harkonen, J., Lampen, T., Luukka, P., Peltola, T., Tuominen, E., Tuovinen, E., Eerola, P., Tuuva, T., Baulieu, G., Boudoul, G., Caponetto, L., Combaret, C., Contardo, D., Dupasquier, T., Gallbit, G., Lumb, N., Mirabito, L., Perries, S., V, er Donckt, M., Viret, S., Agram, J. -L., Andrea, J., Bloch, D., Bonnin, C., Brom, J. -M., Chabert, E., Chanon, N., Charles, L., Conte, E., Fontaine, J. -Ch., Gross, L., Hosselet, J., Jansova, M., Tromson, D., Autermann, C., Feld, L., Karpinski, W., Kiesel, K. M., Klein, K., Lipinski, M., Ostapchuk, A., Pierschel, G., Preuten, M., Rauch, M., Schael, S., Schomakers, C., Schulz, J., Schwering, G., Wlochal, M., Zhukov, V., Pistone, C., Fluegge, G., Kuensken, A., Pooth, O., Stahl, A., Aldaya, M., Asawatangtrakuldee, C., Beernaert, K., Bertsche, D., Contreras-Campana, C., Eckerlin, G., Eckstein, D., Eichhorn, T., Gallo, E., Garcia, J. Garay, Hansen, K., Haranko, M., Harb, A., Hauk, J., Keaveney, J., Kalogeropoulos, A., Kleinwort, C., Lohmann, W., Mankel, R., Maser, H., Mittag, G., Muhl, C., Mussgiller, A., Pitzl, D., Reichelt, O., Savitskyi, M., Schuetze, P., Walsh, R., Zuber, A., Biskop, H., Buhmann, P., Centis-Vignali, M., Garutti, E., Haller, J., Hoffmann, M., Lapsien, T., Matysek, M., Perieanu, A., Scharf, Ch., Schleper, P., Schmidt, A., Schw, t, J., Sonneveld, J., Steinbrueck, G., Vormwald, B., Wellhausen, J., Abbas, M., Amstutz, C., Barvich, T., Barth, Ch., Boegelspacher, F., De Boer, W., Butz, E., Caselle, M., Colombo, F., Dierlamm, A., Freund, B., Hartmann, F., Heindl, S., Husemann, U., Kornmayer, A., Kudella, S., Muller, Th., Simonis, H. J., Steck, P., Weber, M., Weiler, Th., Anagnostou, G., Asenov, P., Assiouras, P., Daskalakis, G., Kyriakis, A., Loukas, D., Paspalaki, L., Sikler, F., Veszpremi, V., Bhardwaj, A., Dalal, R., Jain, G., Ranjan, K., Bakhshiansohl, H., Behnamian, H., Khakzad, M., Naseri, M., Cariola, P., Creanza, D., De Palma, M., De Robertis, G., Fiore, L., Franco, M., Loddo, F., Silvestris, L., Maggi, G., Martiradonna, S., My, S., Selvaggi, G., Albergo, S., Cappello, G., Chiorboli, M., Costa, S., Di Mattia, A., Giordano, F., Potenza, R., Saizu, M. A., Tricomi, A., Tuve, C., Barbagli, G., Brianzi, M., Ciaranfi, R., Ciulli, V., Civinini, C., D'Aless, ro, R., Focardi, E., Latino, G., Lenzi, P., Meschini, M., Paoletti, S., Russo, L., Scarlini, E., Sguazzoni, G., Strom, D., Viliani, L., Ferro, F., Lo Vetere, M., Robutti, E., Dinardo, M. E., Fiorendi, S., Gennai, S., Malvezzi, S., Manzoni, R. A., Menasce, D., Moroni, L., Pedrini, D., Azzi, P., Bacchetta, N., Bisello, D., Dall'Osso, M., Pozzobon, N., Tosi, M., De Canio, F., Gaioni, L., Manghisoni, M., Nodari, B., Riceputi, E., Re, V., Traversi, G., Comotti, D., Ratti, L., Solestizi, L. Alunni, Biasini, M., Bilei, G. M., Cecchi, C., Checcucci, B., Ciangottini, D., Fano, L., Gentsos, C., Ionica, M., Leonardi, R., Manoni, E., Mantovani, G., Marconi, S., Marialli, V., Menichelli, M., Modak, A., Morozzi, A., Moscatelli, F., Passeri, D., Placidi, P., Postolache, V., Rossi, A., Saha, A., Santocchia, A., Storchi, L., Spiga, D., Androsov, K., Azzurri, P., Arezzini, S., Bagliesi, G., Basti, A., Boccali, T., Borrello, L., Bosi, F., Castaldi, R., Ciampa, A., Ciocci, M. A., Dell'Orso, R., Donato, S., Fedi, G., Giassi, A., Grippo, M. T., Ligabue, F., Lomtadze, T., Magazzu, G., Martini, L., Mazzoni, E., Messineo, A., Moggi, A., Morsani, F., Palla, F., Palmonari, F., Raffaelli, F., Rizzi, A., Savoy-Navarro, A., Spagnolo, P., Tenchini, R., Tonelli, G., Venturi, A., Verdini, P. G., Bellan, R., Costa, M., Covarelli, R., Rolo, M. Da Rocha, Demaria, N., Rivetti, A., Dellacasa, G., Mazza, G., Migliore, E., Monteil, E., Pacher, L., Ravera, F., Solano, A., Fern, ez, M., Gomez, G., Jaramillo Echeverria, R., Moya, D., Gonzalez Sanchez, F. J., Vila, I., Virto, A. L., Abbaneo, D., Ahmed, I., Albert, E., Auzinger, G., Berruti, G., Bianchi, G., Blanchot, G., Bonnaud, J., Caratelli, A., Ceresa, D., Christiansen, J., Cichy, K., Daguin, J., D'Auria, A., Detraz, S., Deyrail, D., Dondelewski, O., Faccio, F., Frank, N., Gadek, T., Gill, K., Honma, A., Hugo, G., Casas, L. M. Jara, Kaplon, J., Kottelat, L., Kovacs, M., Krammer, M., Lenoir, P., Mannelli, M., Marchioro, A., Mersi, S., Martina, S., Michelis, S., Moll, M., Onnela, A., Orfanelli, S., Pavis, S., Peisert, A., Pernot, J. -F., Petagna, P., Petrucciani, G., Postema, H., Rose, P., Tropea, P., Troska, J., Tsirou, A., Vasey, F., Vichoudis, P., Verlaat, B., Zwalinski, L., Bachmair, F., Becker, R., di Calafiori, D., Casal, B., Berger, P., Djambazov, L., Donega, M., Grab, C., Hits, D., Hoss, J., Kasieczka, G., Lustermann, W., Mangano, B., Marionneau, M., del Arbol, P. Martinez Ruiz, Masciovecchio, M., Meinhard, M., Perozzi, L., Roeser, U., Starodumov, A., Tavolaro, V., Wallny, R., Zhu, D., Amsler, C., Bosiger, K., Caminada, L., Canelli, F., Chiochia, V., de Cosa, A., Galloni, C., Hreus, T., Kilminster, B., Lange, C., Maier, R., Ngadiuba, J., Pinna, D., Robmann, P., Taroni, S., Yang, Y., Berth, W., Deiters, K., Erdmann, W., Horisberger, R., Kaestli, H. -C., Kotlinski, D., Langenegger, U., Meier, B., Rohe, T., Streuli, S., Chen, P. -H., Dietz, C., Grundler, U., Hou, W. -S., Lu, R. -S., Moya, M., Cussans, D., Flacher, H., Goldstein, J., Grimes, M., Jacob, J., El Nasr-Storey, S. Seif, Cole, J., Hoad, C., Hobson, P., Morton, A., Reid, I. D., Bainbridge, R., Dauncey, P., Hall, G., James, T., Magnan, A. -M., Pesaresi, M., Raymond, D. M., Uchida, K., Coughlan, J. A., Harder, K., Ilic, J., Tomalin, I. R., Garabedian, A., Heintz, U., Narain, M., Nelson, J., Sagir, S., Speer, T., Swanson, J., Tersegno, D., Watson-Daniels, J., Chertok, M., Conway, J., Conway, R., Flores, C., L, er, R., Pellett, D., Ricci-Tam, F., Squires, M., Thomson, J., Yohay, R., Burt, K., Ellison, J., Hanson, G., Olmedo, M., Si, W., Yates, B. R., Gerosa, R., Sharma, V., Vartak, A., Yagil, A., Della Porta, G. Zevi, Dutta, V., Gouskos, L., Inc, ela, J., Kyre, S., Mullin, S., Patterson, A., Qu, H., White, D., Dominguez, A., Bartek, R., Cumalat, J. P., Ford, W. T., Jensen, F., Johnson, A., Krohn, M., Leontsinis, S., Mulholl, Stenson, K., Wagner, S. R., Apresyan, A., Bo, G., Burkett, K., Butler, J. N., Canepa, A., Cheung, H. W. K., Chramowicz, J., Christian, D., Cooper, W. E., Deptuch, G., Derylo, G., Gingu, C., Grunendahl, S., Hasegawa, S., Hoff, J., Howell, J., Hrycyk, M., Jindariani, S., Johnson, M., Kahlid, F., Lei, C. M., Lipton, R., De Sa, R. Lopes, Liu, T., Los, S., Matulik, M., Merkel, P., Nahn, S., Prosser, A., Rivera, R., Schneider, B., Sellberg, G., Shenai, A., Spiegel, L., Tran, N., Uplegger, L., Voirin, E., Berry, D. R., Chen, X., Ennesser, L., Evdokimov, A., Evdokimov, O., Gerber, C. E., Hofman, D. J., Makauda, S., Mills, C., Gonzalez, I. D. S, oval, Alimena, J., Antonelli, L. J., Francis, B., Hart, A., Hill, C. S., Parashar, N., Stupak, J., Bortoletto, D., Bubna, M., Hinton, N., Jones, M., Miller, D. H., Shi, X., Tan, P., Baringer, P., Bean, A., Khalil, S., Kropivnitskaya, A., Majumder, D., Wilson, G., Ivanov, A., Mendis, R., Mitchell, T., Skhirtladze, N., Taylor, R., Anderson, I., Fehling, D., Gritsan, A., Maksimovic, P., Martin, C., Nash, K., Osherson, M., Swartz, M., Xiao, M., Acosta, J. G., Cremaldi, L. M., Oliveros, S., Perera, L., Summers, D., Bloom, K., Claes, D. R., Fangmeier, C., Suarez, R. Gonzalez, Monroy, J., Siado, J., Hahn, K., Sevova, S., Sung, K., Trovato, M., Bartz, E., Gershtein, Y., Halkiadakis, E., Kyriacou, S., Lath, A., Schnetzer, S., Stone, R., Walker, M., Malik, S., Norberg, S., Vargas, J. E. Ramirez, Alyari, M., Dolen, J., Godshalk, A., Harrington, C., Iashvili, I., Kharchilava, A., Nguyen, D., Parker, A., Rappoccio, S., Roozbahani, B., Alex, er, J., Chaves, J., Chu, J., Dittmer, S., McDermott, K., Mirman, N., Rinkevicius, A., Ryd, A., Salvati, E., Skinnari, L., Soffi, L., Tao, Z., Thom, J., Tucker, J., Zientek, M., Akgun, B., Ecklund, K. M., Kilpatrick, M., Nussbaum, T., Zabel, J., Betchart, B., Demina, R., Hindrichs, O., Petrillo, G., Eusebi, R., Osipenkov, I., Perloff, A., Ulmer, K. A., Delannoy, A. G., D'Angelo, P., Johns, W., CMS collaboration, Institut de Physique Nucléaire de Lyon (IPNL), Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), Institut Pluridisciplinaire Hubert Curien (IPHC), Université de Strasbourg (UNISTRA)-Centre National de la Recherche Scientifique (CNRS), CMS, Centre National de la Recherche Scientifique (CNRS)-Université de Strasbourg (UNISTRA), CMS