Search

A low-carbon micro-alloyed (LCMA) steel with a body-centered cubic (bcc) crystal structure suitable for extremely low temperatures was developed by overcoming the intrinsic ductile-to-brittle transition in bcc alloys at cryogenic temperatures. The excellent cryogenic-to-ambient impact toughness in the LCMA rolled plate results from its heterogeneous microstructure, which gradually changes from bamboo-like ultrafine grains (∼ 1.1 μm) on the surface to relatively equiaxed coarse grains in the core (∼ 3.4 μm), accompanied by a distinct texture gradient variation. The heterostructured LCMA steel displays a cryogenic impact toughness of ∼200 J/cm2 at 77 K, which is 24 times higher than the coarse-grained LCMA steel. Such high impact toughness of heterostructured LCMA arises from the coordinated deformation mechanisms over different length-scales coupled with delamination toughening. At 77 K, the heterostructured steel plate deforms by forming cellular sub-structures at the core to the surface, which refines the microstructure and promotes hetero-deformation induced (HDI) hardening to improve intrinsic toughening. Moreover, the subsequent delamination process induces extrinsic toughening by shielding and blunting the cracks, with the local plane-stress conditions induced by delamination promoting ductile fracture of the coarse grains in the core regions. This low alloy steel with its heterogeneous microstructure exhibits extraordinary impact toughness at cryogenic temperatures highlights the possibility of materials design strategies for sustainable development.

The current study proposes a comparison of the plastic anisotropy through the experimental determination of Lankford coefficient (R) via tensile tests for Al-1050, Al-2024 and Al-7075 aluminium alloys after cold rolling with 50% of thickness reduction, accumulative roll bonding (ARB), and cross ARB (CARB) processing up to 2 cycles. The average normal anisotropy ($\bar R$Rˉ) and planar anisotropy (ΔR) parameters have been used to describe the formability of the alloys. The R values were found in the range of 0.60–0.80, 0.18–0.51 and 0.20–0.47 for Al-1050, Al-2024 and Al-7075 alloys, respectively. The results demonstrated that the formability of the three alloys was improved with increasing the ARB and CARB cycles. Regarding the Al-based alloys, the Al-1050 alloy exhibits the best formability, followed by Al-7075 and then Al-2024 alloys. In the case of Al-1050 and Al-2024 alloys, CARB processing for two cycles gives the best combination of high strength and good formability (high $\bar R$Rˉ and low ΔR). However, for the Al-7075 alloy, the best strength and good reduction in the planar anisotropy were obtained after ARB processing for two cycles. [ABSTRACT FROM AUTHOR]

Copyright of Automobile Technology & Material is the property of Automobile Technology & Material Editorial Office and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Mg-6Zn-0.5Mn as a medical magnesium alloy has good biomechanical properties and corrosion resistance, but as a fracture internal-fixation material, its strength, toughness, and corrosion resistance still need to be improved. In this paper, the element Sr, having good biocompatibility, is used as an alloy element. The effects of different Sr contents (0 wt.%, 0.3 wt.%, 0.6 wt.%, 0.9 wt.%, and 1.2 wt.%) on the microstructure, strength, toughness, and corrosion resistance of rolled Mg-6Zn-0.5Mn alloy were studied. The results are as follows. Sr can influence the recrystallization process. When the Sr content is 0.3 wt.% and 0.6 wt.%, the alloy matrix exhibits both non-recrystallized regions and fine recrystallized regions. When the Sr content reaches 0.9 wt.%, the non-recrystallized region decreases significantly, and the fine recrystallized grains develop into equiaxed grains. With the increase of Sr content, the elongation of the alloy decreases. At a content of 0.9 wt.%, the corrosion resistance reaches its optimum value, with an average corrosion rate of 0.75828 mm/y. [ABSTRACT FROM AUTHOR]

In this research paper, the factors impacting electrical conductivity of the flexible graphite foils (GFs) produced by different forming processes, namely, either by rolling or pressing, were studied. The relationship between electrical conductivity and texture and structure that formed when producing the material was examined. Correlation was determined between the texture sharpness and anisotropy of electrical conductivity, as well as the extent of impact from the substructural characteristics on the properties' values. Besides, it was demonstrated that the higher values of micro-strains, as well as the secondary phase substructure, reduced conductivity in foils. Electrical conductivity calculation was optimized for different directions in foils using the Kearns texture parameters and taking into consideration the foil structural characteristics. [ABSTRACT FROM AUTHOR]

