Search

7050 Al alloy was successfully processed by equal-channel angular pressing (ECAP) at room temperature (RT). The effect of ECAP on the subsequent aging precipitation behavior was investigated by using transmission electron microscopy (TEM) and high resolution transmission electron microscopy (HRTEM). The results reveal that the kinds, spatial distribution and sizes of precipitates in the unECAPed and the ECAPed samples are different. ECAP accelerates the process of aging precipitation and results in the broadening of precipitate size distribution. ECAP can produce not only deformation heat but also internal defects such as excess vacancies and high density of dislocations when the sample passes through the main deformation zone. Deformation heat can lead to pre-precipitation, forming a small amount of GPII zones during ECAP processing. Strain-induced excess vacancies make solute segregation along dislocations by the mechanism of nonequilibrium segregation. High density dislocations mainly accelerate the process of aging precipitation. Besides, dislocations also induce the competition between homogeneous precipitation and heterogeneous precipitation on dislocations due to the flow of solutes and vacancies towards dislocations. [ABSTRACT FROM AUTHOR]

Highlights: [•] The substructures in rotation-twinned T (Al20Cu2Mn3) particles were investigated. [•] A flattened hexagonal structural subunit with 20 atomic columns was proposed. [•] The stacking mode of these subunits at APB and TB were revealed. [•] The transition structures at twin domain junctions were unraveled. [ABSTRACT FROM AUTHOR]

Abstract: The deformation and fracture process in Al–Cu–Mg alloy were investigated by using the in situ straining transmission electron microscopy (TEM) method. Some major aspects of the fracture process, including dislocation emission and migration, thinning of dislocation free zone (DFZ), crack propagation (both in continuous and discontinuous manners) and slipping/twinning deformation, can be observed. The rod-like T dispersoids, which may increase the microcrack initiation sensitivity, also can effectively prevent the fast and continuous propagation of the crack. DFZ ahead of crack tip can be thinned in a mixed mode characterized by tearing and shear deformation, while nanovoids, which are typical characteristics in DFZ during discontinuous crack propagation, may originate from the enrichment of defects such as dislocations and vacancies. Deformation twinning at crack tip can slow down crack propagation and change crack propagation path, thus may be beneficial to the fracture toughness of the alloy. [Copyright &y& Elsevier]

Abstract: The high angle annular dark field scanning transmission electron microscopy (STEM-HAADF) tomography technique was applied to understand the three dimensional (3D) morphology and distribution characteristic of grain boundary precipitate (GBP) in peak-aged Al–Cu–Mg alloy. The results indicate that GBPs show both spherical and lenticular shapes and triangularly distribute along grain boundary (GB). Based on 3D observations from various directions, the values of GBP relevant parameters such as GBP size, center to center distance, number of GBPs per unit GB area and area fraction of GB covered by GBPs are further determined. The 3D method for GBP relevant parameter determination seems an effective way to avoid misunderstandings in the conventional two dimensional (2D) methods induced by GBP overlapping and projection effect as well as curved GB surface. [Copyright &y& Elsevier]

Abstract: The heterogeneous precipitation of the S (Al2CuMg) phase along dislocations is investigated using high-resolution transmission electron microscopy various configurations of the S precipitate group form according to the initial dislocation morphology and no more than two S variants coexist along a single dislocation line. The most favorable combination of two S variants is observed to be variants 1 and 4 (or variants 2 and 3), and the variant selection criterion for S precipitate with the classic orientation relationship is proved to be that the dislocation line direction lies in the habit plane of the precipitate. The contribution of S precipitate groups to strengthening is evaluated by comparing the difference in total system energy increment induced by precipitate loop and the equivalent number of Guinier–Preston–Bagaryatsky zones and discrete S particles during plastic deformation. The results show that the average size of the precipitate loops as well as other kinds of precipitate groups has an important influence on the final strengthening effect. By keeping the precipitate groups below a critical size and increasing their density, the strength and thermal stability of the alloy are expected to be improved. [Copyright &y& Elsevier]