collaboration, Adam, W, Bergauer, T, Brondolin, E, Dragicevic, M, Friedl, M, Fruhwirth, R, Hoch, M, Hrubec, J, Konig, A, Steininger, H, Waltenberger, W, Alderweireldt, S, Beaumont, W, Janssen, X, Lauwers, J, Mechelen, P, Remortel, N, Spilbeeck, A, Beghin, D, Brun, H, Clerbaux, B, Delannoy, H, Lentdecker, G, Fasanella, G, Favart, L, Goldouzian, R, Grebenyuk, A, Karapostoli, G, Lenzi, T, Leonard, A, Luetic, J, Postiau, N, Seva, T, Vanlaer, P, Vannerom, D, Wang, Q, Zhang, F, Zeid, S, Blekman, F, Bruyn, I, Clercq, J, D'Hondt, J, Deroover, K, Lowette, S, Moortgat, S, Moreels, L, Python, Q, Skovpen, K, Mulders, P, Parijs, I, Bakhshiansohi, H, Bondu, O, Brochet, S, Bruno, G, Caudron, A, Delaere, C, Delcourt, M, Visscher, S, Francois, B, Giammanco, A, Jafari, A, Komm, M, Krintiras, G, Lemaitre, V, Magitteri, A, Mertens, A, Michotte, D, Musich, M, Piotrzkowski, K, Quertenmont, L, Szilasi, N, Marono, M, Wertz, S, Beliy, N, Caebergs, T, Daubie, E, Hammad, G, Harkonen, J, Lampen, T, Luukka, P, Peltola, T, Tuominen, E, Tuovinen, E, Eerola, P, Tuuva, T, Baulieu, G, Boudoul, G, Caponetto, L, Combaret, C, Contardo, D, Dupasquier, T, Gallbit, G, Lumb, N, Mirabito, L, Perries, S, Donckt, M, Viret, S, Agram, J, Andrea, J, Bloch, D, Bonnin, C, Brom, J, Chabert, E, Chanon, N, Charles, L, Conte, E, Fontaine, J, Gross, L, Hosselet, J, Jansova, M, Tromson, D, Autermann, C, Feld, L, Karpinski, W, Kiesel, K, Klein, K, Lipinski, M, Ostapchuk, A, Pierschel, G, Preuten, M, Rauch, M, Schael, S, Schomakers, C, Schulz, J, Schwering, G, Wlochal, M, Zhukov, V, Pistone, C, Fluegge, G, Kuensken, A, Pooth, O, Stahl, A, Aldaya, M, Asawatangtrakuldee, C, Beernaert, K, Bertsche, D, Contreras-Campana, C, Eckerlin, G, Eckstein, D, Eichhorn, T, Gallo, E, Garcia, J, Hansen, K, Haranko, M, Harb, A, Hauk, J, Keaveney, J, Kalogeropoulos, A, Kleinwort, C, Lohmann, W, Mankel, R, Maser, H, Mittag, G, Muhl, C, Mussgiller, A, Pitzl, D, Reichelt, O, Savitskyi, M, Schuetze, P, Walsh, R, Zuber, A, Biskop, H, Buhmann, P, Centis-Vignali, M, Garutti, E, Haller, J, Hoffmann, M, Lapsien, T, Matysek, M, Perieanu, A, Scharf, C, Schleper, P, Schmidt, A, Schwandt, J, Sonneveld, J, Steinbruck, G, Vormwald, B, Wellhausen, J, Abbas, M, Amstutz, C, Barvich, T, Barth, C, Boegelspacher, F, Boer, W, Butz, E, Caselle, M, Colombo, F, Dierlamm, A, Freund, B, Hartmann, F, Heindl, S, Husemann, U, Kornmayer, A, Kudella, S, Muller, T, Simonis, H, Steck, P, Weber, M, Weiler, T, Anagnostou, G, Asenov, P, Assiouras, P, Daskalakis, G, Kyriakis, A, Loukas, D, Paspalaki, L, Sikler, F, Veszpremi, V, Bhardwaj, A, Dalal, R, Jain, G, Ranjan, K, Bakhshiansohl, H, Behnamian, H, Khakzad, M, Naseri, M, Cariola, P, Creanza, D, Palma, M, Robertis, G, Fiore, L, Franco, M, Loddo, F, Silvestris, L, Maggi, G, Martiradonna, S, My, S, Selvaggi, G, Albergo, S, Cappello, G, Chiorboli, M, Costa, S, Mattia, A, Giordano, F, Potenza, R, Saizu, M, Tricomi, A, Tuve, C, Barbagli, G, Brianzi, M, Ciaranfi, R, Ciulli, V, Civinini, C, D'Alessandro, R, Focardi, E, Latino, G, Lenzi, P, Meschini, M, Paoletti, S, Russo, L, Scarlini, E, Sguazzoni, G, Strom, D, Viliani, L, Ferro, F, Vetere, M, Robutti, E, Dinardo, M, Fiorendi, S, Gennai, S, Malvezzi, S, Manzoni, R, Menasce, D, Moroni, L, Pedrini, D, Azzi, P, Bacchetta, N, Bisello, D, Dall'Osso, M, Pozzobon, N, Tosi, M, Canio, F, Gaioni, L, Manghisoni, M, Nodari, B, Riceputi, E, Re, V, Traversi, G, Comotti, D, Ratti, L, Solestizi, L, Biasini, M, Bilei, G, Cecchi, C, Checcucci, B, Ciangottini, D, Fano, L, Gentsos, C, Ionica, M, Leonardi, R, Manoni, E, Mantovani, G, Marconi, S, Mariani, V, Menichelli, M, Modak, A, Morozzi, A, Moscatelli, F, Passeri, D, Placidi, P, Postolache, V, Rossi, A, Saha, A, Santocchia, A, Storchi, L, Spiga, D, Androsov, K, Azzurri, P, Arezzini, S, Bagliesi, G, Basti, A, Boccali, T, Borrello, L, Bosi, F, Castaldi, R, Ciampa, A, Ciocci, M, Dell'Orso, R, Donato, S, Fedi, G, Giassi, A, Grippo, M, Ligabue, F, Lomtadze, T, Magazzu, G, Martini, L, Mazzoni, E, Messineo, A, Moggi, A, Morsani, F, Palla, F, Palmonari, F, Raffaelli, F, Rizzi, A, Savoy-Navarro, A, Spagnolo, P, Tenchini, R, Tonelli, G, Venturi, A, Verdini, P, Bellan, R, Costa, M, Covarelli, R, Rolo, M, Demaria, N, Rivetti, A, Dellacasa, G, Mazza, G, Migliore, E, Monteil, E, Pacher, L, Ravera, F, Solano, A, Fernandez, M, Gomez, G, Echeverria, R, Moya, D, Sanchez, F, Vila, I, Virto, A, Abbaneo, D, Ahmed, I, Albert, E, Auzinger, G, Berruti, G, Bianchi, G, 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T., Ligabue, F., Lomtadze, T., Magazzu, G., Martini, L., Mazzoni, E., Messineo, A., Moggi, A., Morsani, F., Palla, F., Palmonari, F., Raffaelli, F., Rizzi, A., Savoy-Navarro, A., Spagnolo, P., Tenchini, R., Tonelli, G., Venturi, A., Verdini, P. G., Bellan, R., Costa, M., Covarelli, R., Rolo, M. Da Rocha, Demaria, N., Rivetti, A., Dellacasa, G., Mazza, G., Migliore, E., Monteil, E., Pacher, L., Ravera, F., Solano, A., Fern, Ez, M., Gomez, G., Jaramillo Echeverria, R., Moya, D., Gonzalez Sanchez, F. J., Vila, I., Virto, A. L., Abbaneo, D., Ahmed, I., Albert, E., Auzinger, G., Berruti, G., Bianchi, G., Blanchot, G., Bonnaud, J., Caratelli, A., Ceresa, D., Christiansen, J., Cichy, K., Daguin, J., D'Auria, A., Detraz, S., Deyrail, D., Dondelewski, O., Faccio, F., Frank, N., Gadek, T., Gill, K., Honma, A., Hugo, G., Casas, L. M. 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R., Garabedian, A., Heintz, U., Narain, M., Nelson, J., Sagir, S., Speer, T., Swanson, J., Tersegno, D., Watson-Daniels, J., Chertok, M., Conway, J., Conway, R., Flores, C., L, Er, R., Pellett, D., Ricci-Tam, F., Squires, M., Thomson, J., Yohay, R., Burt, K., Ellison, J., Hanson, G., Olmedo, M., Si, W., Yates, B. R., Gerosa, R., Sharma, V., Vartak, A., Yagil, A., Della Porta, G. Zevi, Dutta, V., Gouskos, L., Inc, Ela, J., Kyre, S., Mullin, S., Patterson, A., Qu, H., White, D., Dominguez, A., Bartek, R., Cumalat, J. P., Ford, W. T., Jensen, F., Johnson, A., Krohn, M., Leontsinis, S., Mulholl, Stenson, K., Wagner, S. R., Apresyan, A., Bo, G., Burkett, K., Butler, J. N., Canepa, A., Cheung, H. W. K., Chramowicz, J., Christian, D., Cooper, W. E., Deptuch, G., Derylo, G., Gingu, C., Grunendahl, S., Hasegawa, S., Hoff, J., Howell, J., Hrycyk, M., Jindariani, S., Johnson, M., Kahlid, F., Lei, C. M., Lipton, R., De Sa, R. Lope, Liu, T., Los, S., Matulik, M., Merkel, P., Nahn, S., Prosser, A., Rivera, R., Schneider, B., Sellberg, G., Shenai, A., Spiegel, L., Tran, N., Uplegger, L., Voirin, E., Berry, D. R., Chen, X., Ennesser, L., Evdokimov, A., Evdokimov, O., Gerber, C. E., Hofman, D. J., Makauda, S., Mills, C., Gonzalez, I. D. S, Oval, Alimena, J., Antonelli, L. J., Francis, B., Hart, A., Hill, C. S., Parashar, N., Stupak, J., Bortoletto, D., Bubna, M., Hinton, N., Jones, M., Miller, D. H., Shi, X., Tan, P., Baringer, P., Bean, A., Khalil, S., Kropivnitskaya, A., Majumder, D., Wilson, G., Ivanov, A., Mendis, R., Mitchell, T., Skhirtladze, N., Taylor, R., Anderson, I., Fehling, D., Gritsan, A., Maksimovic, P., Martin, C., Nash, K., Osherson, M., Swartz, M., Xiao, M., Acosta, J. G., Cremaldi, L. M., Oliveros, S., Perera, L., Summers, D., Bloom, K., Claes, D. R., Fangmeier, C., Suarez, R. Gonzalez, Monroy, J., Siado, J., Hahn, K., Sevova, S., Sung, K., Trovato, M., Bartz, E., Gershtein, Y., Halkiadakis, E., Kyriacou, S., Lath, A., Schnetzer, S., Stone, R., Walker, M., Malik, S., Norberg, S., Vargas, J. E. Ramirez, Alyari, M., Dolen, J., Godshalk, A., Harrington, C., Iashvili, I., Kharchilava, A., Nguyen, D., Parker, A., Rappoccio, S., Roozbahani, B., Alex, Er, J., Chaves, J., Chu, J., Dittmer, S., Mcdermott, K., Mirman, N., Rinkevicius, A., Ryd, A., Salvati, E., Skinnari, L., Soffi, L., Tao, Z., Thom, J., Tucker, J., Zientek, M., Akgun, B., Ecklund, K. M., Kilpatrick, M., Nussbaum, T., Zabel, J., Betchart, B., Demina, R., Hindrichs, O., Petrillo, G., Eusebi, R., Osipenkov, I., Perloff, A., Ulmer, K. A., Delannoy, A. G., D'Angelo, P., Johns, W., Cms, Collaboration, Elementary Particle Physics, Physics, Faculty of Sciences and Bioengineering Sciences, Université de Strasbourg (UNISTRA)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), Helsinki Institute of Physics, Department of Physics, and UCL - SST/IRMP - Institut de recherche en mathématique et physique
Subjects: Detector modelling and simulations II (electric fields, Physics::Instrumentation and Detectors, UPGRADE, electron emission etc), Detector modelling and simulations II (electric fields, charge transport, multiplication and induction, pulse formation, electron emission, etc), Particle tracking detectors (Solid-state detectors), Radiation-hard detectors, Instrumentation, Mathematical Physics, Tracking (particle physics), Settore ING-INF/01 - Elettronica, 01 natural sciences, damage [radiation], design [semiconductor detector], Radiation-hard, detectors, charge transport, multiplication and induction, pulse formation, DETECTORS, TIME, tracking detector, Detectors and Experimental Techniques, Radiation hardening, radiation: damage, Physics, Large Hadron Collider, irradiation, CMS, Detector, Electrical engineering, microstrip [semiconductor detector], electron emission), Upgrade, Physique des particules élémentaires, semiconductor detector: microstrip, pulse formation, Silicon, education, chemistry.chemical_element, Detector modelling and simulations II, 114 Physical sciences, Particle detector, 0103 physical sciences, ddc:530, ddc:610, [PHYS.PHYS.PHYS-INS-DET]Physics [physics]/Physics [physics]/Instrumentation and Detectors [physics.ins-det], 010306 general physics, etc), multiplication and induction, hep-ex, 010308 nuclear & particles physics, business.industry, Detector modelling and simulations II (electric fields, charge transport, multiplication and induction, pulse formation, electron emission), charge transport, chemistry, electron emission, Measuring instrument, business, semiconductor detector: design
Abstract: The upgrade of the LHC to the High-Luminosity LHC (HL-LHC) is expected to increase the LHC design luminosity by an order of magnitude. This will require silicon tracking detectors with a significantly higher radiation hardness. The CMS Tracker Collaboration has conducted an irradiation and measurement campaign to identify suitable silicon sensor materials and strip designs for the future outer tracker at the CMS experiment. Based on these results, the collaboration has chosen to use n-in-p type silicon sensors and focus further investigations on the optimization of that sensor type. This paper describes the main measurement results and conclusions that motivated this decision. © 2017 CERN for the benefit of the CMS collaboration., 0, info:eu-repo/semantics/published
Published: 2017

