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The performance of transition-edge sensors (TES) and their SQUID multiplexed readouts is very sensitive to ambient magnetic field and its fluctuations. In order to run ground experiments on thousands of X-ray TES microcalorimeters with a small uniform ambient magnetic field (< 1 μT, with a uniformity < 0.1 μT), we need a very low ambient field to be trapped into the superconducting magnetic shields. We have designed a sub-Kelvin test platform to reach these specifications. For this purpose, we modeled a new design for the shielding consisting of a series of different mu-metal and superconducting shields, including a niobium shield at 50 mK, a cryoperm (A4K) shield at 3 K, and a mu-metal shield at 300 K. A magnetic field coil is used to vary the local perpendicular magnetic field over the TES array. To optimize this field, we have studied a number of different field-coil designs and the impact of the different shield geometries, in order to reach the required field uniformity. [ABSTRACT FROM AUTHOR]

Superconducting transition-edge sensor (TES) microcalorimeters are being developed for a variety of potential astrophysics missions, including Athena. The X-ray integral field unit instrument on this mission requires close-packed pixels on a 0.25 mm pitch, and high quantum efficiency between 0.2 and 12 keV. In this work, we describe a new approach with 50 μm square TESs consisting of a Mo/Au bilayer, deposited on silicon nitride membranes to provide a weak thermal conductance to a ~ 50 mK heat bath. Larger TESs usually have additional normal metal stripes on top of the bilayer to reduce the noise. However, we have found that excellent spectral performance can be achieved without the need for any normal metal stripes on top of the TES. A spectral performance of 1.58 ± 0.12 eV at 5.9 keV has been achieved, the best resolution seen in any of our devices with this pixel size. [ABSTRACT FROM AUTHOR]

We present the result of the in-flight calibration of the effective area of the Soft X-ray Spectrometer (SXS) on board the Hitomi X-ray satellite using an observation of the Crab nebula. We corrected for artifacts when observing high count rate sources with the Xray microcalorimeter. We then constructed a spectrum in the 0.5-20 keV band, which we modeled with a single power-law continuum attenuated by interstellar extinction. We evaluated the systematic uncertainty of the spectral parameters by various calibration items. In the 2-12 keV band, the SXS result is consistent with the literature values in flux (2.20±0.08×10-8 erg s-1 cm-2 with a 1 s statistical uncertainty) but is softer in the powerlaw index (2.19±0.11). The discrepancy is attributable to the systematic uncertainty of about +6%/-7% and +2%/-5% respectively for the flux and the power-law index. The softer spectrum is affected primarily by the systematic uncertainty of the Dewar gate valve transmission and the event screening. [ABSTRACT FROM AUTHOR]

The X-Ray Spectrometer (XRS) instrument of Suzaku provided the first measurement of the non-X-ray background (NXB) of an X-ray calorimeter spectrometer, but the data set was limited. The Soft X-ray Spectrometer (SXS) instrument of Hitomi was able to provide a more detailed picture of X-ray calorimeter background, with more than 360 ks of data while pointed at the Earth, and a comparable amount of blank-sky data. These data are important not only for analyzing SXS science data, but also for categorizing the contributions to the NXB in X-ray calorimeters as a class. In this paper, we present the contributions to the SXS NXB, the types and effectiveness of the screening, the interaction of the screening with the broad-band redistribution, and the residual background spectrum as a function of magnetic cut-off rigidity. The orbit-averaged SXS NXB in the range 0.3-12 keV was 4 × 10-2 counts s-2 cm-2. This very low background in combination with groundbreaking spectral resolution gave SXS unprecedented sensitivity to weak spectral lines. [ABSTRACT FROM AUTHOR]

We develop superconducting transition-edge sensor (TES) microcalorimeter focal planes for versatility in meeting the specifications of X-ray imaging spectrometers, including high count rate, high energy resolution, and large field of view. In particular, a focal plane composed of two subarrays: one of fine pitch, high count-rate devices and the other of slower, larger pixels with similar energy resolution, offers promise for the next generation of astrophysics instruments, such as the X-ray Integral Field Unit Instrument on the European Space Agency's ATHENA mission. We have based the subarrays of our current design on successful pixel designs that have been demonstrated separately. Pixels with an all-gold X-ray absorber on 50 and 75 μm pitch, where the Mo/Au TES sits atop a thick metal heatsinking layer, have shown high resolution and can accommodate high count rates. The demonstrated larger pixels use a silicon nitride membrane for thermal isolation, thinner Au, and an added bismuth layer in a 250-μm2 absorber. To tune the parameters of each subarray requires merging the fabrication processes of the two detector types. We present the fabrication process for dual production of different X-ray absorbers on the same substrate, thick Au on the small pixels and thinner Au with a Bi capping layer on the larger pixels to tune their heat capacities. The process requires multiple electroplating and etching steps, but the absorbers are defined in a single-ion milling step. We demonstrate methods for integrating the heatsinking of the two types of pixel into the same focal plane consistent with the requirements for each subarray, including the limiting of thermal crosstalk. We also discuss fabrication process modifications for tuning the intrinsic transition temperature ( Tc) of the bilayers for the different device types through variation of the bilayer thicknesses. The latest results on these “hybrid” arrays will be presented. [ABSTRACT FROM PUBLISHER]

