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Background: This study aims to evaluate the microtensile bond strength (µTBS) of different resin composite restorations bonded to mid-coronal dentin and proximal root dentin using light-cured, chemical-cured, and dual-cured adhesives immediately and after aging. Nanoleakage and degree of cure were also assessed. Methods: Eighty-four molars were divided into mid-coronal dentin and proximal root dentin. Each group was further subdivided into three subgroups based on the restorative systems used, which involved the utilization of light-cured, chemical-cured, and dual-cured adhesives. Half of the specimens underwent µTBS testing after 24 h, while the other half after aging. Representative specimens were analyzed for nanoleakage. The degree of cure of the tested adhesive systems was also assessed. Results: Aging showed a significant negative effect on µTBS results and led to increased nanoleakage (p < 0.001). Furthermore, in all subgroups, the µTBS values of proximal root dentin were lower compared to mid-coronal dentin, except in the aged subgroup for the system utilizing the dual-cured adhesive. The restorative systems with chemical and dual-cured adhesives demonstrated comparable bonding properties. However, the system with the light-cured adhesive exhibited the worst bonding properties after aging when bonded to proximal root dentin and cured at a large distance (p < 0.05). Conclusions: All tested restorative systems were negatively affected by aging, and the regional dentin had variable effects on the bonding properties. Clinicians should exercise caution when using the tested light-cured adhesive in areas where the curing distance exceeds 3 mm. [ABSTRACT FROM AUTHOR]

This article comprehensively reviews the performance of simplified direct restorative materials that have the potential to be an alternative to amalgam. Following an understanding of the material structures and clinical performances, this review provides an analysis of the bonding mechanisms and influential factors on the bond strength. These factors include substrate-related variations, involving primary vs. permanent dentin, sound- vs. caries-affected/demineralized dentin comparisons and surface-related factors and pretreatments. Special attention is given to the factors changing the substrate surface, such as different contaminants, remedy methods after contamination and different conditioning methods related to the materials. Variations in sample preparation and bond strength test parameters are also evaluated for the analysis of the outcomes. This review aims to provide an overview of the factors involved in the application procedure of direct restorations together with in vitro testing variations to guide the selection of suitable materials by understanding strengths and shortcomings. [ABSTRACT FROM AUTHOR]

Background and Aims: The bond strength of direct composite restoration to the caries affected dentin is a challenging issue. Preparation of dentin with an antibacterial agent is a method for creating durable bonded restorations. The aim of this study was to investigate the effect of curcumin photosensitizer on the bond strength of a universal adhesive to the caries-affected dentin (CAD). Materials and Methods: In this experimental in vitro study, forty-four decayed human molar teeth were selected. After removing the surface enamel and dentin by a water-cooled saw, the decayed mid-coronal dentin was stained with a caries detection solution. The green and soft infected dentin was removed and CAD and hard and healthy surrounding dentin were left. Then, the remaining dentin surfaces were treated by 600 grit silicon carbide papers and polished. The specimens were divided into two groups (n=22): dentin pretreatment group by curcumin and control with no dentin pretreatment group by curcumin. Each group was divided into two subgroups based on the method of application of All-Bond Universal adhesive (Bisco, USA) (etch and rinseand self-etching methods). After placing the Aelite All Purpose Body (Bisco, USA) composite, all specimens were placed in a universal testing machine for microshear bond strength (µSBS) test. The failure mode of the isolated surfaces was evaluated under a stereomicroscope. Two-way ANOVA analysis was used for statistical analysis. Results: Based on the obtained results, intervention with the adhesive application method and surface pretreatment with curcumin had no significant effect on the bond strength. Also, there was no significant difference in the bond strength of the curcumin group in both etch and rinse and self-etching methods (SE=56.3±27.11 MPa; ER=52.4±84.11 MPa) (P=0.847). In the curcumin-free group, there was no significant difference between the two different adhesive application methods (P=0.187). Conclusion: The results obtained in the present study showed that the pretreatment of dentin affected by caries with light-sensitive curcumin and also use of a universal adhesive by either self-etching or self-etchinf methods had no influence on the microshear bond strength of the composite restoration. [ABSTRACT FROM AUTHOR]

Objective: This systematic review evaluated how different storage times and conditions affect universal adhesives' bond strength and degree of conversion (DC). Methods: A literature search was conducted in PubMed, Scopus, Web of Science, and Google Scholar databases for articles published from January 1st, 2000, until May 15th, 2022. The researchers comprehensively evaluated the articles using a multi-step process to identify articles relevant to the topic of interest. Quality assessment was performed through the ROBDEMAT tool. Due to the high heterogeneity in the preliminary data, performing a meta-analysis was not feasible. Results: A total of 3169 records were obtained, and after removing duplicates, 2267 remained. Following title and abstract screening, 2253 studies were excluded based on the predetermined exclusion criteria. Of the 14 remaining studies, seven were further excluded due to the use of non-universal adhesives, experimental adhesives, or lack of aging protocols. Ultimately, seven studies were included in this systematic review. All studies focused on bond strength, with only one addressing DC. The Findings showed that aging or different storage conditions generally led to reduced bond strength and DC values in universal adhesives, although exceptions with stable or improved properties were noted. Conclusions: Adhesives with higher pH and those containing methacrylamides, HEMA-free compositions, or hydrolytically stable monomers showed better durability than others. Strict adherence to storage instructions, lower storage temperatures, and immediate recapping of adhesive bottles after use is recommended to maintain adhesive properties. These findings provide insights for optimizing the long-term performance of universal adhesives in clinical settings. [ABSTRACT FROM AUTHOR]

The aim of this study was to evaluate the effects of the application of universal adhesive in the etch-and-rinse (ER) strategy with a manual brush (MB) or rotary brush (RB) in adhesion to dentin impregnated (WB) or not (NB) with bioceramic sealer, at 24 h and 1 year. Eighty-eight crowns of bovine incisors were divided into four groups (n=22): WB-MB, WB-RB, NB-MB, NB-RB. After the restorative protocol, dentin penetrability was evaluated by confocal microscopy. Bond strength was evaluated by microtensile test. Data were analyzed using one-way ANOVA/Tukey tests (α=0.05). NB-RB and WB-RB exhibited greater extensions of resin tags in dentin. At 24 h, WB-RB and NB-MB showed the highest and lowest values of bond strength, respectively. At 1 year, WB-MB and WBRB demonstrated the highest bond strength values. The RB increases the formation of resin tags and residues of bioceramic sealer provides higher bond strength in the ER strategy. [ABSTRACT FROM AUTHOR]

Modern conservative dentistry is taking the lead in daily clinical practice and is relying on adhesion. Whether it is a simple composite, ceramic inlays, onlays, veneers or crowns, the common factor for a successful outcome is a good bonding of these elements to dental structures. Thus, the purpose of this study was to evaluate the bond strength of resin composite to dentin when using a new device, the DENTIPURE KM™ (KM, Beirut, Lebanon), which provides a pure air flow, free of any contaminants and without humidity, when compared to other dental equipment. One hundred and eighty extracted human molars were equally divided into three groups according to the device used, the DENTIPURE KM™ (KM, Beirut, Lebanon), the KAVO™ (ESTETICA E30/E70/E80 Vision, KAVO, Biberach, Germany), or the ADEC™ (A-dec Performer 200, Newberg, OR, USA). The shear bond strength (SBS) was evaluated after 24 h of storage in distilled water on a universal testing machine. Statistical analysis was set with a level of significance at p ≤ 0.05. The results revealed that significantly different bond strength was imparted by the DENTIPURE KM™ device and the ADEC™ dental unit (p = 0.042). In conclusion, while the DENTIPURE KM™ device shows promise in providing contaminant-free air during bonding, its impact on dentin bond strength compared to devices like the KAVO™ appears minimal. Further research is needed to fully assess its potential in enhancing dentinal adhesion procedures. [ABSTRACT FROM AUTHOR]

Objective: This study investigated the effect of casein phosphopeptide-amorphous calcium phosphate (CPP-ACP) on the shear bond strength (SBS) of a universal adhesive in self-etch mode to demineralized dentin. Methods: Seventy-five dentin specimens were randomly divided into five groups (n=15) as follows: Group 1, intact dentin; Group 2, demineralized dentin receiving no remineralization agent; and Groups 3-5, demineralized dentin receiving CPP-ACP for 30, 90, and 180 seconds, respectively. All groups were bonded by Adper Single Bond Universal adhesive in self-etch mode. After 24 hours, the SBS test was conducted, and failure modes were recorded. The data were analyzed by one-way ANOVA, Tukey post-hoc test, and chi-square test at the significance level of P<0.05. Results: The highest and lowest mean SBS values were observed in groups 1 (intact dentin: 29.58 ± 8.13 MPa) and 2 (demineralized dentin: 13.41 ± 4.85 MPa), respectively. ANOVA revealed a significant difference in SBS among the groups (P< 0.001). A pairwise comparison revealed that the SBS of demineralized groups (groups 2-5) was significantly lower than that of the intact samples (P< 0.05). Group 5, with CPP-ACP, applied for 180 seconds, showed a significantly higher SBS (20.74 ± 4.54 MPa) compared to group 2 (P< 0.05). Conclusions: Applying CPP-ACP paste for three minutes can increase the bond strength of the universal adhesive in self-etch mode to demineralized dentin, whereas shorter application times are not effective. [ABSTRACT FROM AUTHOR]

