1. Fabrication and characterization of low-shrinkage dental composites containing montmorillonite nanoclay
- Author
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Eduardo Moreira da Silva, Fernanda Pitta Ritto, Hélio Rodrigues Sampaio-Filho, Márcio Antônio Paraizo Borges, Alexandre Luiz Souto Borges, Oklahoma University, Universidade Federal Fluminense (UFF), Universidade Estadual Paulista (UNESP), IOPUC, and Rio de Janeiro State University
- Subjects
Dental composite ,Materials science ,Surface Properties ,Scanning electron microscope ,Cytotoxicity ,engineering.material ,Composite Resins ,Polymerization ,030207 dermatology & venereal diseases ,03 medical and health sciences ,chemistry.chemical_compound ,0302 clinical medicine ,Polymethacrylic Acids ,Flexural strength ,Elastic Modulus ,Filler (materials) ,Materials Testing ,Bisphenol A-Glycidyl Methacrylate ,Composite material ,General Dentistry ,Elastic modulus ,Shrinkage ,030206 dentistry ,Silicon Dioxide ,Polymerization shrinkage ,Montmorillonite ,chemistry ,Nanoclay ,Bentonite ,engineering ,Methacrylates ,Polymer-layered nanocomposites - Abstract
Made available in DSpace on 2022-04-29T08:45:33Z (GMT). No. of bitstreams: 0 Previous issue date: 2022-01-01 Dental composites are aesthetic materials widely used in Dentistry for replacing hard dental tissues lost due to caries or traumas. The aim of this study was to fabricate low-shrinkage dental composite charged with nanoclay fillers (montmorillonite Cloisite®—MMT) and evaluate their cytotoxicity and physicomechanical properties. Four dental composites were produced from the same organic matrix: Bis-GMA/TEGDMA (30 wt.%). The filler system was constituted of BaSi, SiO2, and MMT in the following concentrations (wt.%): 93.8/6.2/0, 89.1/5.9/5, 86.7/5.8/7.5, and 84.4/5.6/10 (E0: 0; E5: 5%; E7.5: 7.5%; E10: 10% of MMT nanoclays). The following properties were tested: in vitro cytotoxicity, flexural strength, elastic modulus, volumetric shrinkage, water sorption, water solubility, and hygroscopic expansion. Scanning electron microscopy was used to characterize composites’ topography. Data were analyzed by one-way ANOVA and Tukey’s HSD post hoc test (p < 0.05). MMT nanoclays did not affect the cytotoxicity. E5 and E7.5 groups showed a significant decrease in polymerization shrinkage while maintained the overall physicomechanical properties. The inclusion of 5 and 7.5 wt.% of MMT nanoclays allowed the fabrication of dental composites with low cytotoxicity and low polymerization shrinkage, without jeopardizing the overall behaviour of their physicomechanical properties (flexural strength, elastic modulus, water sorption, water solubility, and hygroscopic expansion). These aspects suggest that the usage of MMT nanoclays could be an effective strategy to formulate new dental composites with clinical applicability. Department of Operative Dentistry College of Dentistry Oklahoma University Analytical Laboratory of Restorative Biomaterials-LABiom-R Faculdade de Odontologia Universidade Federal Fluminense, Niterói Department of Dental Materials and Prosthodontics School of Dentistry São Paulo State University-UNESP, SP Department of Operative Dentistry IOPUC, Rua Marquês de São Vicente, 389-Gávea, RJ Department of Restorative Dentistry School of Dentistry Rio de Janeiro State University Department of Dental Materials and Prosthodontics School of Dentistry São Paulo State University-UNESP, SP
- Published
- 2021
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