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Start Over Author "Ross J.L. Edgar" Topic biochemistry
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1. Expedient synthesis of highly substituted 3,4-dihydro-1,2-oxathiine 2,2-dioxides and 1,2-oxathiine 2,2-dioxides: revisiting sulfene additions to enaminoketones

Author

Mike W. J. Urquhart, Abby J. Mills, B. Mark Heron, Stuart Aiken, Ross J.L. Edgar, Lewis Cowen, Orlando D. C. C. de Azevedo, Craig R. Rice, Kelechi Anozie, Philippa A. Lawrence, Christopher D. Gabbutt, and Dimitrios Zonidis

Subjects
chemistry.chemical_compound, chemistry, 010405 organic chemistry, Sulfene, Organic Chemistry, Moiety, Physical and Theoretical Chemistry, 010402 general chemistry, 01 natural sciences, Biochemistry, Combinatorial chemistry, 0104 chemical sciences
Abstract

Diversely substituted 1,2-oxathiine 2,2-dioxides, including 3,5,6-triaryl-, 3,6-diaryl-, 3,5-diaryl-, 5,6-diaryl- and selected fused heterocyclic analogues, have been efficiently obtained by the application of a mild Cope elimination of a 4-amino moiety from the requisite 4-amino-3,4-dihydro-1,2-oxathiine 2,2-dioxides, which themselves were readily obtained by the addition of sulfenes to enaminoketones.

Published
2019
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