Copyright of Brazilian Dental Science is the property of Brazilian Dental Science Journal-ICT-UNESP and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

INTRODUCTION: Advances in composite resins have changed the way restorative dentistry is now performed. The objective of restorative dentistry is to replace lost hard tissue with restorative material that has a good prognosis and longevity. In spite of the great improvements in the field of adhesive dentistry, hybridization of caries-affected dentin has been broadly avoided by clinicians and researchers. The loss of mineral content during a caries process is further compounded by action of matrix metalloproteinases (MMPs) on collagen of dentin. Recently, inhibition of MMPs has been the focus of research. OBJECTIVES: To compare the effect of MMP inhibitors on the bond strength of healthy dentin and caries-affected dentin. MMP inhibitors selected for this study were grape seed extract and riboflavin. MATERIAL AND METHODS: Thirty-six extracted teeth were divided into two groups: healthy dentin and caries-affected dentin (CAD). Samples were grounded to expose dentinal surfaces. CAD samples were exposed to 10% citric acid for 5 minutes to simulate caries. The exposed dentinal surfaces of samples in each group were then treated, either with grape seed extract or riboflavin, followed by application of eighth-generation bonding agent and restoration with a composite resin, standardized to a specific height and diameter. This assembly was then subjected to testing in a universal testing machine to evaluate tensile bond strength (TBS) of adhesive layers. RESULTS: The average TBS of healthy dentin treated with grape seed extract was found to be the highest (34.28 MPa) amongst the groups. The lowest TBS was found in the group with caries-affected dentin treated with riboflavin. There was a marked increase in TBS obtained in CAD after the application of MMP inhibitors. CONCLUSIONS: There is a significant difference between the bond strengths of healthy and caries-affected dentins. GSE and riboflavin both enhanced the bonding performance of eighth-generation bonding agent in both healthy dentin and CAD samples. [ABSTRACT FROM AUTHOR]

The aim of this study is to analyze the effects of different endodontic irrigants and adhesive systems on the resin bond strength of fiber post cementation. In total, 144 single-rooted, unrestored human teeth were endodontically treated and randomly divided into 12 groups according to four endodontic irrigants (distilled water as control; EDTA 17%; NaOCl 5%; chlorhexidine digluconate 2%) and three different adhesive/resin cement systems (etch-and-rinse: orthophosphoric acid, Parabond® A+B/Paracore®; self-etch: ParaBond® Non-Rinse Conditioner, Parabond® A+B/Paracore®; Universal: ClearfilTM Universal Bond/ClearfilTM DC Core Plus). Forty-eight hours after post cementation, ten teeth from each group were cross-sectioned into three discs (cervical, middle and apical regions). Thirty specimens of each group (n = 30) were submitted to a push-out test at a crosshead speed of 1 mm/min. The remaining two teeth of each group were sectioned in the same manner, and the resin–dentin interface was evaluated using scanning electron microscopy (SEM). The results were statistically analyzed with the ANOVA test and Tukey's test (p < 0,01). The adhesive protocols and post space region showed no significant effect on bond strength (p > 0.01). The combination of NaOCl 5% and ClearfilTM Universal Bond reduced the adhesive strength (p < 0.01). The NaOCl 5%, in relation to other irrigants, significantly decreased the push-out bond strength. [ABSTRACT FROM AUTHOR]

Purpose: To evaluate the effect of different concentrations of ethylene-diamine-tetra acetic acid (EDTA) on bond strength (BS) and nanoleakage (NL) of fiber posts bonded into root canals. Materials and Methods: Seventy-two single roots were endodontically treated and divided into six groups (n = 12), according to the combination of the following factors: surface treatment (no irrigation [control], 17% EDTA, or 24% EDTA), and composite cement applied with an adhesive used in a self-etch mode (Single Bond Universal/RelyX Ultimate [SB], 3M Oral Care; Ambar Universal/Allcem [AM], FGM). After fiber post cementation, six 1-mm-thick disks were obtained for each root. Push-out bond strength (BS) was evaluated using 8 specimens per group, and the other 4 specimens were used to examine nanoleakage (NL). Data from BS and NL of each adhesive were evaluated by two-way ANOVA (surface treatment vs root region) and Tukey's test (a = 0.05). Results: The application of 17% and 24% EDTA did not influence the bond strengths of either adhesive. In general, the application of 17% and 24% EDTA increased NL values for both adhesives. Conclusion: Pre-treatment with different concentrations of EDTA was not able to improve the adhesion of fiber posts into root canals with universal adhesives. [ABSTRACT FROM AUTHOR]

Objective: To evaluate the effect of etch‐and‐rinse (ER) versus self‐etch (SE) strategies of a universal adhesive applied with a manual brush (MB) or rotary brush (RB) on the bonding interface of fiber post cementation. Methods: Forty bovine incisor roots were prepared and divided into four groups according to the methods of application and strategy of universal adhesive use (MB‐ER, RB‐ER, MB‐SE and RB‐SE). After 6 months, specimens from different thirds of the post space were evaluated of push‐out strength, analysis of adhesive failure patterns, and extent of tags. Results: The RB‐ER and RB‐SE groups showed the highest bond strength values in the cervical and middle thirds of the post space. Cohesive adhesive failure had the highest incidence in the different thirds of the post space in the ER strategy, regardless of the adhesive application method. The RB‐ER group showed the highest tag extensions. Conclusions: The protocols of universal adhesive application with RB provided the greater bond strength, but only the ER strategy favored the formation of a greater extension of tags at the adhesive interface. Clinical Significance: The application of universal adhesive with RB into the post space increases the strength of the post‐cemented fiber bond. [ABSTRACT FROM AUTHOR]

Objective: To investigate the effect of extended air‐drying time on the microshear bond strength (MSBS) of universal adhesives to enamel. Materials and Methods: The distal and mesial specimens from third molars were wet‐ground and randomly assigned to three groups according to adhesives tested (n = 60): Clearfil Bond Universal, Gluma Bond Universal, and G‐Premio Bond. The adhesives were applied in etch‐and‐rinse or self‐etch modes, followed by air‐drying for 5, 15, or 25 s. Composite buildups were constructed and subjected to the MSBS test after 24‐h or thermocycling. MSBS results were evaluated using a four‐way ANOVA. The thickness of the adhesive layer and the degree of solvent evaporation were further evaluated. Results: At 24‐h, MSBS of G‐Premio Bond significantly improved with the 25 s air‐drying in both of the etching modes when compared to the 5 s air‐drying. After thermocycling, the extended air‐drying did not produce a significant difference on the MSBS, regardless of the application strategy. Extended air‐drying (25 s) evaporated almost all of the volatile part of Gluma Bond Universal and G‐Premio Bond. Conclusions: Extended air‐drying times increased solvent evaporation but did not contribute to the bonding effectiveness of the adhesives, regardless of the etching mode. Clinical Significance: Air‐drying applications for more than 5 s had no significant effect on enamel bonding performance of universal adhesives. [ABSTRACT FROM AUTHOR]

Copyright of Current Research in Dental Sciences is the property of Ataturk University Coordinatorship of Scientific Journals and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Purpose: To evaluate the effects of pretreatment with different crosslinking agents on glass-fiber-post adhesive luting. Materials and Methods: Single-rooted human teeth (n = 20) were randomly assigned to four groups: proanthocyanidins (PA) from grape-seed extract, cardol and cardanol (separated from cashew nut-shell liquid) and negative control (hydroethanolic solution). The solutions were applied on 37% phosphoric acid-etched dentin for 60 s. Glassfiber posts were cemented using a three-step etch-and-rinse adhesive (Scotchbond Multi-Purpose, 3M Oral Care) and composite cement (RelyX ARC, 3M Oral Care). Slices for the push-out bond strength test were cut and tested after 24-h or 6-month storage in distilled water. The dentin underlying the adhesive layer was analyzed by micro-Raman spectroscopy to evaluate vibrational formation of collagen crosslinks. Three additional slices per group were also made and the adhesive in-situ degree of conversion (DC) was analyzed by micro-Raman spectroscopy. The results were analyzed using two-way ANOVA and Tukey's test (p < 0.05). Results: No statistically significant changes in bond strength were found over time for any of the groups, except with cardol, which increased bond strength (8.4 ± 3.9 MPa at 24 h to 15.0 ± 2.9 MPa after 6 months, p < 0.001) after aging. The formation of peaks at 1117 cm-1 and 1235 cm-1 showed the presence of collagen crosslinks for all three biomodification agents. The DC outcomes showed no statistically significant differences between groups (p = 0.514). Conclusion: Biomodification agents did not impair adhesive polymerization. Cardol demonstrated a positive influence on intraradicular dentin bonding for glass-fiber post luting. [ABSTRACT FROM AUTHOR]