38. Porous Dipeptide Crystals as Polymerization Nanoreactors

Author: Piero Sozzani, Angiolina Comotti, Gaetano Distefano, Silvia Bracco, M Beretta, Distefano, G, Comotti, A, Bracco, S, Beretta, M, and Sozzani, P
Subjects: Polymers, Acrylic Resins, Nanoreactor, CHIM/04 - CHIMICA INDUSTRIALE, Crystal engineering, Catalysis, topochemistry, microporous material, chemistry.chemical_compound, Isomerism, Polymer chemistry, Nanotechnology, Porosity, Dipeptide, Dipeptides, General Medicine, General Chemistry, peptide, CHIM/02 - CHIMICA FISICA, chemistry, Chemical engineering, Polymerization, Gamma Rays, crystal engineering, polymerization, Crystallization
Abstract: Dipeptide crystals have been used for solid-state polymerization reactions. The porosity of the crystals enables monomer absorption, followed by γ-irradiation to produce polymers with high molecular weights. The crystal channels induce stereoselective reactions to yield 1,4-trans polydienes and isotactic poly(acrylonitrile) with retention of fibrillar morphology
Published: 2012

39. Structural Characterization of Pristine and Modified Fluoromica Using Multinuclear Solid-State NMR

Author: Piero Sozzani, Maurizio Galimberti, Silvia Bracco, Alice Silvia Cattaneo, Hellmut Eckert, Angiolina Comotti, Cattaneo, A, Bracco, S, Comotti, A, Galimberti, M, Sozzani, P, and Eckert, H
Subjects: 19f nmr spectroscopy, Magnesium, Sodium, Analytical chemistry, chemistry.chemical_element, CHIM/04 - CHIMICA INDUSTRIALE, Surfaces, Coatings and Films, Electronic, Optical and Magnetic Materials, Ion, CHIM/02 - CHIMICA FISICA, chemistry.chemical_compound, Crystallography, General Energy, Octahedron, chemistry, Solid-state nuclear magnetic resonance, Lattice (order), phyllosilicate, fluromica, Solid State NMR, XRD, Physical and Theoretical Chemistry, Fluoride
Abstract: The structure of a synthetic fluoromica has been investigated and elucidated by complementary 29Si, 1H, 19F, 23Na, and 27Al single and double resonance experiments. The phyllosilicate possesses a charge heterogeneity arising from the presence of different charged sites in the octahedral sheets of the T-O-T layers. Part of the magnesium atoms in the octahedral sheets is missing, creating vacancies. Charge balancing proceeds mostly by incorporation of sodium ions into the interlayer space and substitution of Mg by sodium in the lattice. The latter process produces a nonexchangeable fraction of sodium ions (∼20% of the total inventory) and creates multiple sites for the fluoride ions, as evidenced from 19F NMR spectroscopy. Detailed quantitative information about the sodium-fluoride distance geometries were obtained from 19F/ 23Na double rotational echo double resonance (REDOR) experiments; furthermore, different types of fluoride sites could be discriminated on the basis of 19F/23Na double resonance experiments. The chemical reactivity of this system was modified by ball milling, cation exchange with octadecylammonium ions, and grafting with an organosilane (γ-aminopropyltriethoxysilane), and the corresponding structural consequences were probed by multinuclear single and double resonance NMR techniques. © 2011 American Chemical Society.
Published: 2011

40. Controlled Orientation of Polyconjugated Guest Molecules in Tunable Host Cavities

Author: Angiolina Comotti, Airon C. Soegiarto, Michael D. Ward, Soegiarto, A, Comotti, A, and Ward, M
Subjects: Long axis, Chemistry, Bilayer, Nanotechnology, General Chemistry, Crystal structure, Conjugated system, Biochemistry, Catalysis, Orientation (vector space), CHIM/02 - CHIMICA FISICA, Crystallography, Colloid and Surface Chemistry, Inclusion compounds, Molecular orientation, Microstructure, Molecule, Lamellar structure, Absorption (chemistry)
Abstract: Linear conjugated guest molecules with high aspect ratios form inclusion compounds with guanidinium organodisulfonate (GDS) host frameworks in which organodisulfonate "pillars" connect opposing GS sheets to generate lamellar architectures that reflect templating by the guest. Through judicious selection of pillars having adjustable lengths (l(S-S), as measured by the separation between distal sulfur atoms) and guests of various lengths (l(g)), the framework architecture can be controlled systematically in a manner that enables regulation of the guest orientation and aggregation in the host framework. Inclusion compounds for which l(g)/l(S-S) ≤ 0.9 exhibit a bilayer architecture with 1-D channels containing guests oriented parallel to the long axis of the pillar. Guests with values of l(g) comparable to l(S-S), however, promote the formation of a brick architecture in which the guests and the pillar are arranged in a herringbone motif. Surprisingly, longer guests (l(g) = 1.25l(S-S)) favor the formation of the bilayer architecture despite their larger volume because the guests are forced to align end-to-end as single-file arrays due to the vertical constraints of the 1-D channels. Bithiophene and biphenyl guests (l(g)l(S-S)) are exceptional, promoting bilayer structures in which turnstile rotations of the pillars afford an unusual motif in which the guests are isolated from one another. The ability to synthesize a large family of compounds based on a common supramolecular building block (the GS sheet) permits construction of a structural "phase diagram" based on two simple molecular parameters, l(g) and l(S-S), that can be used to sort the inclusion compounds according to their framework architectures and enable prediction of crystal structures for new host-guest combinations. The effects of these different framework architectures and packing motifs is manifested as bathochromic shifts in the absorption and emission spectra of the guests compared with their spectra in methanol solutions. This behavior is supported by ab initio TDDFT calculations that reproduce the bathochromic shifts associated with the effects of guest-guest and guest-host interactions, combined with conformational constraints imposed on the guest molecules by the rigid host framework.
Published: 2010