At Štore Steel Ltd., continuously cast billets (180 mm × 180 mm) are reheated and rolled after cooling to room temperature. Hot-rolled bars are controlled as they cool to room temperature in specially designed cooling chambers, minimizing residual stresses and the development of pre-existing surface and internal defects. The bar ends can be additionally covered with insulating material. The cooled, rolled bars undergo examination using automated control lines to detect surface and internal defects, which primarily originate from the casting process. Internal defects are identified using ultrasonic testing. Between January 2022 and June 2023, 1550.0 tons of 61SiCr7 rolled bars, with diameters ranging from 53 mm to 72 mm and lengths from 7010 mm to 7955 mm, were examined using ultrasonic testing. The scrap was 109.6 tons (7.07 %). After collecting data on chemical composition (C, Si, Mn, Cr, Mo, Ni content), the casting process (casting temperature, cooling water pressure and flow in the first, second, and third zones of secondary cooling, as well as the temperature difference between input and output mould cooling water), and rolled bar geometry (diameter, length), scrap modelling after ultrasonic testing was carried using genetic programming. The genetic programming model suggested reducing the length of the rolled bar. Due to length multiplication, it was possible to reduce the rolled bar length from the initial lengths of 7010-7955 mm to the current lengths of 4558-6720 mm in June 2023. Based on this adjustment, a new production of rolled bars was established. By August 2024, 1251.9 tons of 61SiCr7 rolled bars were produced with the mentioned length adjustments. These rolled bars were subsequently examined using ultrasonic testing. The scrap was reduced by nearly 14 times, amounting to only 8.1 tons (0.64 %). [ABSTRACT FROM AUTHOR]

Minimizing geometric error in the bending of large sheets remains a challenging endeavor in the industrial environment. This specific industrial operation is characterized by protracted cycles and limited batch sizes. Coupled with extended cycle times, the process involves a diverse range of dimensions and materials. Given these operational complexities, conducting practical experimentation for data extraction and control of industrial process parameters proves to be unfeasible. To gain insights into the process, finite element models serve as invaluable tools for simulating industrial processes for reducing experimental cost. Consequently, the primary objective of this research endeavor is to develop an intelligent finite element model capable of providing operators with pertinent information regarding the optimal range of key parameters to mitigate geometric error in the bending of large sheets. This prediction model is based on response surface method to predict the bending diameter of the pipe taking into account three main process parameters: the plate thickness, the length, and the roll displacement. These results present promising prospects for the automation of the industrial process because the average geometric error in curvature is recorded at 0.97%, thereby meeting the stringent industrial requirement for achieving such bending with minimal equivalent plastic deformation. [ABSTRACT FROM AUTHOR]

Heterogeneous metallic structures constitute a novel class of materials with excellent mechanical properties. However, the existing process for obtaining heterostructures from a single material does not meet large-scale industrial requirements. In this study, a pure copper heterostructured laminate (HSL) composed of a surface elongated-grain layer and a central equiaxed-grain layer was fabricated by rolling bonding and annealing. To study the effect of the interface on the mechanical properties of gradient-structured materials, both laminate metal composite (LMC) and non-composite laminate (NCL) were fabricated by cold-rolling pretreatment of the center layer (60% reduction) and cold-rolling bonding of the whole blank (67% reduction). Then, the HSL was obtained by controlling the post-annealing regimes, the microstructure of each layer was optimized, and a larger degree of microstructural heterogeneities, such as grain size, misorientation angle, and grain orientation, was obtained, which resulted in obvious mechanical differences. Tensile tests of the HSL, surface layer, center layer, and NCL specimens revealed that the HSL annealed at 300 °C for 1 h had a significantly higher strength than the center layer and a higher elongation than the surface layer. The HSL had a tensile strength and elongation at fracture of 278.08 MPa and 46.2%, respectively, indicating a good balance of strength and plasticity. The improved properties were primarily attributed to the strengthening or strain hardening due to the inhomogeneous deformation of the heterogeneous layers in the laminate and the mutual constraint acquired by the distinct layers with strong mechanical differences. The HSL had an interfacial bonding strength of 178.5 MPa, which played a vital role in the coordinated deformation of the heterogeneous layers. This study proposes an HSL design method that effectively simplifies the process of obtaining heterostructures in homogeneous materials by controlling the cumulative deformation of the surface and center layers. [ABSTRACT FROM AUTHOR]

The article presents a theoretical study of kinematic pairs known as «rolling pairs» used in many areas of mechanical engineering, in particular, mechanisms. The research concerns such bodies (links) as geometric tori, which are well-known bodies of rotation. From the geometric kinematics, new representations of the mechanical motions of a torus in a «torus-torus» connection are described without the reasons that cause this motion. Two options for connecting two tori are analyzed: the axes of the tori are parallel and perpendicular. By analogy, the analysis of kinematic pairs of this type expands the elements of kinematic pairs theory and allows developing their new variants in many mechanisms used in various fields of mechanical engineering.

