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We examined the effect of warm air-drying on the enamel bond strengths and the surface free-energy of three single-step self-etch adhesives. Bovine mandibular incisors were mounted in self-curing resin and then wet ground with #600 silicon carbide (SiC) paper. The adhesives were applied according to the instructions of the respective manufacturers and then dried in a stream of normal (23°C) or warm (37°C) air for 5, 10, and 20 s. After visible-light irradiation of the adhesives, resin composites were condensed into a mold and polymerized. Ten samples per test group were stored in distilled water at 37°C for 24 h and then the bond strengths were measured. The surface free-energies were determined by measuring the contact angles of three test liquids placed on the cured adhesives. The enamel bond strengths varied according to the air-drying time and ranged from 15.8 to 19.1 MPa. The trends for the bond strengths were different among the materials. The value of the [ABSTRACT FROM AUTHOR]

Summary: This paper reviews the performance of current adhesive systems in tests of bond strength between resin composites and tooth structures. The longevity and success of resin composite restorations depend upon the adhesive systems providing durable bonds with tooth substances. Both in vitro and in vivo testing has been used to predict the clinical outcome of treatments with adhesive materials. Subtle variations in sample preparation can severely affect the bond strength, regardless of the test method employed. In addition to the large range of factors that affect bond strength, various load applications have been used to quantify the adhesion between composites and tooth structures. Dentin bond strength is normally evaluated by conducting mechanical tests in the tensile and/or shear mode, but the crosshead speeds used vary over a relatively wide range in the published literature. This review provides an overview of the current characterization of dental adhesives and the factors affecting their performance in bond-strength tests. [Copyright &y& Elsevier]

Koga K, Tsujimoto A, Ishii R, Iino M, Kotaku M, Takamizawa T, Tsubota K, Miyazaki M. Influence of oxygen inhibition on the surface free-energy and dentin bond strength of self-etch adhesives. Eur J Oral Sci 2011; 119: 395-400. © 2011 Eur J Oral Sci We compared the surface free-energies and dentin bond strengths of single-step self-etch adhesives with and without an oxygen-inhibited layer. The labial dentin surfaces of bovine mandibular incisors were wet ground with #600-grit silicon carbide paper. The adhesives were applied to the ground dentin, light-irradiated, and the oxygen-inhibited layer was either retained or removed with ethanol. The surface free-energies were determined by measuring the contact angles of three test liquids placed on the cured adhesives. The dentin bond strengths of specimens with and without the oxygen-inhibited layer were measured. For all surfaces, the value of the estimated surface tension component was relatively constant at 35.5-39.8 mJ m−2. The value of the , Lewis acid component increased slightly when the oxygen-inhibited layer was removed, whereas that of the , Lewis base component decreased significantly. The bond strengths of the self-etch adhesives were significantly lower in specimens without an oxygen-inhibited layer (13.2-13.6 MPa) than in those with an oxygen-inhibited layer (17.5-18.4 MPa). These results indicate that the presence of an oxygen-inhibited layer in single-step self-etch adhesives with advanced photoinitiators promotes higher dentin bond strength. [ABSTRACT FROM AUTHOR]

This study investigated the influence of the bonded surface area and the crosshead speed on the dentin bond strengths of self-etch adhesives. Bovine mandibular incisors were mounted in self-curing resin and the facial surfaces were wet ground with #600 silicon carbide (SiC) paper. The dentin surfaces were treated according to the manufacturer's instructions. Adhesives were applied, and the resin composites were condensed into molds (2.4 or 4.0 mm in internal diameter), placed on to the dentin, and then light activated. Ten samples per test group were shear tested at crosshead speeds of 0.1, 0.5, 1.0, 5.0, and 10.0 mm/mm. The results showed that higher crosshead speeds were associated with higher dentin bond strengths. This relationship was more significant for specimens with a smaller dentin bonding surface area. [ABSTRACT FROM AUTHOR]

The influence of temperature and relative humidity (RH) on the bond strength of orthodontic adhesives was investigated. Two self-etching/composite type, one acid-etching/composite type, and one acid-etching/PMMA type of adhesives were examined under different temperature and RH conditions. Orthodontic brackets were bonded to bovine enamel, and shear bond strength test was performed at a crosshead speed of 1.0 mm/min after 24-hour storage in 37°C water. Data were analyzed by Tukey's HSD test. Each specimen was assigned an ARI score. All the materials tested exhibited their highest bond strength under room conditions at a range of 10.4-17.0 MPa. Conversely, when under a lower RH condition, bond strength for all the systems ranked the lowest within a range of 6.8-12.0 MPa, with bond failure at the bracket-adhesive interface. These results demonstrated that care should be exercised when using orthodontic adhesive systems in the oral environment. [ABSTRACT FROM AUTHOR]