41. Frontispiece: Ultrafast Molecular Rotors and Their CO2 Tuning in MOFs with Rod-Like Ligands

Author: Simona Galli, Angiolina Comotti, Silvia Bracco, Piero Sozzani, M Negroni, Angelo Maspero, and F Castiglioni
Subjects: Chemistry, Organic Chemistry, Supramolecular chemistry, Nanotechnology, General Chemistry, Molecular rotors, Porous medium, Ultrashort pulse, Catalysis
Published: 2017

42. 2D Multinuclear NMR, Hyperpolarized Xenon and Gas Storage in Organosilica Nanochannels with Crystalline Order in the Walls

Author: Lisa Ferretti, Silvia Bracco, Angiolina Comotti, Patrizia Valsesia, Piero Sozzani, Comotti, A, Bracco, S, Valsesia, P, Ferretti, L, and Sozzani, P
Subjects: Diffraction, Chemistry, Analytical chemistry, General Chemistry, CHIM/04 - CHIMICA INDUSTRIALE, Biochemistry, Catalysis, Synchrotron, Homonuclear molecule, law.invention, CHIM/02 - CHIMICA FISICA, Colloid and Surface Chemistry, Adsorption, Mesoporous materials, Microstructure, Porosity, Solid State NMR, Hyperpolarized Xe NMR, Absorption properties, Structure of periodic mesoporous material, hybrid phenylenesilica cryst order, Solid-state nuclear magnetic resonance, Heteronuclear molecule, law, Chemical physics, Molecule, Mesoporous material
Abstract: The combination of 2D 1H-13C and 1H-29Si solid state NMR, hyperpolarized 129Xe NMR, synchrotron X-ray diffraction, together with adsorption measurements of vapors and gases for environmental and energetic relevance, was used to investigate the structure and the properties of periodic mesoporous hybrid p-phenylenesilica endowed with crystalline order in the walls. The interplay of 1H, 13C, and 29Si in the 2D heteronuclear correlation NMR measurements, together with the application of Lee-Goldburg homonuclear decoupling, revealed the spatial relationships (5 angstroms) among various spin-active nuclei of the framework. Indeed, the through-space correlations in the 2D experiments evidenced, for the first time, the interfaces of the matrix walls with guest molecules confined in the nanochannels. Organic-inorganic and organic-organic heterogeneous interfaces between the matrix and the guests were identified. The open-pore structure and the easy accessibility of the nanochannels to the gas phase have been demonstrated by highly sensitive hyperpolarized (HP) xenon NMR, under extreme xenon dilution. Two-dimensional exchange experiments showed the exchange time to be as short as 2 ms. Through variable-temperature HP 129Xe NMR experiments we were able to achieve an unprecedented description of the nanochannel space and surface, a physisorption energy of 13.9 kJ mol-1, and the chemical shift value of xenon probing the internal surfaces. These results prompted us to measure the high storage capacity of the matrix towards benzene, hexafluorobenzene, ethanol, and carbon dioxide. Both host-guest, CH...pi, and OH...pi interactions contribute to the stabilization of the aromatic guests (benzene and hexafluorobenzene) on the extended surfaces. The full carbon dioxide loading in the channels could be detected by synchrotron radiation X-ray diffraction experiments. The selective adsorption of carbon dioxide (ca. 90 wt %) vs that of oxygen and hydrogen, together with the permanent porosity, high thermal stability, and high degree of order, makes this a suitable matrix for purifying hydrogen in clean-energy generation.
Published: 2007

43. Confined Polymerization in Highly Ordered Mesoporous Organosilicas

Author: Silvia Bracco, Angiolina Comotti, J Perego, Mauro Gemmi, M Beretta, Piero Sozzani, Comotti, A, Bracco, S, Beretta, M, Perego, J, Gemmi, M, and Sozzani, P
Subjects: chemistry.chemical_classification, Nanostructure, Nanocomposite, nanostructure, Carbon nanofiber, Organic Chemistry, Nanotechnology, General Chemistry, Polymer, CHIM/04 - CHIMICA INDUSTRIALE, Catalysis, CHIM/02 - CHIMICA FISICA, Mesoporous organosilica, chemistry.chemical_compound, NMR spectroscopy, ladder polymer, Polymerization, chemistry, Acrylonitrile, Porous medium, confined polymerization, mesoporous organosilica
Abstract: Hybrid mesoporous organosilica exhibiting crystal-like order in the walls provided an ideal channel reaction vessel for the confined polymerization of acrylonitrile (PAN). The resulting high-molecular-mass PAN fills the channels at high yield and forms an ordered nanostructure of polymer nanobundles enclosed into the hybrid matrix. The in situ thermal transformation of PAN into rigid polyconjugated and, eventually, into condensed polyaromatic carbon nanofibers, retains the periodic architecture. Simultaneously, the matrix evolves showing the fusion of the p-phenylene rings and the cleavage of carbon-silicon bonds: this gives rise to graphitic-carbon/silica nanocomposites containing hyper-oxydrylated silica nanophases. Interestingly, the 3D hexagonal mesostructure survives in the carbonaceous material. The exploitation of porous materials of high capacity and a hybrid nature, for polymerization in the confined state, followed by high temperature treatments, allowed us to achieve unique and precisely fabricated nanostructures, thus paving the way for the construction of fine-tuned electronic and light-harvesting materials.
Published: 2015

44. Confinement of single polysilane chains in coordination nanospaces

Author: Masanobu Naito, Silvia Bracco, Piero Sozzani, Takashi Kitao, Susumu Kitagawa, Angiolina Comotti, Takashi Uemura, Shu Seki, Kitao, T, Bracco, S, Comotti, A, Sozzani, P, Naito, M, Seki, S, Uemura, T, and Kitagawa, S
Subjects: Conductive polymer, Electron mobility, metal−organic frameworks, conducting polymer, polysilane, confinement of polymer chains, solid state NMR, Porous Coordination Polymers, General Chemistry, CHIM/04 - CHIMICA INDUSTRIALE, Biochemistry, Catalysis, Molecular dynamics, chemistry.chemical_compound, symbols.namesake, Colloid and Surface Chemistry, chemistry, Chemical physics, Polymer chemistry, symbols, Polysilane, Raman spectroscopy
Abstract: Understanding the intrinsic properties of single conducting polymer chains is of interest, largely for their applications in molecular devices. In this study, we report the accommodation of single polysilane chains with hole-transporting ability in porous coordination polymers (PCPs), [Al(OH)(L)]n (1a; L = 2,6-naphthalenedicarboxylate, channel size = 8.5 × 8.5 Å(2), 1b; L = 4,4'-biphenyldicarboxylate, channel size = 11.1 × 11.1 Å(2)). Interestingly, the isolation of single polysilane chains increased the values of carrier mobility in comparison with that in the bulk state due to the elimination of the slow interchain hole hopping. Moreover, even when the chains are isolated one another, the main chain conformation of polysilane could be controlled by changing the pore environment of PCPs, as evidenced by Raman spectroscopy, solid-state NMR measurements, and molecular dynamics simulation. Hence, we succeeded in varying the conducting property of single polysilane chains. Additionally, polysilanes have a drawback, photodegradation under ultraviolet light, which should be overcome for the application of polysilanes. It is noteworthy that the accommodation of polysilane in the nanopores did not exhibit photodegradation. These results highlight that PCP-polysilane hybrids are promising candidates for further use in the field of molecular electronics.
Published: 2015

45. Early markers of Fabry disease revealed by proteomics

Author: Amerigo Beneduci, Pietro Anastasio, O. Petrazzuolo, Angela Bachi, S. Feriozzi, Giovambattista Capasso, C. Comotti, Renzo Mignani, Manuela Cuccurullo, Vittoria Matafora, Antonio Pisani, A. Simeone, Matafora, V, Cuccurullo, M, Beneduci, A, Petrazzuolo, O, Simeone, A, Anastasio, P, Mignani, R, Feriozzi, S, Pisani, Antonio, Comotti, C, Bachi, A, Capasso, G., Anastasio, Pietro, Pisani, A, and Capasso, Giovambattista
Subjects: Adult, Male, Proteomics, medicine.medical_specialty, Tamm–Horsfall protein, Adolescent, Urinary system, proteome, Globotriaosylceramide, Inflammation, Biology, chemistry.chemical_compound, Young Adult, Tamm Horsfall glycoprotein, Internal medicine, Uromodulin, medicine, Cluster Analysis, Humans, Child, Molecular Biology, Aged, Prosaposin, Kidney, Reproducibility of Results, Enzyme replacement therapy, Middle Aged, medicine.disease, biological marker, Fabry disease, medicine.anatomical_structure, Endocrinology, Early Diagnosis, chemistry, Immunology, biology.protein, Fabry Disease, Female, medicine.symptom, Biomarkers, Biotechnology
Abstract: Fabry disease (FD) is an X-linked lysosomal storage disorder caused by a deficiency of the lysosomal hydrolase α-galactosidase A (α-GalA) that leads to the intra-lysosomal accumulation of globotriaosylceramide (Gb3) in various organ systems. As a consequence, a multisystems disorder develops, culminating in stroke, progressive renal and cardiac dysfunction. Enzyme replacement therapy (ERT) offers a specific treatment for patients affected by FD, though the monitoring of treatment is hindered by a lack of surrogate markers of response. Remarkably, due to the high heterogeneity of the Fabry phenotype, both diagnostic testing and treatment decisions are more challenging in females than in males; thus, reliable biomarkers for Fabry disease are needed, particularly for female patients. Here, we use a proteomic approach for the identification of disease-associated markers that can be used for the early diagnosis of FD as well as for monitoring the effectiveness of ERT. Our data show that the urinary proteome of Fabry naïve patients is different from that of normal subjects. In addition, biological pathways mainly affected by FD are related to immune response, inflammation, and energetic metabolism. In particular, the up-regulation of uromodulin, prostaglandin H2 d-isomerase and prosaposin in the urine of FD patients was demonstrated; these proteins might be involved in kidney damage at the tubular level, inflammation and immune response. Furthermore, comparing the expression of these proteins in Fabry patients before and after ERT treatment, a decrease of their concentration was observed, thus demonstrating the correlation between the identified markers and the effectiveness of the pharmacological treatment. © The Royal Society of Chemistry.
Published: 2015

