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The article in Chemistry - Methods discusses the synthesis of salts of the parent carbaborate ion [CB11H12]− and its undecafluorinated form [CHB11F11]−, along with useful starting materials. Ingo Krossing and co‐workers provide detailed synthetic protocols for the large-scale synthesis of these compounds, including instructive videos for reproducibility. The authors also explore the chemical properties of [CHB11F11]− and synthesize its trityl and silver salts for various reactions. More information can be found in the Research Article by I. Krossing and co‐workers. [Extracted from the article]