Abstract Heterogeneous metallic structures constitute a novel class of materials with excellent mechanical properties. However, the existing process for obtaining heterostructures from a single material does not meet large-scale industrial requirements. In this study, a pure copper heterostructured laminate (HSL) composed of a surface elongated-grain layer and a central equiaxed-grain layer was fabricated by rolling bonding and annealing. To study the effect of the interface on the mechanical properties of gradient-structured materials, both laminate metal composite (LMC) and non-composite laminate (NCL) were fabricated by cold-rolling pretreatment of the center layer (60% reduction) and cold-rolling bonding of the whole blank (67% reduction). Then, the HSL was obtained by controlling the post-annealing regimes, the microstructure of each layer was optimized, and a larger degree of microstructural heterogeneities, such as grain size, misorientation angle, and grain orientation, was obtained, which resulted in obvious mechanical differences. Tensile tests of the HSL, surface layer, center layer, and NCL specimens revealed that the HSL annealed at 300 °C for 1 h had a significantly higher strength than the center layer and a higher elongation than the surface layer. The HSL had a tensile strength and elongation at fracture of 278.08 MPa and 46.2%, respectively, indicating a good balance of strength and plasticity. The improved properties were primarily attributed to the strengthening or strain hardening due to the inhomogeneous deformation of the heterogeneous layers in the laminate and the mutual constraint acquired by the distinct layers with strong mechanical differences. The HSL had an interfacial bonding strength of 178.5 MPa, which played a vital role in the coordinated deformation of the heterogeneous layers. This study proposes an HSL design method that effectively simplifies the process of obtaining heterostructures in homogeneous materials by controlling the cumulative deformation of the surface and center layers.

This work investigated the effect of rolling temperature (25–800 °C) on rolling-texture development and sheet formability of pure Ti. The rolling temperature significantly affected the development of the typical transverse-direction (TD)-split basal texture in pure Ti sheet by altering the tilting angle of (0001) basal poles. Notably, a normal-direction (ND) basal texture, where the tilting angle of (0001) basal poles was approximately 0°, developed at an intermediate rolling temperature of 400 °C. This result is remarkable because the ND basal texture is rare in pure Ti. Formation of this unusual ND basal texture was attributed to significant activation of basal slip. In contrast, a typical TD-split basal texture was dominant at the other rolling temperatures. Formation of this typical texture was attributed to pyramidal slip. After subsequent recrystallization annealing, sheet formability was examined. Despite their different textures, the sheets previously rolled at the different rolling temperatures showed similar formability. This similarity occurred because any given texture could not simultaneously provide in-plane stretching uniformity and thinning capability during sheet forming. The present study suggests an important guidance for modifying texture of pure Ti sheets to effectively increase their formability.

In order to develop the aluminum sheets suitable for the twin-belt continuous casting and direct rolling, the composition optimization of Al-Mg-Mn alloys evolved from AA5052 (Al-2.5 Mg) alloy was firstly carried out via the synergy between the PANDAT software and the micro–hardness test. Subsequently, the influence of Er and Zr on the microstructure and mechanical properties of the optimized Al-Mg-Mn sheet (Al-1.5 Mg-0.8Mn) was investigated in this work. The results showed that the tensile properties of Al-1.5 Mg-0.8Mn sheets processed by the rolling and the subsequent annealing were improved by the co-addition of the Zr and Er. The optimized tensile properties (UTS: 320.5 MPa; YS: 231.6 MPa; E.L.: 6.75%) were achieved in Al-1.5 Mg-0.8Mn sheets modified by 0.2 wt.% Zr and 0.3 wt.% Er, which is attributed to the finest fibrous grains, the fine, homogeneously distributed residual Al6Mn, Al3Zr and Al3(Zr, Er) second phases and more nano-sized Al3(Zr, Er) precipitations. [ABSTRACT FROM AUTHOR]