46. Dipolar rotors orderly aligned in mesoporous fluorinated organosilica architectures

Author: Piero Sozzani, Silvia Bracco, Ke Zhao, Charles T. Rogers, Alice Cattaneo, Angiolina Comotti, Andrea Falqui, M Beretta, Bracco, S, Beretta, M, Cattaneo, A, Comotti, A, Falqui, A, Zhao, K, Rogers, C, and Sozzani, P
Subjects: chemistry.chemical_classification, Dielectric spectroscopy, Double bond, Chemistry, Molecular rotor, Chemistry (all), Nanotechnology, General Chemistry, Dielectric, General Medicine, CHIM/04 - CHIMICA INDUSTRIALE, Catalysis, Catalysi, Dipole, CHIM/02 - CHIMICA FISICA, NMR spectroscopy, Chemical physics, Covalent bond, Porous material, Molecule, Mesoporous material, Hybrid material
Abstract: New mesoporous covalent frameworks, based on hybrid fluorinated organosilicas, were prepared to realize a periodic architecture of fast molecular rotors containing dynamic dipoles in their structure. The mobile elements, designed on the basis of fluorinated p-divinylbenzene moieties, were integrated into the robust covalent structure through siloxane bonds, and showed not only the rapid dynamics of the aromatic rings (ca. 10(8) Hz at 325 K), as detected by solid-state NMR spectroscopy, but also a dielectric response typical of a fast dipole reorientation under the stimuli of an applied electric field. Furthermore, the mesochannels are open and accessible to diffusing in gas molecules, and rotor mobility could be individually regulated by I2 vapors. The iodine enters the channels of the periodic structure and reacts with the pivotal double bonds of the divinyl-fluoro-phenylene rotors, affecting their motion and the dielectric properties.
Published: 2015