Most laser clad surface layers on aluminium alloys consist of a hard carbide phase and an aluminium alloy matrix phase. The distribution of the carbide phase and the strength of the matrix phase are not always satisfactory. The paper describes a method to fabricate a metal matrix composite layer on Al 6061 by adopting the laser induced reaction synthesis technique. Powder of pure titanium, pure carbon, pure tungsten or tungsten carbide are mixed at various proportions and then pasted on an Al 6061 surface. Laser cladding with Ni–Al powders delivered by a coaxial nozzle onto the above pasted surface using a 2 kW Nd:YAG laser was carried out. During laser cladding, exothermic reactions of Ti–C, W–C and Ni–Al expedite the melting and alloying of the coatings. X-Ray diffraction and scanning electronic microscopy results show that TiC and WC phases were in situ synthesized during the cladding process and they appear in a Ni–Al matrix. The microstructure, hardness and pin-on-disk wear of the coatings are investigated and discussed. [Copyright &y& Elsevier]

Cryorolling (CR) can effectively avoid room temperature rolling cracking of high-strength aluminum alloy. In this work, solution-treated bulk Al 7085 alloy samples were subjected to CR and room temperature rolling (RTR), respectively. When the deformation was 70%, the RTR sample was broken, while the CR one still had no cracks when the deformation was up to 90%. Consequently, the microstructure and mechanical properties of the CR samples before and after ageing treatment were investigated. The results show that after the solution-treated bulk Al 7085 alloy samples were cryorolled, the yield strength (YS) and the ultimate tensile strength (UTS) were increased by 74% and 31%, respectively. However, the elongation to failure (EtF) was decreased. After the subsequent 100 °C/20 h peak ageing (PA) treatment, the YS and UTS can be further increased by 14% and 10%, respectively, and the EtF was increased by 39% compared with that of the CR samples. After PA treatment, nanosized GP zones and η′ precipitates were precipitated. Precipitation strengthening is the main contributor to the strength enhancement of CR samples after PA treatment, which can not only compensate for the reduction caused by the decrease in dislocation density but also improve the strength of the material. • Al 7085 alloy was processed by cryorolling and subsequent ageing treatment. • Strength and ductility of the cryorolled sample can be simultaneously improved after peak ageing treatment. • The aged sample contains nanosized GP zone and η′ precipitates. • Precipitation strengthening is the main contributor for strength enhancement of the cryolled + peak aged sample. [ABSTRACT FROM AUTHOR]

Cryorolling (CR) can effectively avoid room temperature rolling cracking of high-strength aluminum alloy. In this work, solution-treated bulk Al 7085 alloy samples were subjected to CR and room temperature rolling (RTR), respectively. When the deformation was 70%, the RTR sample was broken, while the CR one still had no cracks when the deformation was up to 90%. Consequently, the microstructure and mechanical properties of the CR samples before and after ageing treatment were investigated. The results show that after the solution-treated bulk Al 7085 alloy samples were cryorolled, the yield strength (YS) and the ultimate tensile strength (UTS) were increased by 74% and 31%, respectively. However, the elongation to failure (EtF) was decreased. After the subsequent 100 °C/20 h peak ageing (PA) treatment, the YS and UTS can be further increased by 14% and 10%, respectively, and the EtF was increased by 39% compared with that of the CR samples. After PA treatment, nanosized GP zones and η′ precipitates were precipitated. Precipitation strengthening is the main contributor to the strength enhancement of CR samples after PA treatment, which can not only compensate for the reduction caused by the decrease in dislocation density but also improve the strength of the material. • Al 7085 alloy was processed by cryorolling and subsequent ageing treatment. • Strength and ductility of the cryorolled sample can be simultaneously improved after peak ageing treatment. • The aged sample contains nanosized GP zone and η′ precipitates. • Precipitation strengthening is the main contributor for strength enhancement of the cryolled + peak aged sample. [ABSTRACT FROM AUTHOR]