Purpose: To investigate the effects of root-canal dentin pretreatment with the crosslinker EDC combined with chitosan nanoparticles (Csnp) on the bonding quality of fiber posts in root canals in terms of bond strength, nanoleakage, quantification of collagen degradation, and degree of conversion (DC) of adhesive. Materials and Methods: Forty-eight single-rooted teeth were prepared endodontically and etched using UNI-ETCH (Bisco) as per the adhesive procedure for fiber posts. They were randomly divided into three groups before adhesive (All-Bond 3) application, according to different pretreatments: a. immersed in 2.5% glutaraldehyde for 24 h; b. treated with Csnp solution under ultrasonic agitation for 60 s and immersed in EDC crosslinker for 24 h; c. without treatment (control). Bond strength, nanoleakage, DC within the interface, and collagen fiber degradation were evaluated. Results: The pretreatments had a significant influence on the bonding stability of fiber posts in root canals, but not on the degree of conversion (p = 0.552). Enzymatic degradation significantly influenced bond strength for all groups (p = 0.001), with the greatest effect found in group c. The amount of amino acids released from the adhesive interface differed significantly between groups after hydrolysis and enzymatic degradation (p = 0.000); group c released the highest amount of amino acids. Conclusions: Csnp binding to dentin in combination with EDC reduced degradation of dentinal collagen and improved the stability of the adhesive interface without jeopardizing adhesive polymerization. [ABSTRACT FROM AUTHOR]

Amorphous calcium phosphate (ACP) which is a transient phase in the natural bio -mineralization process has recently gained the spotlight. This study aimed to assess the effect of the incorporation of nano -ACP (NACP) in a dental adhesive with/without surface treatment with silane coupling agent on bond strength. NACP was synthesized by the wet chemical precipitation technique. To characterize the structure of NACP, X-ray diffraction, scanning electron microscopy, and energy -dispersive X-ray spectroscopy were used. Forty molars were randomized into 4 groups of 10. The teeth were restored with composite resin and the bonding agent (one of the four groups). Adper Single Bond 2 was used as the control group. In the 4 wt% NACP group, NACP fillers were added to the bonding agent. In 0.4 wt% and 4 wt% SNACP groups, silanized NACP fillers were added to the bonding agent. Finally, the mode of failure of specimens was determined. Data were analyzed by one -way ANOVA and Tukey's post -hoc tests. P< 0.05 was considered statistically significant. The addition of 4 wt% non -silanized NACP decreased the bond strength compared with the control group (P< 0.05). The bond strength of the groups with silanized fillers was not significantly different from that of the control group. The addition of silanized NACP to dental adhesive had no significant adverse effect on bond strength, which is a promising finding to pave the way for the synthesis of bonding agents containing bioactive fillers. [ABSTRACT FROM AUTHOR]

The composition of universal adhesives, as well as the adhesive strategy, may influence bonding effectiveness and durability. This study aimed to evaluate the microtensile bond strength (µTBS) and nanoleakage (NL), immediately and after 6-month aging, and in situ degree of conversion (DC), of two universal adhesives (Scotchbond Universal Adhesive, SBU; Xeno Select, XEN) applied with etch-and-rinse (ER) and self-etch (SE) strategies, in comparison with a two-step SE adhesive (Clearfil SE Bond, CSE). Dentin surfaces of fifty human third molars were randomly assigned to the following adhesives: two universal adhesives, SBU and XEN, applied in ER or SE mode and CSE, used as control. Teeth were sectioned into beams to be tested under µTBS, half of them after 24 h, and the rest after 6 months of water aging. Selected beams from each tooth were used for NL evaluation and in situ DC quantification. SBU and CSE showed significantly higher mean µTBS and lower nanoleakage than XEN, regardless of the evaluation time and adhesion strategy. XEN-SE yielded the lowest degree of conversion. Therefore, adhesive properties of universal adhesives to dentin are material dependent, regardless of the adhesion strategy, exhibiting XEN a significantly worse performance than SBU. [ABSTRACT FROM AUTHOR]

Objectives: In this study, it was aimed to investigate the effects of different waiting periods on resin‐dentin bond strength (BS), degree of conversion (DC), contact angle (CA), surface tension (ST), solvent evaporation (weight loss) and the characteristics of adhesive interfaces of the current six universal adhesive resins (ARs). Materials and Methods: A total of 216 caries‐free human lower third molar teeth were used. Composite resin restorations were performed by applying six universal ARs in etch‐and‐rinse and self‐etch mode on standardized dentin surfaces after 0, 5, and 30 min waiting time. Then, a micro‐shear BS test, SEM examination and characterization of the adhesive interface were performed. In addition, DC, CA, ST, solvent evaporation of all tested ARs were evaluated. Results: The obtained data were statistically anaIyzed. The tested ARs did not show any statistical difference between 0 and 5 min evaluations in all parameters evaluated except for weight loss (p > 0.05). While the weight loss, ST and CA of all ARs increased in 30 min (p < 0.05), the BS, DC, thickness of the adhesive layer and the hybrid layer, resin tag length and number of resin tags varied according to the ARs used. When the ARs were used in etch‐and‐rinse mode, all the parameters evaluated also varied according to the AR used. Higher adhesive layer thickness and lower hybrid layer thickness were found in the self‐etch mode (p < 0.05). Conclusions: All of the adhesives tested can be safely used up to 30 min. This could also prevent economical loss caused by waste adhesive material. Clinical Significance: It is important to know how the bond strength, degree of conversion, adhesion, contact angle and surface tension properties of the adhesive resin waiting in the dispensing cup for a long time during clinical use are affected to make ideal restorations. [ABSTRACT FROM AUTHOR]

Purpose: To evaluate the effect of human and bovine root dentin age on the bond strength of fiber posts fixed with resin cements. The degree of conversion (DC) of the resin cements in different root thirds also was evaluated. Materials and Methods: Ninety-six single-rooted teeth were divided into groups according to the origin and age: young human (20-30 years), old human (over 60 years), young bovine (24-36 months) and adult bovine (over 48 months). The teeth were endodontically treated, and fiber posts were cemented with resin cements (RelyX Ultimate and RelyX U200). After 24 h, the teeth were sectioned perpendicularly and the push-out test was performed in a universal testing machine at a speed of 0.5 mm/min, until failure. One specimen from each third from each group (n = 6) was selected, and the DC of the resin cements was analyzed by FT-Raman spectroscopy. Results: For both resin cements, the young human root dentin group presented the highest bond strengths and the old human root dentin group presented the lowest (p < 0.05). The bond strengths of bovine root dentin groups were not affected by aging (p > 0.05). For the DC of resin cements, there were differences among the root thirds (p < 0.05), with the lowest values observed in the apical third. Conclusions: The bond strengths were higher in the young human root canal than in the bovine substrate, with a negative effect of aging in the human substrate. The DC of dual-curing resin cements decreased from the coronal to apical root thirds. [ABSTRACT FROM AUTHOR]

The aim of this study was to evaluate published data regarding riboflavin (RF) as a cross-linker for improved adhesive bond strength to dentin and to analyze previous studies for optimal concentration of riboflavin range suitable for dentin bond. Saliva and distilled water were used as storage media and aging time was 24 h and 6 months. Results of meta-analysis were synthesized using a statistical method of inverse variance in random effects with a 95% Confidence Interval (CI). Cochrane review manager 5.4.1 was used to determine results of the meta-analysis. In total, 3172 articles were found from search databases "PubMed", "Scopus", and "Google Scholar". Six of the fifteen studies were eligible for meta-analysis. Micro tensile strength shows significant improvement with the addition of riboflavin (p < 0.05) compared to without the addition of riboflavin from with 95% CI. A significant difference has been found in micro tensile bond strength between use of the riboflavin cross-linker and without use of the riboflavin crosslinker in the dentin adhesive system. With a 95% confidence interval (CI), the I2 for micro tensile strength was 89% with strong heterogeneity, Chi2 = 44.76, df = 5 (p < 0.00001), and overall effect size is Z = 2.22 (p = 0.03) after immediate aging. Chiang et al. 2013 shows maximum mean differences which is 38.50 [17.93–59.07]. After 6 months of aging in distilled water or artificial saliva micro tensile bond strength has been increased with the addition of riboflavin (p < 0.05). It can be clearly seen that pooled effect and 95% CI did not cross the line of no effect. With a 95% confidence interval (CI), the I2 for micro tensile strength was 96% with strong heterogeneity, Chi2 = 117.56, df = 5 (p < 0.00001), and overall effect size is Z = 2.30 (p = 0.02). Subgroup analysis proved a similar effect of distilled water and artificial saliva as storage media on micro tensile bond strength after incorporating riboflavin as a collagen crosslinker. An artificial saliva aged forest plot also showed considerable heterogeneity with I2 = 96%; Tau2 = 257.32; Chi2 = 94.37; df = 2 (p < 0.00001); test for overall effect, Z = 1.06 (p = 0.29). Riboflavin prior to or with bonding is recommended to improve the bonding of different adhesive systems. [ABSTRACT FROM AUTHOR]