47. Impact of low-dose electron irradiation on n+p silicon strip sensors

Author: S. Michelis, Joshua Thompson, A. Kuensken, Gaelle Boudoul, Alexis Kalogeropoulos, Ivan Vila, Adrian Perieanu, S. Mättig, N. Van Remortel, Kevin Stenson, P. Verdier, C. Barth, Achim Stahl, Malte Hoffmann, Carlo Civinini, M. Olmedo, Jean-Marie Brom, T. Nussbaum, Wolfgang Lange, Duncan Leggat, Panja-Riina Luukka, Caleb Fangmeier, Roberto Ciaranfi, Alex Garabedian, R. Gonzalez Suarez, Richard Lander, J. Nelson, Gregor Mittag, Jennifer Chu, T. du Pree, J. Gray, Liliana Teodorescu, Marko Dragicevic, Willard Johns, Po-Hsun Chen, Stefano Mersi, Ievgen Korol, M. Lo Vetere, Simone Gennai, Umesh Joshi, Simon Spannagel, K. Bösiger, Laurent Mirabito, Steven Lowette, H. Maser, GN Kaufman, Rachel Yohay, T. Pakulski, M. Kovacs, T. Barvich, James Alexander, Doris Eckstein, J. Watson-Daniels, Gaia Maria Berruti, Stefano Casasso, G. Schwering, A. K. Honma, Salvatore Rappoccio, Loukas Gouskos, Stephen Robert Wagner, Ferdinando Giordano, Jordan Tucker, Th. Müller, Matthieu Marionneau, Arne-Rasmus Draeger, Alexander Dierlamm, P. Van Mulders, M. Printz, Stefan Michael Heindl, Xavier Janssen, M. Salvatore, L. M. Cremaldi, Michele Selvaggi, Clemens Lange, Mia Tosi, Satoshi Hasegawa, R. Stringer, Mark Grimes, S. Mallows, B. Baldin, Ping Tan, Mark Pesaresi, H. Yin, J. Swanson, Urs Langenegger, Martino Dall'Osso, Hallie Trauger, P. Steck, A. Prosser, John Gabriel Acosta, A. Tropiano, R. Wilken, Tommaso Dorigo, Sandra Malvezzi, P. Tropea, Alberto Zucchetta, Gregor Kasieczka, Marco Meschini, Andrei Starodumov, B. Nodari, Roberto Castello, C. Vander Velde, David Mark Raymond, Christophe Delaere, Lodovico Ratti, Jose Monroy, David Fehling, Ian R Tomalin, Gino Bolla, Marco Costa, M. De Palma, Attilio Santocchia, Jeson Jacob, Tuure Tuuva, J. Chramowicz, Ryan Rivera, M. Hrycyk, F. Kahlid, Andrew Ivanov, Daniela Bortoletto, L. Kottelat, L. Perera, Xin Shi, Piero Giubilato, S. Pavis, Stephen Sanders, Daniel Bloch, Avraham Yagil, Peter R Hobson, M. Hoch, Angelo Rivetti, P. Martinez Ruiz del Arbol, Tobias Lapsien, Ch Henkel, Oliver Pooth, David Sabes, Anders Ryd, G. De Lentdecker, D. C. Christian, Daniel Pitzl, A. Kumar, Vivek Sharma, Adrien Caudron, Giuseppe Benedetto Cerati, Gianluca Petrillo, F. Loddo, E. Salvati, Johannes Haller, T. Weiler, Giorgio Maggi, P. Vichoudis, Janna Katharina Behr, Frank Raupach, Philip Harris, I. De Bruyn, Michael Krohn, Ulysses Grundler, E. Conti, H. Postema, Charles Dietz, M. Schroeder, Renato Potenza, Guenter Eckerlin, Annik Olbrechts, Paula Eerola, G. Beaulieu, F.J. Gonzalez Sanchez, Daniele Pedrini, Hadi Behnamian, J. Thomson, Susan Dittmer, Gigi Cappello, Ivan Reid, Anastasia Grebenyuk, Ijaz Ahmed, Dmitry Hits, L. Charles, Ernesto Migliore, Hans-Jürgen Simonis, Andreas Mussgiller, Ali Harb, Felix Bachmair, D. I. Sandoval Gonzalez, Hanno Perrey, Konrad Deiters, Teppo Mäenpää, Didar Dobur, Fabio Ravera, N. Frank, M. Miñano Moya, G. Fluegge, G. Blanchot, Alessandra Romero, W. De Boer, Karl Gill, Jean-Laurent Agram, Daniele Comotti, J. Ellison, Rylan Conway, Nathan Mirman, Massimiliano Chiorboli, A. Nuernberg, Eva Halkiadakis, S. Los, Elisabetta Gallo, G. Sala, Luigi Moroni, U. Roeser, Waclaw Karpinski, Mauro Menichelli, Valerio Re, Luca Perniè, Roland Horisberger, Kevin Nash, Valentina Dutta, G. De Robertis, Olga Evdokimov, Wolfgang Lohmann, Lieselotte Moreels, Ashutosh Bhardwaj, Riccardo Bellan, Ian Anderson, Tomislav Seva, Livio Fanò, Petra Merkel, Markus Friedl, Jorge Chaves, Robert Stone, Frank Meier, Leonard Spiegel, S. Streuli, W. Treberspurg, E. Voirin, Roberto Covarelli, Armin Burgmeier, Amitabh Lath, P.P. Trapani, J. Hosselet, J. Garay Garcia, David Miller, Robert Klanner, Marcos Fernandez, S. Martina, Kevin Burkett, Aaron Dominguez, Abdollah Mohammadi, Kristian Allan Hahn, Natale Demaria, R. Jaramillo Echeverria, Marc Weber, F. Boegelspacher, Marco Rossini, C. Goetzmann, G. Fluke, Patrizia Azzi, Georg Steinbrück, Johannes Hauk, Boris Mangano, Yang Yang, D. Tersegno, Jonathan Hollar, Georg Auzinger, Ganna Dolinska, A. Marchioro, Anirban Saha, Matthew Jones, Esa Tuovinen, Suzan Basegmez, Hans-Christian Kaestli, Francois Vasey, Michael Wlochal, David Jonathan Hofman, Nazar Bartosik, E. Scarlini, S. Detraz, Christoph Grab, C. Muhl, Lutz Feld, Peter Robmann, Bruno Casal, D. White, D. Ceresa, Henning Flacher, M. Rzonca, Ulrich Heintz, Paolo Petagna, G. Pierschel, Claude Nuttens, M. Richer, J.-Ch. Fontaine, Barbara Clerbaux, Sara Alderweireldt, Joachim Erfle, Bora Akgun, Marvin Johnson, S. Marconi, Wolfgang Waltenberger, D. M. Strom, Daniele Passeri, Wolfram Erdmann, Daniel Noonan, A. Peisert, A. Evdokimov, Louise Skinnari, Silvia Taroni, Eckhart Fretwurst, Pavel Jez, Stephane Perries, A. Kornmeyer, Cristina Tuve, I. Van Parijs, Frank Hartmann, M. Casele, Luca Pacher, Valentina Gori, Petar Maksimovic, Piergiulio Lenzi, Rainer Wallny, A. D'Auria, M. Vander Donckt, Geoffrey Hall, M. Matysek, G. P. Van Onsem, A. L. Virto, F. De Canio, R. Eber, Martina Malberti, Pascal Vanlaer, Benedikt Freund, Douglas Berry, N. Hinton, Benedikt Vormwald, W-S Hou, L. Bissi, Devdatta Majumder, Donato Creanza, Riccardo Andrea Manzoni, J. Howell, Andrés G Delannoy, J. Christiansen, Erik Butz, J. N. Butler, Vincenzo Chiochia, Joel Goldstein, Lea Caminada, Rong-Shyang Lu, Sandro Gonzi, Karl Matthew Ecklund, Vitaliano Ciulli, Benjamin Kilminster, Matthias Geisler, Enrico Robutti, E. Bartz, Daniel Duggan, Loic Quertenmont, Maral Alyari, S. Abu Zeid, Paolo Lariccia, J. Ilic, Philip Baringer, Aidan Randle-Conde, R. Fruehwirth, David Cussans, C. Mathieu, Timo Peltola, Luigi Calligaris, Tiehui Liu, Christopher Martin, James Zabel, Didier Contardo, P. Cariola, K. Cichy, H. Biskop, Josef Hrubec, Thomas Poehlsen, J. Hoff, A. Onnela, Jorgen D'Hondt, D. Magalotti, John Perry Cumalat, John A Coughlan, D. Felici, N. Lumb, Sten Luyckx, Raffaello D'Alessandro, S. Seif El Nasr-storey, Harry Cheung, Peter Schleper, Mauro Donegà, Salvatore My, Keith Ulmer, Marc Osherson, Florian Zenoni, J. Conway, G. Derylo, W. E. Cooper, Aruna Nayak, Nikoloz Skhirtladze, M. Lei, Paul Dauncey, Valery Zhukov, W. Beaumont, A. Van Spilbeeck, Giuseppe Barbagli, James Keaveney, Gervasio Gomez, Quentin Python, Joe Incandela, A. Shenai, Nickolas Mccoll, Kirika Uchida, M. Park, D. Michotte, E. Albert, Otto Hindrichs, Lukas Bäni, Mikhail Makouski, Laurent Forthomme, Daniel R Claes, Adish Vartak, L. Servoli, M. Bubna, Ron Lipton, B. Checcucci, Burton Betchart, H. Mendez, Andreas Werner Jung, J. E. Ramirez Vargas, F. J. Munoz Sanchez, James Dolen, C. Bonnin, Andrea Giammanco, Kristian Harder, Christine O'Brien, Chad Flores, Stefaan Tavernier, Diego Ciangottini, Andrii Gizhko, Mario Masciovecchio, Mohsen Naseri, Dario Bisello, Nicola Pozzobon, R. Becker, Horst Breuker, Philipp Eller, Werner Lustermann, Andromachi Tsirou, Sergej Schuwalow, Maiko Takahashi, H. Mathez, Sara Fiorendi, Claudia Seitz, Freya Blekman, Sergo Jindariani, J. Schwandt, Josh Kaisen, Simone Paoletti, D. J. Summers, Giacomo Bruno, Tomas Hreus, Dario Menasce, J. Wellhausen, Duccio Abbaneo, Claudia Pistone, Wolfgang Adam, U. Horisberger, Ettore Focardi, H. Bakhshiansohl, Kirill Skovpen, Marcello Mannelli, Gabriele Benelli, Jeremy Andrea, Patrizia Barria, Marco Musich, M. A. Saizu, D. di Calafiori, G. Zevi Della Porta, Anne-Marie Magnan, Andreas Kornmayer, T. Lenzi, Steve Schnetzer, Eric Conte, Mark Raymond Adams, Ulrich Husemann, S. Kyre, Valentina Sola, Jan Troska, F. Squires, Y. Zoccarato, Robert Bainbridge, Karsten T. Hansen, A. Zuber, Meng Xiao, Cécile Caillol, Marc Dünser, Aniello Spiezia, Jennifer Ngadiuba, Luigi Gaioni, Michael Moll, J. Sammet, Alexandre Léonard, Nicola Bacchetta, M. Matulik, Jonathan Fulcher, Gianluca Traversi, Ennio Monteil, Natalie Heracleous, Rainer Mankel, B. De Callatay, Eric Christian Chabert, J. Kaplon, E. Daubie, B. Verlaat, Davide Pagano, Gregory Habib Hammad, Stefan Schael, J. F. Pernot, Sudhir Malik, Ia Iashvili, Luca Perrozzi, Manfred Krammer, Beat H. Meier, Kevin Sung, Federico Faccio, Andrei Gritsan, Kirti Ranjan, Fabio Colombo, T. Speer, L. Gross, G. Gallbit, Marco Trovato, C. Gingu, A. De Cosa, Matti J Kortelainen, Tilman Rohe, Jing Wang, Avto Kharchilava, Tapio Lampén, L. Djambazov, S. Sevova, M. Franco, Sébastien Viret, Eleni Ntomari, Lorenzo Uplegger, Jan Hoss, William T. Ford, R. Maier, Christian Autermann, Melody A. Swartz, Maxwell Chertok, Danek Kotlinski, Kira Burt, Mauro Emanuele Dinardo, M. Centis-Vignali, Nhan Viet Tran, Domenico Giordano, D. Moya, Lukasz Zwalinski, Kenneth Bloom, Meenakshi Narain, C. Scharf, A. Di Mattia, Thomas Eichhorn, D. Deyrail, Willi Bertl, Massimo Manghisoni, J. Daguin, P. Van Mechelen, Laurent Thomas, Katja Klein, F. Canelli, Jimin George, Karl Heinz Hoffmann, Gordon H. Hanson, Claude Amsler, H. Esser, Ilya Osipenkov, Laurent Favart, Joanne Cole, Eija Tuominen, Luigi Fiore, Lucia Perrini, Andrey Ostapchuk, Nikita Beliy, Thomas Reis, Martin Lipinski, Giovanna Selvaggi, John Stupak, T. Maerschalk, Erika Garutti, T. Caebergs, M. Edelhoff, Alexx Perloff, Steve Nahn, Giancarlo Mantovani, P. Buhmann, P. D'Angelo, Lorenzo Viliani, Sandra Oliveros, Jennifer Poehlsen, Ricardo Eusebi, Claus Kleinwort, T. Hauth, Mariarosaria D'Alfonso, Camilla Galloni, Andrew Godshalk, M. Vidal Marono, S. De Visscher, Alice Bean, Julia Thom, Volker Blobel, Lucia Silvestris, Neeti Parashar, Sebastiano Albergo, B. K. Kapustka, Paul Turner, Alexandra Junkes, Maurizio Biasini, Sinan Sagir, G. Bianchi, Dave Pellett, Fabrizio Ferro, Cecilia Elena Gerber, P. Rose, Ada Solano, Pisana Placidi, Salvatore Costa, Thomas Bergauer, Ludivine Ceard, Gian Mario Bilei, Regina Demina, Matthew Walker, Grzegorz Deptuch, Richard J. K. Taylor, Kevin Deroover, Bruno Wittmer, Suvadeep Bose, Deborah Pinna, L. Winstrom, Alessandro Gaz, Stefan Gruenendahl, Sam Daniel Mullin, Giacomo Sguazzoni, Marius Preuten, Giovanni Petrucciani, Alexander Schmidt, Nadir Daci, Mohsen Khakzad, M. Brianzi, C. Combaret, Loriano Storchi, Luisa Alunni Solestizi, Alessia Tricomi, Jaakko Härkönen, Markus Stoye, Institut de Physique Nucléaire de Lyon (IPNL), Centre National de la Recherche Scientifique (CNRS)-Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3), Institut Pluridisciplinaire Hubert Curien (IPHC), Université de Strasbourg (UNISTRA)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), CMS, Adam, W, Bergauer, T, Dragicevic, M, Friedl, M, Fruehwirth, R, Hoch, M, Hrubec, J, Krammer, M, Treberspurg, W, Waltenberger, W, Alderweireldt, S, Beaumont, W, Janssen, X, Luyckx, S, Van Mechelen, P, Van Remortel, N, Van Spilbeeck, A, Barria, P, Caillol, C, Clerbaux, B, De Lentdecker, G, Dobur, D, Favart, L, Grebenyuk, A, Lenzi, T, Leonard, A, Maerschalk, T, Mohammadi, A, Pernie, L, Randle-Conde, A, Reis, T, Seva, T, Thomas, L, Vander Velde, C, Vanlaer, P, Wang, J, Zenoni, F, Abu Zeid, S, Blekman, F, De Bruyn, I, D'Hondt, J, Daci, N, Deroover, K, Heracleous, N, Keaveney, J, Lowette, S, Moreels, L, Olbrechts, A, Python, Q, Tavernier, S, Van