We are exploring the properties of electron-beam evaporated molybdenum thin films on silicon nitride coated silicon wafers at substrate temperatures between room temperature and 650 °C. The temperature dependence of film stress, transition temperature, and electrical properties are presented. X-ray diffraction measurements are performed to gain information on molybdenum crystallite size and growth. Results show the dominant influence of the crystallite size on the intrinsic properties of our films. Wafer-scale uniformity, wafer yield, and optimal thermal bias regime for TES fabrication are discussed. [ABSTRACT FROM PUBLISHER]

The science and an overview of the Soft X-ray Spectrometer onboard the STRO-H mission are presented. The SXS consists of X-ray focusing mirrors and a microcalorimeter array and is developed by international collaboration lead by JAXA and NASA with European participation. The detector is a 6×6 format microcalorimeter array operated at a cryogenic temperature of 50 mK and covers a 3′×3′ field of view of the X-ray telescope of 5.6 m focal length. We expect an energy resolution better than 7 eV (FWHM, requirement) with a goal of 4 eV. The effective area of the instrument will be 225 cm at 7 keV; by a factor of about two larger than that of the X-ray microcalorimeter on board Suzaku. One of the main scientific objectives of the SXS is to investigate turbulent and/or macroscopic motions of hot gas in clusters of galaxies. [ABSTRACT FROM AUTHOR]

We report on the development of position-sensitive transition-edge sensors (PoST's) for future X-ray astronomy missions such as the International X-ray Observatory (IXO), under study by NASA and ESA. PoST's consist of multiple absorbers each with a different thermal coupling to one or more transition-edge sensors (TESs). This results in a characteristic pulse shape for each absorber element and allows position discrimination. PoST development is motivated by a desire to achieve maximum focal-plane area with the fewest number of readout channels. We report detailed characterization of our single TES PoST's or Hydras, which consist of four electroplated AuIBi absorbers coupled to a low noise Mo/Au TES. Using a numerical model of the Hydra we fit to measured complex impedance curves and determine device parameters that allow us to accurately reproduce the measured pulse shapes and noise spectra. Results from Hydras with different internal thermal conductances reveal the trade-offs in optimizing for energy resolution or position-sensitivity. We report a best achievable energy resolution of <6.0 eV across all pixels for a device with transition temperature of 86 mK, coupled with straightforward position discrimination by rise-time. [ABSTRACT FROM AUTHOR]

The EBIT calorimeter spectrometer (ECS) is a new high-resolution, broadband x-ray spectrometer that has recently been installed at the Electron Beam Ion Trap Facility (EBIT) at the Lawrence Livermore National Laboratory. The ECS is an entirely new production class spectrometer that replaces the XRS/EBIT spectrometer that has been operating at EBIT since 2000. The ECS utilizes a 32-pixel x-ray calorimeter array from the XRS instrument on the Suzaku x-ray observatory. Eighteen of the pixels are optimized for the 0.1–10 keV band and yield 4.5 eV full width at half maximum energy resolution and 95% quantum efficiency at 6 keV. In addition, the ECS includes 14 detector pixels that are optimized for the high-energy band with a bandpass from 0.5 to over 100 keV with 34 eV resolution and 32% quantum efficiency at 60 keV. The ECS detector array is operated at 50 mK using a five stage cryogenic system that is entirely automated. The instrument takes data continuously for over 65 h with a 2.5 h recycle time. The ECS is a nondispersive, broadband, highly efficient spectrometer that is one of the prime instruments at the EBIT facility. The instrument is used for studies of absolute cross sections, charge exchange recombination, and x-ray emission from nonequilibrium plasmas, among other measurements in our laboratory astrophysics program. [ABSTRACT FROM AUTHOR]

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Abstract: The Japan/US Suzaku (formerly Astro-E2) astrophysics mission has been successfully launched. Suzaku is a powerful new orbiting observatory for studying extremely energetic processes in the universe. Sensitive X-ray spectrometers have been designed to enable precise measurements of high-energy processes in stars, supernova remnants, galaxies, clusters of galaxies, and the environments around neutron stars and black holes. One of the instruments is the high resolution X-ray spectrometer (XRS) that features a 32-pixel array of microcalorimeters with 6eV (FWHM) spectral resolution, the first such device to be placed into orbit. We will describe the capabilities of the XRS instrument and present some of the very early in-flight results, which clearly show that this new technology can work extremely well in space. [Copyright &y& Elsevier]

X-ray microcalorimeter arrays are well suited to address key problems in high-energy astrophysics. The Japan/US Astro-E2 mission will deploy a 32-pixel array of microcalorimeters with 6 eV resolution. This mission is scheduled for launch in 2005. Beyond Astro-E2, NASA is formulating the Constellation-X mission to provide a dramatic increase in collecting area with four separate spacecraft each with large area optics and 1 k-pixel calorimeter arrays providing an energy resolution of 2–4 eV.We will describe the microcalorimeter instrumentation on these missions and mention some of their scientific objectives. [Copyright &y& Elsevier]