To solve the proble ms of composite restoration failure caused by secondary caries, this study reports a light curable antibacterial triclosan derivative (TCS-IH), which was synthesized and added to the existing commercial universal adhesive to achieve a long-term antibacterial effect The effect of mixing different mass percentages of TCS-IH on the bond strength of dentin was also investigated.TCS-IH was synthesized by solution polymerization and characterized by nuclear magnetic resonance hydrogen spectroscopy (1H NMR) and Fourier transform infrared (FTIR) spectroscopy. Two commercial universal adhesives, Single Bond Universal and All Bond Universal, were selected and used as the control group, and universal adhesives with different mass percentages (1 wt%, 3 wt%, 5 wt% and 7 wt%) of TCS-IH were used as the experimental group. The antibacterial properties were analysed by means of colony count experiments, biofilm formation detection, plotting of growth curves, biofilm metabolic activity detection, insoluble extracellular polysaccharide measurements and observations by confocal laser scanning microscopy and scanning electron microscopy (SEM). The effect of adhesives on biofilm formation, metabolism, extracellular matrix production, distribution of live and dead bacteria, and bacterial morphology of Streptococcus mutans (S. mutans) was analysed. The mechanical properties were evaluated by the degree of conversion and microtensile bonding strength under different conditions. Its biosafety was tested. We found that the addition of TCS-IH significantly improved the antibacterial performance of the universal adhesive, with the 5 wt% and 7 wt% groups showing the best antibacterial effect and effectively inhibiting the formation of biofilm. In addition, the adhesive strength test results showed that there was no statistical difference (p < 0.05) in the microtensile bond strength measured under various factors in all experimental groups except for the 7 wt% group in the self-etch bonding mode, and all of them had good biosafety. In summary, the 5 wt% group of antibacterial monomer TCS-IH was selected as the optimum addition to the universal adhesive to ensure the antimicrobial properties of the universal adhesive and the stability and durability of the adhesive interface. This study provides a reference for the clinical application of adhesives with antimicrobial activity to improve the stability and durability of adhesive restorations. [ABSTRACT FROM AUTHOR]

Purpose: To evaluate the microshear bond strength (µSBS) of composite cement bonded to two machined glass ceramics and its durability, comparing conventional surface conditioning (hydrofluoric acid + silane) to a one-step primer (Monobond Etch & Prime). Materials and Methods: Machined slices of lithium disilicate ceramic (LDC) (IPS e.max CAD) and feldspathic ceramic (FC) (VITA Mark II) glass ceramics were divided into two groups (n = 10) according to two factors: 1. surface treatment: HF+S (ca 5% hydrofluoric acid [IPS Ceramic Etching GEL] + silane coupling agent [SIL; Monobond Plus]) or MEP (single-component ceramic conditioner; Monobond Etch & Prime); 2. storage condition: baseline (without aging; tested 24 h after cementing) or aged (70 days of water storage + 12,000 thermal cycles). Composite cement (Multilink Automix, Ivoclar Vivadent) was applied to starch matrices on the treated ceramic surfaces and photoactivated. A µSBS test was performed (0.5 mm/min) and the failure pattern was determined. Contact angle and micromorphological analyses were also performed. Data were analyzed with Student's t-test (α = 5%). Results: For both ceramic materials, HF+S resulted in higher mean µSBS (MPa) at baseline (LDC: HF+S 21.2 ± 2.2 > MEP 10.4 ± 2.4; FC: HF+S 19.6 ± 4.3 > MEP 13.5 ± 5.4) and after aging (LDC: HF+S 14.64 ± 2.31 > MEP 9 ± 3.4; FC HF+S: 14.73 ± 3.33 > MEP 11.1 ± 3.3). HF+S resulted in a statistically significant decrease in mean µSBS after aging (p = 0.0001), while MEP yielded no significant reduction. The main failure type was adhesive between composite cement and ceramic. HF+S resuted in the lowest contact angle. Conclusions: Hydrofluoric acid + silane resulted in higher mean µSBS than Monobond Etch & Prime for both ceramics; however, Monobond Etch & Prime had stable bonding after aging. [ABSTRACT FROM AUTHOR]

Purpose: To evaluate the microtensile bond strength (µTBS) and nanoleakage (NL) of several universal adhesives to eroded dentin (ED), using etch-and-rinse (ER) or self-etch (SE) strategies, and to characterize the surface using two pH cycling models to erode dentin (citric acid and a soft drink). Materials and Methods: Molars were eroded either by soft-drink or citric acid cycling, or were left untreated as control (SD). For each surface, the following adhesives were applied: 1. All-Bond Universal; 2. Ambar Universal; 3. Clearfil Universal; 4. Futurabond U; 5. One Coat 7 Universal; 6. Peak Universal Bond; 7. Prime&Bond Elect; 8. Scotchbond Universal; 9. Tetric n-bond Universal, and 10. Xeno Select. After application of the composite, specimens were sectioned into composite-dentin sticks and tested under tension (0.5 mm/min). Selected sticks from each tooth were used to assess NL. The occlusal dentin surfaces after erosive cycling were examined using SEM. Data were analyzed by three-way ANOVA and Tukey's post-hoc test (α = 0.05). Results: In ED, there was no difference in µTBS and NL between ER and SE strategies (p > 0.61). Most µTBS and NL values obtained for ED were, respectively, lower and higher than those for SD (p < 0.01), being worse for citric acid ED (p < 0.001). Citric-acid-eroded dentin showed more enlarged tubules, with partial loss of peritubular dentin when compared to soft-drink eroded dentin. Conclusion: The different pH cycling models reduced µTBS and increased NL of the composite/eroded-dentin interface; however, in ED, the performance of the universal adhesives did not depend on the adhesive strategy used. [ABSTRACT FROM AUTHOR]

This in vitro study aimed to evaluate the effect of different bonding strategies on the micro-shear bond strength (μSBS) of luting agents to CAD–CAM composites. Surface scanning electron microscopy (SEM) and spectroscopy by energy-dispersive X-ray spectroscopy (EDS) were performed to analyze the surfaces of the composite before and after bonding treatment. Three CAD–CAM composites were evaluated: Lava Ultimate restorative (LU), Brava Blocks (BR), and Vita Enamic (VE). The LU and BR surfaces were sandblasted using aluminum oxide, while the VE surfaces were etched using a 5% hydrofluoric acid gel according to the manufacturers' recommendations. All surfaces were subjected to the following bonding strategies (n = 15): adhesive with silane and MDP (ScotchBond Universal, 3M Oral Care, St Paul, MI, USA); adhesive with MDP (Ambar Universal, FGM, Joinville, Brazil); adhesive without silane or MDP (Prime&Bond Elect, Dentsply Sirona, Charlotte, NC, USA), pure silane without MDP (Angelus, Londrina, Brazil), and pure silane with MDP (Monobond N, Ivoclar Vivadent, Schaan, Liechtenstei). Afterwards, tygons were filled with RelyX Ultimate (3M Oral Care), AllCem (FGM), or Enforce (Dentsply Sirona), which were light-cured and subjected to the μSBS test. Data were analyzed using two-way ANOVA and Bonferroni's post hoc test (α = 0.05). Additional blocks (n = 15) were subjected to scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS) before and after the surface treatment. The μSBS values on VE surfaces were higher than those observed on LU and BR surfaces (p < 0.001). Silane without MDP (Allcem) promoted the highest μSBS values, while silane with MDP (RelyX Ultimate) provided the highest values among all bonding strategies (p < 0.001). Enforce promoted no significant difference in μSBS values. SEM and EDS analyses detected noticeable changes to the surface morphology and composition after the surface treatment. The effectiveness of the bonding strategy may vary according not only to the CAD–CAM composite but also to resin cement/bonding agent/silane used. [ABSTRACT FROM AUTHOR]