Mulders, P, Van Onsem, G, Van Parijs, I, Strom, D, Basegmez, S, Bruno, G, Castello, R, Caudron, A, Ceard, L, De Callatay, B, Delaere, C, Du Pree, T, Forthomme, L, Giammanco, A, Hollar, J, Jez, P, Michotte, D, Nuttens, C, Perrini, L, Pagano, D, Quertenmont, L, Selvaggi, M, Vidal Marono, M, Beliy, N, Caebergs, T, Daubie, E, Hammad, G, Harkonen, J, Lampen, T, Luukka, P, Maenpaa, T, Peltola, T, Tuominen, E, Tuovinen, E, Eerola, P, Tuuva, T, Beaulieu, G, Boudoul, G, Combaret, C, Contardo, D, Gallbit, G, Lumb, N, Mathez, H, Mirabito, L, Perries, S, Sabes, D, Vander Donckt, M, Verdier, P, Viret, S, Zoccarato, Y, Agram, J, Conte, E, Fontaine, J, Andrea, J, Bloch, D, Bonnin, C, Brom, J, Chabert, E, Charles, L, Goetzmann, C, Gross, L, Hosselet, J, Mathieu, C, Richer, M, Skovpen, K, Autermann, C, Edelhoff, M, Esser, H, Feld, L, Karpinski, W, Klein, K, Lipinski, M, Ostapchuk, A, Pierschel, G, Preuten, M, Raupach, F, Sammet, J, Schael, S, Schwering, G, Wittmer, B, Wlochal, M, Zhukov, V, Pistone, C, Fluegge, G, Kuensken, A, Geisler, M, Pooth, O, Stahl, A, Bartosik, N, Behr, J, Burgmeier, A, Calligaris, L, Dolinska, G, Eckerlin, G, Eckstein, D, Eichhorn, T, Fluke, G, Garay Garcia, J, Gizhko, A, Hansen, K, Harb, A, Hauk, J, Kalogeropoulos, A, Kleinwort, C, Korol, I, Lange, W, Lohmann, W, Mankel, R, Maser, H, Mittag, G, Muhl, C, Mussgiller, A, Nayak, A, Ntomari, E, Perrey, H, Pitzl, D, Schroeder, M, Seitz, C, Spannagel, S, Zuber, A, Biskop, H, Blobel, V, Buhmann, P, Centis-Vignali, M, Draeger, A, Erfle, J, Fretwurst, E, Garutti, E, Haller, J, Henkel, C, Hoffmann, M, Junkes, A, Klanner, R, Lapsien, T, Mattig, S, Matysek, M, Perieanu, A, Poehlsen, J, Poehlsen, T, Scharf, C, Schleper, P, Schmidt, A, Schuwalow, S, Schwandt, J, Sola, V, Steinbruck, G, Vormwald, B, Wellhausen, J, Barvich, T, Barth, C, Boegelspacher, F, De Boer, W, Butz, E, Casele, M, Colombo, F, Dierlamm, A, Eber, R, Freund, B, Hartmann, F, Hauth, T, Heindl, S, Hoffmann, K, Husemann, U, Kornmeyer, A, Mallows, S, Muller, T, Nuernberg, A, Printz, M, Simonis, H, Steck, P, Weber, M, Weiler, T, Bhardwaj, A, Kumar, A, Ranjan, K, Bakhshiansohl, H, Behnamian, H, Khakzad, M, Naseri, M, Cariola, P, De Robertis, G, Fiore, L, Franco, M, Loddo, F, Sala, G, Silvestris, L, Creanza, D, De Palma, M, Maggi, G, My, S, Selvaggi, G, Albergo, S, Cappello, G, Chiorboli, M, Costa, S, Giordano, F, Di Mattia, A, Potenza, R, Saizu, M, Tricomi, A, Tuve, C, Barbagli, G, Brianzi, M, Ciaranfi, R, Civinini, C, Gallo, E, Meschini, M, Paoletti, S, Sguazzoni, G, Ciulli, V, D'Alessandro, R, Gonzi, S, Gori, V, Focardi, E, Lenzi, P, Scarlini, E, Tropiano, A, Viliani, L, Ferro, F, Robutti, E, Lo Vetere, M, Gennai, S, Malvezzi, S, Menasce, D, Moroni, L, Pedrini, D, Dinardo, M, Fiorendi, S, Manzoni, R, Azzi, P, Bacchetta, N, Bisello, D, Dall'Osso, M, Dorigo, T, Giubilato, P, Pozzobon, N, Tosi, M, Zucchetta, A, De Canio, F, Gaioni, L, Manghisoni, M, Nodari, B, Re, V, Traversi, G, Comotti, D, Ratti, L, Bilei, G, Bissi, L, Checcucci, B, Magalotti, D, Menichelli, M, Saha, A, Servoli, L, Storchi, L, Biasini, M, Conti, E, Ciangottini, D, Fano, L, Lariccia, P, Mantovani, G, Passeri, D, Placidi, P, Salvatore, M, Santocchia, A, Solestizi, L, Spiezia, A, Demaria, N, Rivetti, A, Bellan, R, Casasso, S, Costa, M, Covarelli, R, Migliore, E, Monteil, E, Musich, M, Pacher, L, Ravera, F, Romero, A, Solano, A, Trapani, P, Jaramillo Echeverria, R, Fernandez, M, Gomez, G, Moya, D, Gonzalez Sanchez, F, Munoz Sanchez, F, Vila, I, Virto, A, Abbaneo, D, Ahmed, I, Albert, E, Auzinger, G, Berruti, G, Bianchi, G, Blanchot, G, Breuker, H, Ceresa, D, Christiansen, J, Cichy, K, Daguin, J, D'Alfonso, M, D'Auria, A, Detraz, S, De Visscher, S, Deyrail, D, Faccio, F, Felici, D, Frank, N, Gill, K, Giordano, D, Harris, P, Honma, A, Kaplon, J, Kornmayer, A, Kortelainen, M, Kottelat, L, Kovacs, M, Mannelli, M, Marchioro, A, Marconi, S, Martina, S, Mersi, S, Michelis, S, Moll, M, Onnela, A, Pakulski, T, Pavis, S, Peisert, A, Pernot, J, Petagna, P, Petrucciani, G, Postema, H, Rose, P, Rzonca, M, Stoye, M, Tropea, P, Troska, J, Tsirou, A, Vasey, F, Vichoudis, P, Verlaat, B, Zwalinski, L, Bachmair, F, Becker, R, Bani, L, Di Calafiori, D, Casal, B, Djambazov, L, Donega, M, Dunser, M, Eller, P, Grab, C, Hits, D, Horisberger, U, Hoss, J, Kasieczka, G, Lustermann, W, Mangano, B, Marionneau, M, Martinez Ruiz Del Arbol, P, Masciovecchio, M, Perrozzi, L, Roeser, U, Rossini, M, Starodumov, A, Takahashi, M, Wallny, R, Amsler, C, Bosiger, K, Caminada, L, Canelli, F, Chiochia, V, De Cosa, A, Galloni, C, Hreus, T, Kilminster, B, Lange, C, Maier, R, Ngadiuba, J, Pinna, D, Robmann, P, Taroni, S, Yang, Y, Bertl, W, Deiters, K, Erdmann, W, Horisberger, R, Kaestli, H, Kotlinski, D, Langenegger, U, Meier, B, Rohe, T, Streuli, S, Chen, P, Dietz, C, Grundler, U, Hou, W, Lu, R, Moya, M, Wilken, R, Cussans, D, Flacher, H, Goldstein, J, Grimes, M, Jacob, J, Seif El Nasr-Storey, S, Cole, J, Hobson, P, Leggat, D, Reid, I, Teodorescu, L, Bainbridge, R, Dauncey, P, Fulcher, J, Hall, G, Magnan, A, Pesaresi, M, Raymond, D, Uchida, K, Coughlan, J, Harder, K, Ilic, J, Tomalin, I, Garabedian, A, Heintz, U, Narain, M, Nelson, J, Sagir, S, Speer, T, Swanson, J, Tersegno, D, Watson-Daniels, J, Chertok, M, Conway, J, Conway, R, Flores, C, Lander, R, Pellett, D, Squires, F, Thomson, J, Yohay, R, Burt, K, Ellison, J, Hanson, G, Malberti, M, Olmedo, M, Cerati, G, Sharma, V, Vartak, A, Yagil, A, Zevi Della Porta, G, Dutta, V, Gouskos, L, Incandela, J, Kyre, S, Mccoll, N, Mullin, S, White, D, Cumalat, J, Ford, W, Gaz, A, Krohn, M, Stenson, K, Wagner, S, Baldin, B, Bolla, G, Burkett, K, Butler, J, Cheung, H, Chramowicz, J, Christian, D, Cooper, W, Deptuch, G, Derylo, G, Gingu, C, Gruenendahl, S, Hasegawa, S, Hoff, J, Howell, J, Hrycyk, M, Jindariani, S, Johnson, M, Jung, A, Joshi, U, Kahlid, F, Lei, M, Lipton, R, Liu, T, Los, S, Matulik, M, Merkel, P, Nahn, S, Prosser, A, Rivera, R, Shenai, A, Spiegel, L, Tran, N, Uplegger, L, Voirin, E, Yin, H, Adams, M, Berry, D, Evdokimov, A, Evdokimov, O, Gerber, C, Hofman, D, Kapustka, B, O'Brien, C, Sandoval Gonzalez, D, Trauger, H, Turner, P, Parashar, N, Stupak, J, Iii, C, Bortoletto, D, Bubna, M, Hinton, N, Jones, M, Miller, D, Shi, X, Tan, P, Baringer, P, Bean, A, Benelli, G, Gray, J, Majumder, D, Noonan, D, Sanders, S, Stringer, R, Ivanov, A, Makouski, M, Skhirtladze, N, Taylor, R, Anderson, I, Fehling, D, Gritsan, A, Maksimovic, P, Martin, C, Nash, K, Osherson, M, Swartz, M, Xiao, M, Acosta, J, Cremaldi, L, Oliveros, S, Perera, L, Summers, D, Bloom, K, Bose, S, Claes, D, Dominguez, A, Fangmeier, C, Gonzalez Suarez, R, Meier, F, Monroy, J, Hahn, K, Sevova, S, Sung, K, Trovato, M, Bartz, E, Duggan, D, Halkiadakis, E, Lath, A, Park, M, Schnetzer, S, Stone, R, Walker, M, Malik, S, Mendez, H, Ramirez Vargas, J, Alyari, M, Dolen, J, George, J, Godshalk, A, Iashvili, I, Kaisen, J, Kharchilava, A, Rappoccio, S, Alexander, J, Chaves, J, Chu, J, Dittmer, S, Kaufman, G, Mirman, N, Ryd, A, Salvati, E, Skinnari, L, Thom, J, Thompson, J, Tucker, J, Winstrom, L, Akgun, B, Ecklund, K, Nussbaum, T, Zabel, J, Betchart, B, Demina, R, Hindrichs, O, Petrillo, G, Eusebi, R, Osipenkov, I, Perloff, A, Ulmer, K, Delannoy, A, D'Angelo, P, Johns, W, Physics, Elementary Particle Physics, Helsinki Institute of Physics, Department of Physics, CMS Collaboration, UCL - SST/IRMP - Institut de recherche en mathématique et physique, European Commission, Bundesministerium für Bildung und Forschung (Deutschland), European Organization for Nuclear Research, The European Commission under the FP7 Research Infrastructures project AIDA, grant agreement no. 262025., and Federal Ministry of Education and Research (Germany)
Subjects: Physics - Instrumentation and Detectors, Annealing (metallurgy), Surface damage, Analytical chemistry, ComputingMilieux_LEGALASPECTSOFCOMPUTING, Settore ING-INF/01 - Elettronica, 7. Clean energy, damage [radiation], Charge sharing, Charge collection, Radiation damage, Silicon strip sensors, Nuclear and High Energy Physics, Instrumentation, Ionization, Detectors and Experimental Techniques, ComputingMilieux_MISCELLANEOUS, Physics, yield [charge], CMS, microstrip [semiconductor detector], Charge density, Instrumentation and Detectors (physics.ins-det), electric field, Chemistry, RADIATION-DAMAGE, Physique des particules élémentaires, Silicon strip sensor, oxygen [silicon], CHARGE, Engineering sciences. Technology, irradiation [electron], Silicon, PIXEL, education, FOS: Physical sciences, chemistry.chemical_element, density [charge], Radiation, 114 Physical sciences, Nuclear physics, Electric field, DETECTORS, Electron beam processing, ddc:530, [PHYS.PHYS.PHYS-INS-DET]Physics [physics]/Physics [physics]/Instrumentation and Detectors [physics.ins-det], numerical calculations, temperature dependence [damage], Hadron-Hadron Scattering, hep-ex, FISICA DELLE PARTICELLE, Physics and Astronomy, chemistry, Data_GENERAL, spatial distribution [electric field], Beyond standard model
Abstract: Under a Creative Commons license., The Tracker Group of the CMS Collaboration.-- et al., The response of n+p silicon strip sensors to electrons from a 90Sr source was measured using a multi-channel read-out system with 25 ns sampling time. The measurements were performed over a period of several weeks, during which the operating conditions were varied. The sensors were fabricated by Hamamatsu Photonics on 200 μm thick float-zone and magnetic-Czochralski silicon. Their pitch was 80 μm, and both p-stop and p-spray isolation of the n+ strips were studied. The electrons from the 90Sr source were collimated to a spot with a full-width-at-half-maximum of 2 mm at the sensor surface, and the dose rate in the SiO2 at the maximum was about 50 Gy(SiO2)/d. After only a few hours of making measurements, significant changes in charge collection and charge sharing were observed. Annealing studies, with temperatures up to 80 °C and annealing times of 18 h showed that the changes can only be partially annealed. The observations can be qualitatively explained by the increase of the positive oxide-charge density due to the ionization of the SiO2 by the radiation from the β source. TCAD simulations of the electric field in the sensor for different oxide-charge densities and different boundary conditions at the sensor surface support this explanation. The relevance of the measurements for the design of n+p strip sensors is discussed., The research leading to these results has received funding from the European Commission under the FP7 Research Infrastructures project AIDA, grant agreement no. 262025. We are also grateful to the HGF Alliance Physics at the Terascale, which has partially funded the setup used for the measurements, and to the BMBF, the Ministry of Research and Education of the German Federal Republic, for funding the Ph.D. position of J. Erfle within the Forschungsschwerpunkt FSP-102, Elementarteilchenphysik mit dem CMS-Experiment., Open Access funded by CERN.
Published: 2015

