1. Recycling Y and Eu fromWaste Fluorescent Powder and High Temperature Solid-State Synthesis of Y2O3:Eu Phosphors.
- Author
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Xiaodong Chen, Nian Liu, Guangjun Mei, and Mingming Yu
- Subjects
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PHOSPHORS , *CHEMICAL synthesis , *LEACHING , *SINTERING , *X-ray diffraction , *DIFFERENTIAL thermal analysis - Abstract
Y2O3:Eu were prepared through precursors synthesized by leaching tests, removing impurities, enrichment of Y and Eu from residual purified liquors, annealing treatment, and high temperature solid-state reaction method, which is the most suitable for large-scale production. The analysis of product shows that the purity is 99.42%. The resultant powders were characterized by X-ray diffraction (XRD), differential thermal analysis (TG-DTA), scanning electron microscope (SEM), and photoluminescence (PL). Compared with the commercial phosphors, the XRD spectrum of the product samples revealed the synthesized particles to have a pure cubic Y2O3:Eu structure without any impurities in the crystalline phase. On the morphology, the Y2O3:Eu particles synthesized by a combustion and high temperature solid state process with sintering aids, were large and uniform. For luminescence property, the emission intensity of Y2O3:Eu phosphors synthesized by combustion process and high temperature solid state process with sintering aids were higher than those without sintering aids, at 1400 °. [ABSTRACT FROM AUTHOR]
- Published
- 2017
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