The present study evaluated the bond strength (μTBS) of dentin treated with chlorhexidine and propolis subjected to simulated pulpal pressure (SPP) and thermocycle aging. One hundred and twenty healthy human molars were sectioned to obtain 2 mm of dentin thickness and were divided into two groups (n = 60): SPP (15 cm H2O) and no SPP (Control group). Dentin surfaces were conditioned with 37% phosphoric acid for 15 s and were divided according to the dentin treatment (n = 20): Control; Chlorhexidine gluconate (0.2% for 30 s) and Propolis (aqueous propolis extract for 30 s). Half of the specimens were submitted to 15,000 thermocycle aging (5 ± 2°C and 55 ± 2°C). The samples were sectioned into beams and submitted to μTBS. Data were analyzed by three‐way ANOVA (SPP × Dentin treatment × Thermocycle aging) and the Tukey's tests (p <.001). With regard to the SPP, ANOVA revealed that the Control group (32.98 MPa) had significantly higher values of μTBS when compared to the SPP (29.19 MPa). With regard to Thermocycle aging, no aging (34.05 MPa) had significantly higher values of μTBS when compared to the aging (28.12 MPa). With regard to the dentin treatment, Propolis and Chlorhexidine did not statistically influence the results (p >.05). The SPP and thermocycle aging negatively influenced the bond strength between the dentin and resin; the 0.2% chlorhexidine digluconate and aqueous propolis extract solutions did not interfere in the bond strength between the resin and dentin. The use of chlorhexidine and propolis as a dental treatment may not influence the dentin bond strength, but SPP and thermocycle aging may damage the longitudinal dentin bond strength. Research Highlights: Chlorhexidine and propolis as a dental treatment may not influence the dentin bond strength.Simulated pulpal pressure and thermocycle aging may damage the longitudinal dentin bond strength. [ABSTRACT FROM AUTHOR]

This paper evaluates the effect of an additional hydrophobic resin coat (extra HL) associated with universal adhesives on sound and eroded dentin and evaluated immediately or after 2 years of water storage to improve the microtensile bond strength (μTBS) and nanoleakage (NL) when compared to the use of universal adhesives only. Sixty-four molars were assigned to eight groups using the following combinations: 1. dentin substrate, including sound and eroded dentin; 2. treatment, including the control and extra HL and storage time (immediately and after two-years of storage). Two universal adhesives (Prime & Bond Active or Scotchbond Universal) were evaluated. Before restoration, half of the teeth were subjected to soft-drink erosion. Composite buildups were bonded; specimens were stored (37 °C/24 h), sectioned into resin–dentin bonded sticks and tested for microtensile bond strength and nanoleakage using SEM (immediately and after two-years of storage). Three-way ANOVA and Tukey's test (α = 0.05%) were used. In the immediate testing, the application of extra HL did not increase microtensile bond strength values compared with the control group in either substrate (p > 0.05). However, extra HL significantly decreased nanoleakage values when applied to eroded and sound dentin (p = 0.0001). After two years, the application of extra HL produced significantly higher microtensile bond strength and lower nanoleakage values than the control group for both adhesives (p = 0.0001). In all cases, sound dentin showed higher microtensile bond strength and lower nanoleakage values than eroded dentin (p = 0.000001). An extra HL increased the bond strength and reduced nanoleakage in eroded dentin after two-years of storage. [ABSTRACT FROM AUTHOR]

This study aimed at evaluating the influence of glass-fiber post (GFP) relining with composites of different opacities on resin cement layer thickness (CLT), bond strength (BS) to root dentin, and resin cement degree of conversion (DC%). Standardized roots of 52 bovine incisors had their canals prepared and were distributed into 4 groups (n = 10 for CLT and BS; n = 3 for DC%) according to the post used: WP3 (Control)—Whitepost DC3; groups DE, EN and TR—Whitepost DC0.5 relined, respectively, with dentin, enamel, and translucent shade composites. After cementation, specimens were sectioned into six 1.0 mm-thick discs that were submitted to push-out BS test. CLT and failure pattern were evaluated using a stereomicroscope and DC% by micro-Raman spectroscopy. Data were analyzed by two-way ANOVA and Tukey test (α = 0.05). The control group showed greater CLT than all relined groups (p < 0.05), which did not differ from each other (p > 0.05). Groups relined with low opacity composites (TR; EN) showed the highest BS and DC% means (p < 0.05). BS was not different among root thirds (p > 0.05), while DC% decreased from cervical to apical third (p < 0.05). Adhesive failures between cement and dentin were predominant, except for group DE with frequent mixed failures. It could be concluded that composite opacity did not influence CLT, which was thinner when GFP were relined and that relining GFP with lower opacity composites led to higher BS and DC%. [ABSTRACT FROM AUTHOR]

Purpose: To evaluate the effect of sonic application of 5 different self-etch adhesives on the push-out bond strength of fiber posts in root canals. Materials and Methods: In a preliminary test, 24 teeth were treated with manual and sonically assisted bonding, then a composite cylinder was built up to test the shear bond strength as a proof of principle. In the main test, 120 root canals were endodontically prepared and divided into 10 groups: 5 self-etch adhesives (Futurabond DC, Futurabond M, Futurabond U, Optibond XTR, Universalbond), each applied under manual and sonic application modes. After insertion of the fiber posts using the specific adhesive and a dual-curing composite, the teeth were sectioned and the push-out test was performed. The specimens were analyzed by light and scanning electron microscopy. Statistical analysis was performed using the Shapiro-Wilk test, one-way ANOVA and the Tamhane test. Results: Sonic application of self-etch adhesive systems did not increase the bond strength of fiber posts in root canals. In general, the bond strength decreased from the coronal to the apical part of the root canal, irrespective of the applied method. The best post retention was achieved with Futurabond U and Optibond XTR. Conclusion: Sonic application of self-etch adhesives did not improve the fiber post retention in the root canal and can therefore not be recommended. Nevertheless, sonic application of etch-and-rinse adhesives can increase the bond strength to coronal dentin. [ABSTRACT FROM AUTHOR]

Purpose: To evaluate the effect of a silane and an adhesive containing MDP, used alone or combined in the same solution, on the microshear bond strength (µSBS) to lithium disilicate ceramics immediately and after 1-year water storage, and compare the bond strength results with the Raman spectra of the treated lithium disilicate surfaces. Materials and Methods: A total of 30 CAD/CAM blocks of lithium disilicate (LD; IPS e.max CAD) were cut into four square sections (6 x 6 x 6 mm; n = 60 per group) and processed as recommended by the manufacturer. The LD specimens were divided into 12 groups according to the following independent variables: silane coupling agent (no silane; silane without 10-MDP [MBS, Monobond S]; silane with 10-MDP [MB+, Monobond Plus]) and adhesive + luting composite (no adhesive + Enforce; no adhesive + RelyX Ultimate; Prime & Bond Elect [PBE], a silane-and MDPfree universal adhesive + Enforce; Scotchbond Universal Adhesive [SBU], a silane-and MDP-containing universal adhesive + RelyX Ultimate). After each treatment, cylindrical, transparent matrices were filled with a luting composite and light cured. Specimens were stored in water (37°C for 24 h or 1 year) and submitted to the microshear bond strength (µSBS) test. The failure pattern and µSBS were statistically evaluated (a = 0.05). In addition, specimens were examined for chemical interaction using Raman spectroscopy. Results: The use of the adhesive PBE alone showed higher mean µSBS compared with both groups with silane (MSB or MB+) without PBE (p < 0.001) at 24 h. The use of the SBU adhesive or MBS silane alone, as well as MB+ associated with SBU, showed higher mean µSBS (p < 0.001) at 24 h. After 1-year water storage, all groups showed a significant decrease in mean µSBS. However, the application of PBE or SBU associated with MB+ silane showed higher 1-year mean µSBS (p < 0.001). In terms of chemical interaction, when silane (MSB or MB+) was applied, only a slight decrease of Si-O peaks occurred. Otherwise, when PBE or SBU adhesives were applied, methacrylate peaks were only observed in the SBU groups. Conclusion: The best results in terms of bond strength after water storage were obtained when an MDP-containing silane was associated with a universal adhesive. The use of a simplified bonding protocol that includes either a silane or a universal adhesive is not recommended. [ABSTRACT FROM AUTHOR]