The 7046 aluminum alloy possesses a favorable fatigue property, corrosion resistance and weldability, but its moderate strength and plasticity limit its wider application and development. In the present study, severe plastic deformation (SPD) was applied prior to T6 treatment to significantly enhance the strength and toughness of the 7046 aluminum alloy. The results show that the alloy processed by four passes of equal channel angular pressing (ECAP) at 300 °C prior to T6 treatment exhibits an excellent mechanical performance, achieving an ultimate tensile strength (UTS) and elongation (EL) of 485 MPa and 19%, respectively, which are 18.6% and 375% higher than that of the T6 alloy. The mechanical properties of the alloy are further improved by an additional room temperature (RT) rolling process, resulting in a UTS of 508 MPa and EL of 23.4%, respectively. The increased presence of η′ and Al6Mn phases in the 300°C4P-R80%-T6 and 300°C4P-T6 alloys contributes to a strengthening and toughening enhancement in the SPD-processed T6 alloy. The findings from this work may shed new insights into enhancing the 7046 aluminum alloy. [ABSTRACT FROM AUTHOR]

Rolling plays an important role in shaping the characteristic quality of black tea. However, the dynamic alterations in volatile compounds during the rolling process remain unclear, which hampers the quality control of black tea. In this study, the dynamic changes of volatile compounds in Congou black tea throughout the rolling process were explored by a combination of GC-E-Nose and GC-MS analysis. The results of PCA and PLS-DA by GC-E-Nose revealed significant alterations in the volatile profiles, particularly at the 15-min rolling stage. A total of 82 volatile compounds including eight categories were identified in Congou black tea during the rolling process. The most abundant volatiles were aldehydes, alcohols, and esters. Through the integration of variable importance in the projection >1 and p < 0.05, 21 volatile compounds were pinpointed as pivotal volatiles responsible for distinguishing diverse rolling processes. According to their pathways, glycoside-derived volatiles (GDVs) (such as linalool and geraniol) and fatty acid-derived volatiles (FADVs) (such as (Z)-2-hexen-1-ol and hexanal) highlighted the pivotal role in the formation of the aroma of black tea during rolling process. GDVs, characterized by floral, honeyed, and fruity aromas, reached the lowest point at 35-min rolling and subsequently rebounded. FADVs exhibited an ascending trajectory during the initial 15-min rolling, followed by a downward trend. These findings provide invaluable insights into the aroma evolution during the rolling stage, offering strategies for enhancing the aroma quality of Congou black tea. [ABSTRACT FROM AUTHOR]

Recent losses in the abundance and diversity of arthropods have been documented in many regions and ecosystems. In grasslands, such insect declines are largely attributed to land use, including modern machinery and mowing regimes. However, the effects of different mowing techniques on arthropods remain poorly understood. Using 11 years of data from 111 agricultural grassland plots across Germany, we analyzed the influence of various grassland management variables on the abundance and abundance‐accounted species richness of four arthropod orders: Araneae, Coleoptera, Hemiptera, and Orthoptera. The analysis focused on detailed mowing information, for example, days after mowing and mower type, and compared their effect with other aspects of grassland management, that is, rolling, leveling, fertilization, and grazing. We found strong negative effects of mowing on all four arthropod orders, with arthropod abundance being lowest directly after mowing and steadily increasing to three to seven times the abundance after 100 days post‐mowing. Likewise, Hemiptera and Coleoptera species richness was 30% higher 100 days after mowing. Mower width showed a positive effect on Orthoptera abundance, but not on the other arthropods. Arthropod abundance and Coleoptera species richness were lowest when a mulcher was used compared to rotary or bar mowers. In addition to mowing, intensive grazing negatively affected Orthoptera abundance but not the other orders. Mowing represents a highly disturbing and iterative stressor with negative effects on arthropod abundance and diversity, likely contributed by mowing‐induced mortality and habitat alteration. While modifications of mowing techniques such as mower type or mowing height and width may help to reduce the negative impact of mowing on arthropods, our results show that mowing itself has the most substantial negative effect. Based on our results, we suggest that reduced mowing frequency, omission of mowing in parts of the grassland (refuges), or extensive grazing instead of mowing have the greatest potential to promote arthropod populations. [ABSTRACT FROM AUTHOR]

