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1. Green coupling of 3,5-diamino-1H-1,2,4-triazole into the azo compound.

Author

Xie, Mingzhen, Gong, Jiaxu, Zhou, Jie, Wang, Jiaheng, Cao, Yulong, Zhou, Tianlong, and Dai, Yatang

Subjects
*AZO compounds, *DOUBLE bonds, *VOLTAGE control, *NICKEL oxide, *OXIDATIVE coupling, *SODIUM hypochlorite
Abstract

[Display omitted] The nitrogen–nitrogen double bond between two molecules of 3,5-diamino-1 H -1,2,4-triazole is successfully constructed using a one-step electrochemical coupling method. The oxidation occurs selectively when the electrochemical parameters are properly adjusted to provide a yield of 45.77%. Subsequently, the oxidative coupling of this substrate with electrochemically generated hydroxy nickel oxide or sodium hypochlorite is verified. [ABSTRACT FROM AUTHOR]

Published
2023
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