Objectives: This study aimed at evaluating the microtensile bond strength (μTBS) and the resin-dentine ultramorphology (24 h and 10 months ageing) of contemporary universal adhesives applied in self-etch (SE) or etch-and-rinse (ER) mode. Materials and methods: Sixty-four sound human molars were collected and randomly allocated in 4 main experimental groups (n = 16) according to the adhesive system employed and subsequently divided into two subgroups depending on their application mode SE or ER (n = 8): ZipBond X (ZBX-SE; ZBX-ER), Prime and Bond Active (PBA-SE; PBA-ER), Clearfil Universal Bond Quick (CBQ-SE; CBQ-ER) or Scotchbond Universal (SCH-SE; SCH-ER). The specimens were cut into sticks with a cross-sectional area of approximately 0.9 mm2 and subjected to μTBS testing at 24 h or after 10 months of ageing in artificial saliva (AS). Five representative fractured specimens from each group were analysed using field-emission scanning electron microscopy (FE-SEM). Resin-dentine slabs (Ø 0.9mm2) from each experimental group were immersed in Rhodamine B and subsequently analysed using confocal microscopy analysis (CLSM). The μTBS results were analysed using a two-way ANOVA and Newman–Keuls multiple-comparison test (α = 0.05). Results: ZBX, PBA and SCH exhibited greater μTBS values than CQB at 24 h in both SE and ER modes (p < 0.05). CQB showed a significant decrease in μTBS values after ageing both when used in SE and ER mode (p < 0.05). ZBX-ER exhibited no significant differences in the μTBS test after ageing (p > 0.05), while a significant drop in μTBS was seen in SCH-ER and APB-ER after 10-month ageing (p < 0.05). Clear signs of degradation were evident in the resin-dentine interface created with CQB regardless of the application mode or the ageing time. In APB-ER and SCH-ER groups, such signs of degradation were evident after ageing in AS. ZBX showed slight dye infiltration both when used in ER and SE mode. Conclusions: The long-term bonding performance of modern universal adhesives is usually influenced by the adhesive strategy employed; self-etching application should be prioritised during dentine bonding. Moreover, the use of shortened bonding protocols may compromise the quality of the resin-dentine interface and the bonding performance of most modern universal adhesives. Clinical relevance: The use of etch-and-rinse bonding procedures, as well as "shortened" application protocols should be eluded when using modern universal adhesives in dentine. However, new generation universal adhesives based on innovative chemical formulations may probably allow clinicians to achieve long-term bonding performance with such simplified system also when employed in ER mode. [ABSTRACT FROM AUTHOR]

Since the adhesion of resin composites to calcium silicate-based cement is considered challenging. Therefore, the best adhesion strategy should be indicated. This review aimed to assess the effect of different adhesive systems on the bond strength of resin composite to calcium silicate-based cement through a systematic review and meta-analysis. The subsequent PICOS framework used was: population, calcium silicate-based cement; intervention, use of self-etch adhesive systems; control, use of total-etch adhesive systems; outcome, bond strength; study design, in vitro studies. The literature search was conducted independently by two reviewers up to 18 February 2021. Electronic databases (PubMed, ISI Web of Science, SciELO, Scopus, and Embase) were searched for applicable articles. In vitro manuscripts studying the effect of adhesive systems on the bond strength of calcium silicate-based cement were considered. The meta-analyses were performed using Review Manager Software version 5.3.5 (The Nordic Cochrane Centre, The Cochrane Collaboration, Copenhagen, Denmark). Bond strength comparisons were made considering the type of calcium silicate-based cement (Mineral Trioxide Aggregate (MTA), Biodentine™, or TheraCal LC®). A p-value < 0.05 was considered statistically significant. A total of 7321 studies were retrieved in databases searched. After full-text evaluation, 37 eligible papers were assessed for qualitative analysis, leaving a total of 22 papers for the quantitative analysis. According to the meta-analysis, the bond strength values of resin composite materials to MTA and TheraCal LC® cement were favored when a total-etch adhesive system was used (p ≤ 0.02). On the other hand, the meta-analysis of the bond strength of resin-based materials to Biodentine™ calcium silicate-based cement was similar between both approaches (p = 0.12). The in vitro evidence suggests that the bond strength of resin-based materials to both MTA and TheraCal LC® cement was preferred by using the total-etch adhesive strategy. However, when bonding to Biodentine™, the use of self-etch or total-etch strategies displayed promising results. Given the lack of evidence related to the chemical interaction of self-etch adhesive materials with the bioceramics, if self-etch adhesives are used for bonding resin-based restorations to calcium silicate-based cement, a pretreatment with phosphoric acid could be recommended. [ABSTRACT FROM AUTHOR]

Objectives: To evaluate the effect of Nd:YAG laser irradiation as a prior desensitizing strategy on immediate and medium-term microtensile bond strength (µTBS) to simulated hypersensitive dentin. Materials and methods: Flat mid-coronal dentin was obtained from third molars and submitted to a 600-grit SiC paper (1 min; N: normal dentin) or subsequently challenged with citric acid (6%, 1 min; H: simulated hypersensitive dentin). Afterwards, dentin was or was not (C: control; HC, NC — each n = 7) irradiated with Nd:YAG laser (L: laser; 1.0 W/10 Hz/100 mJ/4 irradiations of 50-60 s; HL, NL — each n = 7). A 2-step self-etch adhesive (Clearfil SE Bond) was applied and composite (Filtek Z350) buildups were constructed. After 24-h (distilled water/37 °C) storage, specimens were sectioned into beams and tested (µTBS; 0.5 mm/min) immediately or after 6-month aging. Three-way ANOVA and Tukey tests were applied (α = 0.05). Qualitative evaluation of the adhesive interface (n = 1 extra tooth per group) was performed by Confocal Laser Scanning Microscopy. Results: Substrate condition (p < 0.001), laser irradiation (p < 0.001), and aging (p = 0.002) influenced the results. Furthermore, there was interaction between substrate and irradiation (p < 0.001). Laser irradiation favored µTBS exclusively to hypersensitive dentin immediately and after aging. µTBS to hypersensitive dentin was higher than that to the normal substrate only when it was laser-irradiated. In any case, immediate µTBS was always higher than that after aging. CLSM revealed longer and more numerous resin tags for simulated hypersensitive dentin, and shorter and fewer resin tags for laser-irradiated dentin. No differences were observed in the hybrid layer itself. Conclusion: Nd:YAG laser irradiation prior to restoration favored the µTBS of a self-etch adhesive and resin composite to hypersensitive dentin. Clinical relevance: Desensitizing strategies are usually tried before performing restorative treatments in hypersensitive dentin; therefore, they may influence behavior of the adhesive interface established. However, instead of causing concern, Nd:YAG laser irradiation revealed a favorable effect on the aforementioned interface. [ABSTRACT FROM AUTHOR]

PURPOSE. This study aimed to compare the effect of different surface treatments and luting agent types on the shear bond strength of two ceramics to commercially pure titanium (Cp Ti). MATERIALS AND METHODS. A total of 160 Cp Ti specimens were divided into 4 subgroups (n = 40) according to surface treatments received (control, 50 μm airborne-particle abrasion, 110 μm airborne-particle abrasion, and tribochemical coating). The cementation surfaces of titanium and all-ceramic specimens were treated with a universal primer. Two cubic all-ceramic discs (lithium disilicate ceramic (LDC) and zirconia-reinforced lithium silicate ceramic (ZLC)) were cemented to titanium using two types of resin-based luting agents: self-cure and dual-cure (n = 10). After cementation, all specimens were subjected to 5000 cycles of thermal aging. A shear bond strength (SBS) test was conducted, and the failure mode was determined using a scanning electron microscope. Data were analyzed using three-way ANOVA, and the Tukey-HSD test was used for post hoc comparisons (P < .05). RESULTS. Significant differences were found among the groups based on surface treatment, resin-based luting agent, and ceramic type (P < .05). Among the surface treatments, 50 μm air-abrasion showed the highest SBS, while the control group showed the lowest. SBS was higher for dual-cure resin-based luting agent than self-cure luting agent. ZLC showed better SBS values than LDC. CONCLUSION. The cementation of ZLC with dual-cure resin-based luting agent showed better bonding effectiveness to commercially pure titanium treated with 50 μm airborne-particle abrasion. [ABSTRACT FROM AUTHOR]

The objective was to evaluate the influence of active bonding applications (ABA) for different time intervals after selective dentin etching (SDE) for 3 s on the microtensile bond strength (μTBS) to dentin of two universal adhesive systems (UAs): one containing 2-hydroxyethyl methacrylate (HEMA) (Scotchbond Universal, SBU), and one that was HEMA-free (Prime&Bond Universal, PBU). Dentin bovine specimens were divided into four groups: self-etch as control (SE), SDE + ABA for 15 s (SDE15), SDE + ABA for 20 s (SDE20), and SDE + ABA for 25 s (SDE25). The μTBS test was performed after a water storage of 24 h and 6 months. Scanning electron microscopy (SEM) was used in order to examine the resin–dentin interface. For the PBU, the µTBS was significantly influenced only by the aging factor (p < 0.026). A statistically significant decrease in the µTBS after 6 months of aging was observed only for the SDE15 group. For SBU, µTBS was significantly influenced by the protocol application and the aging time (p ≤ 0.041). The groups SDE15, SDE20, and SDE25 achieved statistically significant higher values (after 24 h and 6 months). No considerable variances were noticed in the homogeneity and continuity of the hybrid layer (HL) among the groups. In conclusion, SDE and ABA improved the µTBS only of a HEMA-containing universal adhesive. [ABSTRACT FROM AUTHOR]