48. Impact of preoperative steroids administration on ischemia-reperfusion injury and systemic responses in liver surgery: A prospective randomized study

Author: Gianfranco Ferla, Laura Soldini, Luca Aldrighetti, Carlo Pulitano, Laura Comotti, Renato Finazzi, Marcella Arru, Marco Catena, Aldrighetti, L, Pulitano, C, Arru, M, Finazzi, R, Catena, M, Soldini, L, Comotti, L, and Ferla, G
Subjects: Adult, Male, Surgical stress, medicine.drug_class, Bilirubin, medicine.medical_treatment, Anti-Inflammatory Agents, Ischemia, Liver transplantation, Methylprednisolone, Proinflammatory cytokine, chemistry.chemical_compound, medicine, Humans, Aged, Aged, 80 and over, Transplantation, Hepatology, business.industry, Anticoagulant, Middle Aged, medicine.disease, Liver, chemistry, Reperfusion Injury, Anesthesia, Female, Surgery, business, Reperfusion injury, medicine.drug
Abstract: Hepatic injury secondary to warm ischemia-reperfusion (I/R) injury and alterations in haemostatic parameters are often unavoidable events after major hepatic resection. The release of inflammatory mediator is believed to play a significant role in the genesis of these events. It has been suggested that preoperative steroid administration may reduce I/R injury and improve several aspects of the surgical stress response. The aim of this prospective randomized study was to investigate the clinical benefits on I/R injury and systemic responses of preoperatively administered corticosteroids. Seventy-six patients undergoing liver resection were randomized either to a steroid group or to a control group. Patients in the steroid group received preoperatively 500 mg of methylprednisolone. Serum levels of alanine aminotransferase (ALT), aspartate aminotransferase (AST), total bilirubin, coagulation parameters, and inflammatory mediators, interleukin 6 and tumor necrosis factor alpha were compared between the 2 groups. Length of stay, and type and number of complications were recorded as well. Postoperative serum levels of ALT, AST, total bilirubin, and inflammatory cytokines were significantly lower in the steroid than in the control group at postoperative days 1 and 2. Changes in hemostatic parameters were also significantly attenuated in the steroid group. In conclusion, the incidence of postoperative complications in the steroid group tended to be significantly lower than the control group. It is of clinical interest that preoperative steroids administration before major surgery may reduce I/R injury, maintain coagulant/anticoagulant homeostasis, and reduce postoperative complications by modulating the inflammatory response.
Published: 2006

49. Beam test results for the SuperB-SVT thin striplet detector

Author: G. A. Beck, R. Cenci, M. Ceccanti, L. Lanceri, S. Zambito, Eugenio Paoloni, A. Perez, S. Coelli, B. Oberhof, Luca Bombelli, Alberto Stabile, C. Stella, Luigi Gaioni, F. F. Wilson, G. Petragnani, Mauro Villa, M. Citterio, Alberto Lusiani, Antonio Zoccoli, M. Prest, A. Bernardelli, G. Batignani, Stefano Zucca, Laura Fabbri, G.-F. Dalla Betta, Adrian John Bevan, G. Balestri, Massimo Manghisoni, S. Bettarini, P. Cristaudo, Gianluca Traversi, B. Liberti, A. Profeti, B. Nasri, Valentino Liberali, G. Casarosa, G. Fontana, D. Lietti, J. J. Walsh, L. Bosisio, M. Povoli, Carla Sbarra, Irina Rashevskaya, Giovanni Verzellesi, F. Giorgi, A. Berra, Filippo Bosi, N. Semprini-Cesari, Daniele Comotti, G. Rizzo, Lodovico Ratti, F. Palombo, Lucio Pancheri, Nicola Neri, E. Quartieri, F. Ganaway, Valerio Re, D. Gamba, John Morris, P. Mammini, G. Pellegrini, M.A. Giorgi, M. Monti, Alessia Manazza, F. Forti, Fabio Morsani, Alessandro Gabrielli, G. Alampi, G. Cotto, A. Soldani, Carlo Fiorini, Sara Valentinetti, M. Bomben, L. Vitale, L. Fabbri, D. Comotti, M. Manghisoni, V. Re, G. Traversi, A. Gabrielli, F. Giorgi, G. Pellegrini, C. Sbarra, N. Semprini-Cesari, S. Valentinetti, M. Villa, A. Zoccoli, A. Berra, D. Lietti, M. Prest, A. Bevan, F. Wilson, G. Beck, J. Morri, F. Ganaway, R. Cenci, L. Bombelli, M. Citterio, S. Coelli, C. Fiorini, V. Liberali, M. Monti, B. Nasri, N. Neri, F. Palombo, A. Stabile, G. Balestri, G. Batignani, A. Bernardelli, S. Bettarini, F. Bosi, G. Casarosa, M. Ceccanti, F. Forti, M.A. Giorgi, A. Lusiani, P. Mammini, F. Morsani, B. Oberhof, E. Paoloni, A. Perez, G. Petragnani, A. Profeti, G. Rizzo, A. Soldani, J. Walsh, L. Gaioni, A. Manazza, E. Quartieri, L. Ratti, S. Zucca, G. Alampi, G. Cotto, D. Gamba, S. Zambito, G.-F. Dalla Betta, G. Fontana, L. Pancheri, M. Povoli, G. Verzellesi, M. Bomben, L. Bosisio, P. Cristaudo, L. Lanceri, B. Liberti, I. Rashevskaya, C. Stella, L. Vitale, L., Fabbri, D., Comotti, M., Manghisoni, V., Re, G., Traversi, A., Gabrielli, F., Giorgi, G., Pellegrini, C., Sbarra, N., Semprini Cesari, S., Valentinetti, M., Villa, A., Zoccoli, A., Berra, D., Lietti, M., Prest, A., Bevan, F., Wilson, G., Beck, J., Morri, F., Ganaway, R., Cenci, L., Bombelli, M., Citterio, S., Coelli, C., Fiorini, V., Liberali, M., Monti, B., Nasri, N., Neri, F., Palombo, A., Stabile, G., Balestri, G., Batignani, A., Bernardelli, S., Bettarini, F., Bosi, G., Casarosa, M., Ceccanti, F., Forti, M. A., Giorgi, A., Lusiani, P., Mammini, F., Morsani, B., Oberhof, E., Paoloni, A., Perez, G., Petragnani, A., Profeti, G., Rizzo, A., Soldani, J., Walsh, L., Gaioni, A., Manazza, E., Quartieri, L., Ratti, S., Zucca, G., Alampi, G., Cotto, D., Gamba, S., Zambito, G. F., Dalla Betta, G., Fontana, L., Pancheri, M., Povoli, G., Verzellesi, Bomben, Marco, Bosisio, Luciano, P., Cristaudo, Lanceri, Livio, B., Liberti, Rashevskaya, Irina, Stella, Carlo, and Vitale, Lorenzo
Subjects: Vertex detectors, strip sensors, striplets, Nuclear and High Energy Physics, Silicon, Physics::Instrumentation and Detectors, Instrumentation, chemistry.chemical_element, Strip sensors, Striplet detector, Striplets, STRIPS, Settore ING-INF/01 - Elettronica, Particle detector, law.invention, Optics, law, Vertex detector, Nuclear Experiment, Vertex detectors Strip sensors Striplets Striplet detector Silicon tracking Charged particle tracking, Physics, Large Hadron Collider, sezele, MICROSTRIP DETECTORS, business.industry, Detector, charged particle tracking, silicon tracking, Semiconductor detector, chemistry, Strip sensor, Physics::Accelerator Physics, striplet detector, High Energy Physics::Experiment, business, Beam (structure)
Abstract: The baseline detector option for the first layer of the SuperB Silicon Vertex Tracker (SVT) is a high resistivity double-sided silicon device with short strips (striplets) at 451 angle to the detector’s edge. A prototype was tested with a 120 GeV/c pion beam in September 2011 at the SPS-H6 test-beam line at CERN. In this paper studies on efficiency, resolution and cluster size are reported.
Published: 2013

50. Methane and Carbon Dioxide Storage in a Porous van der Waals Crystal

Author: Roberto Simonutti, Piero Sozzani, Silvia Bracco, Angiolina Comotti, L. Ferretti, Sozzani, P, Bracco, S, Comotti, A, Ferretti, L, and Simonutti, R
Subjects: Nanostructure, Nanotechnology, General Medicine, General Chemistry, CHIM/04 - CHIMICA INDUSTRIALE, Catalysis, Methane, Crystal, CHIM/02 - CHIMICA FISICA, chemistry.chemical_compound, symbols.namesake, Adsorption, chemistry, Chemical engineering, gas adsorption, storage of CH4 and CO2, porous crystal, weak interactions, inclusion compounds, solid state NMR, Carbon dioxide, symbols, Pi interaction, van der Waals force, Porosity
Abstract: The first molecular crystal showing permanent porosity, made by of tris-o-phenylenedioxycyclotriphosphazene TPP molecules, is presented. The empty-pore hexagonal structure was solved after isolation of diffraction-quality single crystals and showed no residual electron density in the large unoccupied volume, shaped as straight nanochannels with a minimum diameter of 4.6 Å. Weak intermolecular interactions consolidate molecular stacks along the c axis (repeat period of 10.16 Å) and layers on the a–b plane (a=11.45 Å), ensuring the stability of the assembly. We showed the remarkable sorption properties of the porous molecular crystal with respect to important gases that participate in a network of soft interactions. Methane and carbon dioxide could be incorporated with high efficiency in the novel adducts (60% and 100% occupation, respectively, of the available sites, guest–host molar fraction of up to 1.25) with high selectivity over other gases. Unprecedented observations of the gases in van der Waals crystals and their topology could be provided by fast MAS NMR spectroscopy. The impressive upfield shifts caused by the aromatic ring currents of the host on gas molecules at the van der Waals contacts provided an unconventional tool for measuring the intermolecular gas-host distances and ricognizing the specific interactions that contribute to the overall stabilization. The multiple receptors lining the channel walls and the tight fit with the guests recall the specificity of biological nanochannels.
Published: 2005

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