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4. A fortuitously straightforward synthesis of 4-acetoxy-2-propyltetrahydrothiophene.

Author

Ma, Bianbian, Yang, Shaoxiang, Tao, Feiyan, Sun, Baoguo, Liu, Yongguo, and Tian, Hongyu

Subjects
*THIOPHENE derivatives, *PROPYL compounds, *EPOXIDATION, *METHANESULFONATES, *TRANSESTERIFICATION, *ACETATES, *HEPTANOL
Abstract

4-Acetoxy-2-propyltetrahydrothiophene was synthesised from 1-hepten-4-ol by a three-step route involving epoxidation and mesylation to 1,2-epoxy-4-heptyl mesylate and then reaction with thioacetate. An acetoxylated cyclic product was formed instead of the expected thioacetate, and a mechanism for its formation using an intramolecular transesterification is proposed. [ABSTRACT FROM AUTHOR]

Published
2015
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5. ChemInform Abstract: A Fortuitously Straightforward Synthesis of 4-Acetoxy-2-propyltetrahydrothiophene.

Author

Ma, Bianbian, Yang, Shaoxiang, Tao, Feiyan, Sun, Baoguo, Liu, Yongguo, and Tian, Hongyu

Subjects
*THIOPHENES, *CHEMICAL synthesis, *EPOXIDATION
Abstract

The title tetrahydrothiophene is synthesized by a three-step procedure involving a known epoxidation step of 1-hepten-4-ol and subsequent mesylation and acetoxylation-ring closing reactions. [ABSTRACT FROM AUTHOR]

Published
2016
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