Quantum microcalorimeters show promise in being able to fully resolve x-ray spectra from heavy highly charged ions, such as would be found in hot plasmas with temperatures in excess of 50 keV. Quantum microcalorimeter arrays are able to achieve this as they have a high-resolving power and good effective quantum efficiency for hard x-ray photons up to 60 keV. To demonstrate this, we present a measurement using an array of thin HgTe quantum microcalorimeters to measure the K-shell spectrum of hydrogenlike through carbonlike praseodymium (Z=57). With this device we are able to attain a resolving power, E/ΔE, of 1000 at a photon energy of 37 keV. [ABSTRACT FROM AUTHOR]

The x-ray spectrometer (XRS) instrument is a revolutionary nondispersive spectrometer that will form the basis for the Astro-E2 observatory to be launched in 2005. We have recently installed a flight spare XRS microcalorimeter spectrometer at the EBIT-I and SuperEBIT facility at LLNL replacing the XRS from the earlier Astro-E mission and providing twice the resolving power. The XRS microcalorimeter is an x-ray detector that senses the heat deposited by the incident photon. It achieves a high energy resolution by operating at 0.06 K and by carefully engineering the heat capacity and thermal conductance. The XRS/EBIT instrument has 32 pixels in a square geometry and achieves an energy resolution of 6 eV at 6 keV, with a bandpass from 0.1 to 12 keV (or more at higher operating temperature). The instrument allows detailed studies of the x-ray line emission of laboratory plasmas. The XRS/EBIT also provides an extensive calibration “library” for the Astro-E2 observatory. [ABSTRACT FROM AUTHOR]

The first two of four observatories in the constellation will be launched together in 2013 and followed a year later by the launch of the remaining pair. The four will independently orbit the Sun–Earth Lagrange point L2. An instrument compliment resides in the focal plane module (FPM) of each observatory 10 m from the optics module and consists of three hard X-ray telescope (HXT) detectors, a reflection grating spectrometer (RGS) focal plane CCD camera (RFC) and an X-ray microcalorimeter spectrometer (XMS). Instrument awards are scheduled for early 2006. The reference detector system for XMS is a 32 × 32 array of microcalorimetric superconducting transition edge sensors (TES) with SQUID based multiplexed readout and amplification. A multi-stage continuous ADR will provide the stable 50 mK desired for the TES array and a stable 1 K for the SQUID amplifiers while also lifting thermal parasitic and inefficiency loads to a 6 K cryocooler interface. The 6 K cryocooler is expected to emerge from the joint-project advanced cryocooler technology development program (ACTDP) in which Constellation-X is an active partner. Project pre-formulation activities are marked by extensive technology development necessitating early, but realistic, thermal and cooling load requirements for ADR and ACTDP-cryocooler design points. Such requirements are driven by the encompassing XMS cryostat and ultimately by the thermal environment imposed by the FPM. It is further desired that the XMS instrument be able to operate horizontally in the laboratory, with a warm vacuum shell, during an extensive calibration regime. It is that highly integrated reference instrument (microcalorimeter, ADR, cryocooler and cryostat) that will be examined here. [Copyright &y& Elsevier]

The Soft X-ray Spectrometer (SXS) instrument (Mitsuda et al., 2010) [1] on Astro-H (Takahashi et al., 2010) [2] will use a 3-stage ADR (Shirron et al., 2012) to cool the microcalorimeter array to 50 mK. In the primary operating mode, two stages of the ADR cool the detectors using superfluid helium at ⩽1.20 K as the heat sink (Fujimoto et al., 2010). In the secondary mode, which is activated when the liquid helium is depleted, the ADR uses a 4.5 K Joule–Thomson cooler as its heat sink. In this mode, all three stages operate together to continuously cool the (empty) helium tank and single-shot cool the detectors. The flight instrument – dewar, ADR, detectors and electronics – were integrated in 2014 and have since undergone extensive performance testing. This paper presents a thermodynamic analysis of the ADR’s operation, including cooling capacity, heat rejection to the heat sinks, and various measures of efficiency. [ABSTRACT FROM AUTHOR]

A 3-stage adiabatic demagnetization refrigerator (ADR) (Shirron et al., 2012) is used on the Soft X-ray Spectrometer instrument (Mitsuda et al., 2010) on Astro-H (Takahashi et al., 2010) [3] to cool a 6 × 6 array of X-ray microcalorimeters to 50 mK. The ADR is supported by a cryogenic system (Fujimoto et al., 2010) consisting of a superfluid helium tank, a 4.5 K Joule–Thomson (JT) cryocooler, and additional 2-stage Stirling cryocoolers that pre-cool the JT cooler and cool radiation shields within the cryostat. The ADR is configured so that it can use either the liquid helium or the JT cryocooler as its heat sink, giving the instrument an unusual degree of tolerance for component failures or degradation in the cryogenic system. The flight detector assembly, ADR and dewar were integrated into the flight dewar in early 2014, and have since been extensively characterized and calibrated. This paper summarizes the operation and performance of the ADR in all of its operating modes. [ABSTRACT FROM AUTHOR]