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A walk-in type 222Rn calibration chamber of volume 22.7 m3, which has traceability to international standards, is established at the Centre for Advanced Research in Environmental Radioactivity, Mangalore University, India. It has a human–machine interface communication system, a programmable logic controller and sensor feedback circuit for controlling and data acquisition of relative humidity (RH) and temperature (T). An innovative method for the generation of desired 222Rn concentration (a few hundred Bq m−3 up to about 36 kBq m−3) using soil gas as a source was adopted. Leak rates of 222Rn from the chamber for the mixing fan ON and OFF conditions were determined to be 0.0011 and 0.00018 h−1 respectively. With the exhaust system fully turned on, the maximum clearance rate of the chamber was 0.58 ± 0.07 h−1. Excellent spatial uniformity in 222Rn concentration in the chamber was confirmed (with a mean value of relative standard deviation < 12%) through measurements at 23 locations using CR-39 film-based passive devices. Demonstration of calibration applications was performed using charcoal canister and PicoRad vials as the 222Rn adsorption devices. The study shows that gamma spectrometry is a convenient alternative approach to liquid scintillation analysis of PicoRad vials for 222Rn measurement. [ABSTRACT FROM AUTHOR]

Carbon content (%) measurement for determination of 14C specific activity (Bq kg−1C) in environmental matrices based on thermal oxidation of the sample using pyrolyser is discussed. The carbon content in biota samples (N = 574) of the tropical region were in the range 30–45%, 28–47%, 31–46%, 32–45%, 43–49%, and 37–50% with corresponding mean values of 38 ± 3.1%, 38 ± 4.4%, 41 ± 3.1%, 41 ± 3.7%, 46 ± 1.5%, and 44 ± 5.1% respectively for wild plant leaves, vegetables, fruits, cereals, wood, and fish samples. The present study shows that carbon content within the species and category (fruit, leaves, vegetables, etc.) of the sample may differ up to ~ 20% points. [ABSTRACT FROM AUTHOR]