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24 cycles Ti-TiN-Zr-ZrN soft-hard alternating multilayer film was deposited on TC11 titanium alloy by vacuum cathodic arc deposition method. The structure and performance of the multilayer film, especially wear and sand erosion resistance were investigated by various analytical methods including pin on disc wear tester, sand erosion tester, 3D surface topography instrument, scanning electron microscopy (SEM), X-ray diffraction(XRD), micro-hardness tester and scratch adhesion tester. The results indicate that the Vickers-hardness of the multilayer film with thickness of 5.8μm can reach up to 28.10GPa. The adhesive strength of these coatings can be as high as 56N. Wear rate of the multilayer coated alloy is one order of magnitude smaller than bare one, which decreased from 7.06×10-13 m3·N-1·m-1 to 3.03×10-14m3·N-1·m-1. Multilayer films can play the role in hindering the extension of cracks, and thus sand erosion properties of the TC11 titanium alloy substrates are improved.

The precipitation orientation of α phases in a Ti-55511 alloy during the heat treatment and the subsequent hot deformation is investigated. It is observed that the β grains prominently influence the precipitation process of α phases, i.e., for the neighbouring β grains without similar {110} pole, the precipitation orientation of grain boundary (GB) α phases (α GB) keep {0001}//{110}β1 or {0001}//{110}β2 to maintain the burgers orientation relationship (BOR) with the neighbouring β grains. For the neighbouring β grains with similar {110} pole, the {0001} poles of α GB phases precipitate parallel to this similar {110} pole and maintain BOR with the neighbouring β grains. For the neighbouring β grains with multiple similar {110} poles, the {0001} poles of α GB phases precipitate along these similar poles and maintain BOR with the neighbouring β grains. Besides, the interface instability nucleation and sympathetic nucleation are the main nucleation modes of the GB widmanstatten α phase (α WGB), which primarily precipitate within β grains with the similar orientation of α GB phases. The intracrystalline widmanstatten phase (α WI) precipitate in a single β grain with 12 precipitation orientations. The BOR between α WI phases and β grains is destroyed during the subsequent hot compressive deformation. • Precipitation orientation of α phases in Ti-55511 alloy during heat treatment plus hot deformation is studied. • Precipitation orientation of GB α phases maintains the BOR with neighbouring β grains along different poles. • Interface instability and sympathetic nucleations are the main nucleation modes of GB widmanstatten α phases. • The intracrystalline widmanstatten phases (α WI) precipitate in a single β grain with 12 precipitation orientations. • The BOR between α WI phases and β grains is destroyed during the subsequent hot compressive deformation. [ABSTRACT FROM AUTHOR]

Hot compression features of Ti-55511 alloy are investigated by high-temperature compression tests in α+β region. It is found that the flow stress and softening mechanisms are obviously influenced by deformation conditions. The true stress decreases with the reduced strain rate or the raised temperature. The spheroidization of α phase and dynamic recrystallization (DRX) of β phase easily occur at low temperatures such as 973, 1003 and 1033 K, while the dynamic recovery (DRV) of β phase mainly occurs at high temperatures such as 1063 K because of the transformation from α phase to β phase at relatively high temperatures A dislocation density-based constitutive model, which is associated with DRV, work hardening mechanisms and the spheroidization of α phases, is established and validated to describe flow behavior. The correlation coefficient (R) and average absolute relative error (AARE) of the established model are 0.9924 and 6.8%, respectively. 3D power dissipation efficiency maps and processing maps are established to determine the appropriate processing window, i.e., too low temperatures (lower than 973 K) or too high strain rates (higher than 1 s−1) easily induce flow instability. Therefore, the medium temperature (1003–1063 K) and the low strain rate (0.001–0.1 s−1) are applicable for thermal compression of the studied titanium alloy. • Hot compression features of Ti-55511 alloy is investigated by high-temperature compression tests in α+β region. • DRX easily occurs at low temperatures, while DRV mainly occurs at high temperatures. • A accurate dislocation density-based constitutive model considering the spheroidization of α phases is established. • The optimal forming temperature and strain rate are 1003–1063 K and 0.001–0.1 s−1. [ABSTRACT FROM AUTHOR]

Spheroidization and dynamic recrystallization (DRX) mechanisms of a Ti-55511 alloy during hot compression in α+β region is investigated. It is found that the spheroidization of lamellar α phases and DRX of β phases, which are obviously influenced by deformation conditions, are the main softening mechanisms. The spheroidization fraction of lamellar α phases first increases with the raised temperature or strain rate. However, the spheroidization fraction of lamellar α phases begins to drop at about 700 °C as the strain rate is higher than 0.01 s−1, and the maximum spheroidization fraction of lamellar α phase is about 2.3%. This phenomenon is attributed to the Implanting-Mechanism, which is induced by the common or close orientation relationships of the spheroidized and equiaxed α phases, as well as few dislocations between the spheroidized and equiaxed α phases. Contrarily, the lamellar α phases are obstructed from equiaxed α phases by a mass of dislocations. Additionally, the DRX degree of β phases increases with the reduced temperature or the raised strain rate. • Spheroidization and DRX mechanisms of a Ti-55511 alloy during hot compression in α+β region is investigated. • Spheroidization fraction of lamellar α phase first increases then drops with the raised strain rate. • The maximum spheroidization fraction of lamellar α phase is about 2.3% near 700 °C and 0.01 s−1. • Implanting-Mechanism, induced by the close orientation relationships of spheroidized and equiaxed α phases, is proposed. • The DRX extent of β phases increases with the reduced temperature and raised strain rate. [ABSTRACT FROM AUTHOR]