Purpose: To evaluate whether the etch-and-rinse or self-etching mode of a universal adhesive is the best protocol to optimize bond strength to primary and permanent artificially-induced caries-affected dentin. Materials and Methods: Flat midcoronal dentin surfaces were exposed in 24 primary and 24 permanent molars and submitted to pH cycling for 14 days to induce artificial caries-affected dentin. For each tooth type (primary and permanent), the teeth were randomly assigned to 4 different groups according to the adhesive systems and bonding strategy: a universal adhesive, Scotchbond Universal Adhesive, in self-etching and etch-and-rinse modes; a twostep etch-and-rinse adhesive, Adper Single Bond 2 (control); and two-step self-etching system, Clearfil SE Bond (control). After bonding and restorative procedures, specimens were sectioned to obtain rectangular sticks (0.8 mm2) that were submitted to microtensile tests (crosshead speed: 1 mm/min). The data were analyzed using two-way ANOVA (α = 0.05). Results: The universal adhesive showed bond strengths similar to those of the control groups, irrespective of the bonding strategy. Likewise, statistically similar bonding performance was observed for all adhesives to either artificially- induced caries-affected primary or permanent dentin. Conclusion: The new universal adhesive, Scotchbond Universal Adhesive, can be used in both application modes in artificially-induced caries-affected primary and permanent dentin, as the bond strength was not influenced by the different substrates or application mode. [ABSTRACT FROM AUTHOR]

Purpose: To evaluate the effect of a scrubbing technique with one-step self-etching adhesives on bond strengths and nanoleakage expression at the resin/dentin interface. Materials and Methods: Flat human dentin surfaces bonded with one of two mild self-etching adhesives, SE One (SE) or Scotchbond Universal (SU) applied either with scrubbing or without scrubbing technique, were prepared (n = 5). The microtensile bond strengths (μTBS), SE micrographs of morphological changes on treated dentin surfaces, and expression of nanoleakage along the bonded dentin interfaces as shown with TEM were evaluated. μTBS data were analyzed using two-way ANOVA and the post-hoc t-test at the significance level of 0.05. Results: The scrubbing technique had a significant positive effect on the μTBS of SU (p < 0.05), while it produced no significant difference for SE (p > 0.05). Morphological evaluation of the treated dentin surfaces demonstrated that SU with scrubbing showed the highest etching ability, followed by scrubbing SE > nonscrubbing SE > nonscrubbing SU. In the nonscrubbing groups, nanoleakage formation using SU exhibited a reticular pattern throughout the hybridized complex, whereas with SE, water-tree nanoleakage was only found in the adhesive layer at dentinal tubule orifices. The scrubbing groups of both adhesives did not exhibit any nanoleakage expression. Conclusion: Using a scrubbing technique when applying mild self-etching adhesives could improve resin monomer infiltration into dentin, chase water on adhesive surfaces, and facilitate smear layer removal. [ABSTRACT FROM AUTHOR]

Aim: To prolong the clinical success and durability of bonded restorations, hybrid layer stabilization is crucial for better adhesion between the resin and tooth substrate. The aim of this in vitro study was to assess the ability of self-assembling peptide (curodont protect) and a remineralizing agent (MI paste plus) in promoting biomimetic remineralization for stabilization of the hybrid layer to improve the resin-dentin bond durability. Materials and Methods: Standardized mesio-occlusal (MO) and disto-occlusal (DO) cavities were prepared on 60 mandibular molars. Teeth were randomly allocated to different groups and after acid etching, half of the MO cavities (n = 30) of dentin were treated with curodont protect and another half (n = 30) with MI paste plus. Half of the DO cavities (n = 30) were pretreated with chlorhexidine, whereas the other half did not receive any dentin pretreatment before placing adhesive restoration. Half of the samples from each group (n = 15) were subjected to thermomechanical load cycles. Immediate and after aging bond strengths were estimated using a universal testing machine, and the type of bond failure was assessed under a scanning electron microscope. Data obtained in megapascals were analyzed by one-way analysis of variance and Tukey's multiple post hoc test with the significance level set as P ≤ 0.05. Results: Immediate bond strength values were significantly high for the control group and low for the MI paste plus group (P = 0.002). Significant differences were not observed between the curodont protect and chlorhexidine (P = 0.0514) treated groups. In all groups, bond strength values were decreased significantly after thermomechanical cyclic (TMC) loading (P = 0.0001). Adhesive type fractures were reported more in failure mode analysis. Conclusion: All groups exhibited reduced microtensile bond strength values after aging. The dentin treated with chlorhexidine, curodont protect, and MI paste plus produced more durable bonding than the control group. [ABSTRACT FROM AUTHOR]

Dentin erosion is a frequent clinical condition that requires restorative interventions, especially in cases with moderate to severe wear. This requires clinicians to have knowledge about the characteristics of dentin, etiological factors involved, and restorative approaches to be made. Minimally invasive restorations have been indicated for rehabilitation of these cases, in order to preserve the largest possible amount of dental tissue. To achieve this, effective and durable adhesion to the eroded dentin must be obtained. However, the histological and morphological changes resulting from the erosive challenge have make eroded dentin a much more challenging substrate to treat than sound dentin. In order to minimize these limitations, mechanical and chemical strategies, as well as changes in the adhesive protocol, have been reported in the literature. The purpose of this review was to present these limitations and discuss the effectiveness of the strategies suggested, based on the results of bond strength to eroded dentin. [ABSTRACT FROM AUTHOR]

This study evaluated the effects of remaining dentin thickness (RDT), different smear layers, and aging on the microtensile bond strength (μTBS) of universal adhesives to dentin when applied in self-etch mode. Ninety-six human third molars were randomly allocated to 12 groups (n=8) based on adhesives: ClearfilTM SE Bond 2 (SE, control), ClearfilTM Universal Bond (CU) and ScotchBondTM Universal Adhesive (SB); smear layers: prepared either with 600-grit SiC paper (P) or regular diamond bur (B); and aging: stored in distilled water at 37ºC for 24 hours (24h) or 1 year (1y). μTBS was significantly affected by the type of adhesives, smear layers, and aging (p<0.001). A statistically significant and positive linear relationship was also observed between μTBS and RDT (p<0.05) in all the tested groups, except for SEB1y and CUB24h (p>0.05). RDT, smear layer types, and aging can influence the bonding performances of universal adhesives when applied in self-etch mode. [ABSTRACT FROM AUTHOR]

Purpose: To evaluate the effect of the alcohol wet-bonding technique on bond performance of the adhesive interface produced by two-step etch-and-rinse adhesive systems. Materials and Methods: Composite buildups were bonded to sectioned human third molars using Adper Single Bond 2 (SB) bonded to acid-etched dentin saturated with water (control) or ethanol, or XP Bond (XP) bonded to acid-etched dentin saturated with water (control) or tert-butanol. A simplified dentin dehydration protocol was performed using 100% ethanol or 99.5% tert-butanol directly applied to dentin for 60 s. Specimens were cut into nontrimming dentin-composite beams that were divided equally in two subgroups: immediately tested and after immersion in 10% NaOCI solution for 1 h. Specimens were tested in tension at a crosshead speed of 1 mm/ min until failure, and the failure mode was evaluated. Data were statistically analyzed with three-way ANOVA and Tukey's test (a = 0.05). Additional dentin disks were bonded using the same groups tested and examined for leakage under light microscopy after immersion in ammoniacal silver nitrate solution. Results: The SB control group showed significantly higher bond strength values than did SB used on ethanol-saturated dentin (p < 0.05); this tendency was confirmed by the silver nitrate deposition. The use of tert-butanol did not influence XP bond strength values (p > 0.05) or silver nitrate penetration. NaOCI solution significantly reduced the bond strength of all groups tested (p < 0.05) and also increased the interfacial silver nitrate penetration. Conclusion: The simplified alcohol wet-bonding technique used in the present study was not able to improve resin/dentin bond performance for simplified etch-and-rinse adhesive systems. [ABSTRACT FROM AUTHOR]

This study evaluated the influence of a bonding approach using proanthocyanidins (PAs) combined with ethanol‐wet bonding (EWB) and a hydrophobic adhesive on the bonding quality of fibre posts. After endodontic treatment and post‐space preparation, 72 single‐rooted extracted human teeth were etched, thoroughly rinsed, and then treated using the following procedures (n = 24 teeth per group): group 1, no pretreatment; group 2, pretreatment with absolute ethanol three times, for 30 s each time; or group 3, pretreatment with absolute ethanol solution containing 5% PAs three times, for 30 s each time. Six teeth per group were dried according to a dry and a wet drying protocol and then observed using field emission‐scanning electron microscopy. The remaining 18 teeth in each group were cemented with fibre posts: All‐Bond 3 and Duo‐Link cement were used for group 1; and hydrophobic adhesive and Duo‐Link cement were used for groups 2 and 3. Push‐out bond strength, failure mode, and nanoleakage were evaluated immediately and after collagenase treatment. Higher push‐out bond strength and less nanoleakage were observed in the two ethanol‐pretreatment groups, regardless of storage conditions. Teeth pretreated with PAs + ethanol exhibited significantly higher push‐out bond strength after collagenase treatment than did teeth pretreated with ethanol alone. Within the limits of this study, the bonding approach of PAs combined with EWB and a hydrophobic adhesive synergistically improved the durability of fibre post bonds. [ABSTRACT FROM AUTHOR]

