Author: "Han, Ruirui" / Topic: amide synthesis - Searchworks@Jio Institute Digital Library Search Results

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Start Over Author "Han, Ruirui" Topic amide synthesis

Author: Zhang, Yi, Zhong, Zhihao, Han, Yingmei, Han, Ruirui, and Cheng, Xu
Subjects: *AMIDE synthesis, *BORON trifluoride, *CATALYSTS, *TEMPERATURE effect, *BIOCONVERSION, *SOLVENTS
Abstract: Abstract: A convenient synthesis of bisamide from aldehyde and amide with BF3 etherate as catalyst was reported. Both aryl and aliphatic bisamides could be prepared with this procedure in high yield at room temperature and the catalyst loading as low as 0.5 mol % was achieved. Fine-tuned solvent was utilized for both rapid conversion and simple isolation. Two CB2 receptor inverse agonists were synthesized with this protocol in high yield. [Copyright &y& Elsevier]
Published: 2013
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Author: Zhang, Yi, Zhong, Zhihao, Han, Yingmei, Han, Ruirui, and Cheng, Xu
Subjects: *AMIDE synthesis, *CATALYSIS, *ALDEHYDES, *CHEMICAL reactions, *ORGANIC compounds
Abstract: BF3-catalyzed reaction of carboxylic amides with a variety of aldehydes allows the synthesis of bisamides under very mild reaction conditions. [ABSTRACT FROM AUTHOR]
Published: 2014
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