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Purpose: To evaluate the in vitro bond strength of universal adhesive systems to indirect substrates. Material and Methods: Two reviewers performed a literature search up to March 2018 in seven databases: PubMed, Web of Science, SciELO, Scopus, LILACS, IBECS, and BBO. The review included studies that compared the bond strength of universal adhesives and well‐established material‐specific primers to indirect substrates: lithium disilicate ceramic, yttrium‐stabilized zirconium dioxide ceramic, leucite‐reinforced ceramic, feldspathic porcelain, polymer infiltrated ceramic material, resin composite or metal alloys. Analyses were carried out using RevMan 5.3.5. A global comparison was performed with the standardized mean difference using a random‐effects models at a significance level of p < 0.05. Results: A total of 45 studies were included in the qualitative analysis, and the meta‐analysis was performed with 42 studies. Bond strength to glass‐based ceramics and alloys was improved with the use of a specific‐primer as separate step before the bonding procedures (lithium disilicate, p < 0.001; alloys, p < 0.001). The bond strength to zirconium substrates was improved with the use of universal adhesives (p < 0.001). For bond strength to composite resin as indirect substrate, universal adhesives performed in a manner similar to that of the material‐specific primer (p = 0.11). Conclusions: The clinical procedure of luting zirconia and resin composite restorations could be simplified by using single‐bottle universal adhesives. However, the ability of universal adhesives to achieve an adequate and durable bond to glass‐based ceramics and alloys appears to be limited. [ABSTRACT FROM AUTHOR]

The aim of this in vitro investigation was to evaluate the effects of different dentin treatments on µTBS values of three different universal adhesives. Sixty extracted bovine incisors were used. The teeth were horizontally sectioned from the enamel-cement junction and embedded in an acrylic resin. Enamel was removed with 180-grit SiC paper to expose dentin. The exposed dentin surfaces were further polished with 600-grit SiC paper to provide a standardized smear layer. Teeth were randomly divided into three groups, according to the universal adhesives: All-Bond Universal, Single Bond Universal, and G-Bond Plus. Each group was then assigned into four subgroups, according to the dentin treatments: etch-and-rinse mode (ER), ER + 2% chlorhexidine (CHX), ER + %2.5 genipin (GE), and self-etch mode (SE). Samples were longitudinally sectioned across the bonded-interfaces to obtain resin-dentin beams. Beams were prepared from the same teeth were randomly and equally divided into two groups: immediate µTBS testing and µTBS testing after 6-month. The failure loads were recorded in MPa, and failure modes were evaluated at 30× magnification. The data were analyzed using a two-way ANOVA, to determine the effects of dentin treatment and storage time, and the interaction of these two factors on the µTBS of universal adhesives. Dentin treatments were showed significant differences (p < 0.05). ER mode exhibited higher µTBS than SE mode. However, universal adhesives were more durable in the SE mode than ER mode. Also, chlorhexidine treatment significantly improved adhesive performance of all universal adhesives, while no significant improvement was detected with genipin treatment. [ABSTRACT FROM AUTHOR]

Statement of the Problem: Universal or multi-mode adhesives are new adhesive systems that can be used in both etch-and-rinse (ER) and self-etch (SE) modes. Lesser technical sensitivity and dual use of these adhesives have made them popular among dentists. Studies are being conducted to analyze the advantages and disadvantages these adhesives in different conditions Purpose: The aim of this study was to compare shear bond strength (SBS) of a multimode adhesive in different etching modes to Er,Cr:YSGG laser ablated and bur-cut dentin. Materials and Method: Buccal and lingual surfaces of 30 sound human molars, randomly divided to three groups, were prepared by bur and Er,Cr:YSGG (4 Watt and 5 Watt, 20 Hz, 96% water, 60% air, and 600-μm spot size) to reach a flat surface in superficial dentin. Each group was randomly divided into 2 subgroups (ER and SE), and then Scotchbond Universal adhesive was applied. Composite cylinders were attached to the surfaces and cured. Specimens were stored in 37 °C water for 24 hours and thermocycled (500 cycles) and were tested for SBS and failure modes were determined by stereomicroscope. Data was analyzed using SPSS19 and one- way ANOVA and Tukey's post hoc tests and p< 0.05 was considered as significance level. Results: Bur-cut dentin with ER method had the highest mean SBS value (33.80 MPa). SBS in bur-cut and 4Watt laser in ER mode were significantly higher than SE mode (p= 0.002 and p= 0.000 respectively). Highest mean SBS value in lased dentin was achieve in 4 Watt ER mode. Conclusion: SBS of Scotchbond universal adhesive to dentine is highest in bur-cut and ER mode and in 4-Watt lased-dentin is higher than 5-Watt lased-dentin. Moreover, in 4-Watt lased-dentin, SBS of ER mode is more than SE mode. [ABSTRACT FROM AUTHOR]

Copyright of RSBO: Revista Sul-Brasileira de Odontologia is the property of UNIVILLE and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Introduction: The purpose of this in vitro study was to assess the effects of anatomic root levels, different adhesive strategies and cementation system on bond strength (BS), nano leakage (NL) and degree of conversion (DC) after fiber posts cementation. Methods and Materials: Sixty-six roots of human premolars were endodontically prepared and divided according to the combination of adhesive application technique (manual passive, manual active and active vibratory) and the cementation system (Adper Single Bond 2/RelyX ARC [SBAR] and Single Bond Universal/RelyX Ultimate [SBUL]). Specimens were transversally sectioned into six 1-mm-thick serial slices, which were subjected to BS testing (n=7), to NL analysis using scanning electron microscopy (SEM) after slice immersion in silver nitrate (n=2), and micro-Raman spectroscopy for DC (n=2). Data were analyzed using two-way ANOVA and Bonferroni post-hoc test (α=5%). Results: Bond strength values significantly increased with active vibratory application technique (P<0.001), no significant difference was noted between adhesive systems. The cementation system Single Bond Universal/RelyX Ultimate demonstrated the lowest nano leakage values (P<0.05). The manual active and vibratory application techniques showed statistically higher degree of conversion values than the manual passive technique at the coronal and medium thirds (P<0.05); and the lowest results were observed with manual passive application to Single Bond Universal/RelyX Ultimate (P=0.016). Conclusion: The study concluded that techniques with active application (vibratory and manual) resulted in higher bond strength values. The mode of adhesive application influence the results. [ABSTRACT FROM AUTHOR]

Currently, the long-term success of esthetic rehabilitation with ceramics is required. Hence, professional knowledge about the most indicated dental material for each clinical situation as well as its usage protocol is essential. The aim of this systematic review of clinical and laboratorial studies was to compare the bond strength of prostheses using silane incorporated to universal adhesives or applied separately. The literature search in databases "Cochrane Library," "MEDLINE," "Web of Science," "Scopus," "LILACS," "Scielo," and "Google Scholar" was based on the keywords "Silane;" "Silanes;" "Silane coupling agent;" "Universal adhesive;" and "Universal adhesives." A total of five articles were included in this review. In general, the studies showed better results for ceramic etching with hydrofluoric acid and application of silane separately to the universal adhesive. As a conclusion, the treatment with pure silane or as an additional pretreatment with universal adhesives improved the bond strength of glass ceramics. Hence, higher shear bond strength can be achieved, resulting in treatment longevity. [ABSTRACT FROM AUTHOR]

Aim: The aim of this study is to evaluate the impact of dentin condition on bond strength of multi-mode adhesive systems (MMAS) to sound and artificially induced caries-affected dentin (CAD). Methods: Flat dentin surfaces of 112 bovine incisors were assigned to 16 subgroups (n = 7) according to the substrate condition (sound and CAD- pH-cycling for 14 days); adhesive systems (Scotchbond Universal, All-Bond Universal, Prime and Bond Elect, Adper Single Bond Plus and Clearfil SE Bond) and etching strategy (etch-and-rinse and self-etch). All systems were applied according to the manufacturer's instructions and resin composite restorations were built. After 24 h of water storage, specimens were sectioned (0.8 mm2) and submitted to the microtensile test. Statistical Analysis: Data (MPa) were analyzed using three-way analysis of variance and Tukey's test (α = 0.05). Results: MMAS presented similar bond strength values, regardless etching strategy in each substrate condition. Bond strength values were lower when MMAS were applied to CAD in the etch-and-rinse strategy. Conclusion: The etching strategy did not influence the bond strength of MMAS to sound or CAD, considering each substrate separately. However, CAD impact negatively on bond strength of MMAS in etch-and rinse mode. [ABSTRACT FROM AUTHOR]