Introduction: The availability of high-quality gilthead seabream (Sparus aurata) larvae in larviculture represents a major bottleneck to the aquaculture. This challenge can be compounded by losses resulting from the emergence of a clinical disorder's symptomatology. In this study, the observed syndrome included a rotated positioning of the larval sagittal plane and in most cases leading eventually to death. Methods: Herein, we examined using amplicon sequencing of the 16S rDNA the bacterial communities associated with S. aurata larvae at different conditions (including both fish with no evidence of the syndrome and fish with syndrome) during the early developmental stages along with the contribution of rearing water, organic matter and provided feed in the microbiota during an experiment of 18 days. Results: Over the development of larvae, differences were observed in the bacterial composition between healthy and symptomatic larvae as well as between components of the system. A remarkable presence of members of the Psychrobacter genus was observed in symptomatic larvaewith a significant increase at 18dph. The healthy larvae harbor different bacterial profile with a dominance of Vibrio and Bacillus genera during 3-8dph, various members of Alphaproteobacteria during 11-14dph and Marinifilum at 18dph. The rearing water showed a different bacterial profile compared to the other components, with a slight effect of healthy larvae at 3-8dph. The bacteriome of feeds provided during the rearing of larvae was found to be diverse. Chlorella was mainly dominated by members of Firmicutes, while Rotifer and Artemia were mainly dominated bymembers of Proteobacteria including different species of Psychrobacter. At 18dph, Artemia feed seems to affect the symptomatic larvae bacteriome, where it enhanced the presence of Psychrobacter spp. Discussion: Interestingly, the comparative network analysis at 18dph indicated that the bacterial associations in symptomatic larvae were primarily driven by members of the Psychrobacter genus. While various phyla contributed to bacterial associations in healthy larvae with different frequencies including mainly members of Proteobacteria, Bacteroidota and Firmicutes phyla. Finally, the Gammaproteobacteria/Alphaproteobacteria ratio was found to be related to the health condition of larvae. This study provides valuable informationwhich can be used as indicators for monitoring the health status of S. aurata larvae. [ABSTRACT FROM AUTHOR]

The steel industry represents a sector of great importance in the production chain, being directly related to the economic development of the world. The straightening process, an important phenomenon of plastic deformation during steel production can bring changes in the results of mechanical properties. The goal of this study is to analyze the interaction between the variables involved in the natural strain ageing, straightening (manual and mechanical) and in the chemical composition (low and medium carbon steels) of the wire rod, being the variation of the mechanical properties - through the tensile test – and microstructural – from the microstructural characterization – the analysis parameters. The results indicate a trend towards an increase in the yield and resistance limits of the materials that were submitted to the straightening and strain aging process, and it is possible to notice the pattern, from the contour and response surface graphs, that the higher the levels of straightening and percentage of carbon, the higher the values of yield strength and resistance.

The present investigation systematically explores the effect of a minor addition of silicon on the microstructure, texture, and mechanical properties of FCC CrFeNi medium entropy alloy during rolling at room temperature. The addition of 2 at% Si in CrFeNi alloy results in the reduction of stacking fault energy from 22.4 mJ/m2 for CrFeNi to 18.6 mJ/m2 for (CrFeNi)98Si2 alloy. Bulk texture analysis reveals the presence of Brass and Goss texture components in the 90 % rolled samples. Microtextural study reveals that in CrFeNi and (CrFeNi)98Si2 alloy, Goss-orientated grains exhibit greater stability throughout the deformation compared to Cu-oriented grains. In addition to twinning, profuse shear banding was observed in both alloys at 90 % rolling reduction. The mechanical properties of homogenised (CrFeNi)98Si2 alloy demonstrate the enhanced combination of yield strength and hardness due to improved solid solution strengthening and dislocation strengthening accompanied by a marginal decrease in ductility due to twinning-induced strain hardening. While in 90 % rolled CrFeNi and (CrFeNi)98Si2 alloy, both yield strength and ultimate tensile strength increase drastically due to enhanced solid solution and dislocation strengthening though with a significant decrease in ductility.

In an industrial context, selecting an appropriate crystal plasticity (CP) model that balances efficiency and accuracy when modelling deformation texture (DT) is crucial. This study compared DTs in IF-steel after undergoing cold rolling reductions using different CP models for two input texture scenarios. Three mean-field (MFCP) models were utilised in their most basic configurations, without considering grain fragmentation or strain hardening, in addition to a dislocation-density-based full-field (FFCP) model. The study quantitatively compared the results from the MFCP models with those from the FFCP models. Furthermore, all CP model results were compared with experimental textures obtained from electron back-scatter diffraction (EBSD) experiments. The findings revealed that certain MFCP models could predict deformation textures as accurately as the FFCP models. Notably, one of the MFCP models exhibited a superior match with experimental textures for cold rolling reductions at 60%. Upon closer examination of specific crystallographic components, it was observed that MFCP models tended to predict a stronger {111}〈211〉 component, while the full-field model favours the {111}〈011〉 component. It is crucial to emphasise the importance of quantifying the texture within individual grains when assessing the macro-level deformation texture in rolling simulations.

Automobiles are the inevitable mode of transportation. However, increasing fuel prices and carbon dioxide emissions are posing a serious threat to automobile users and the environment. Thus, the development of new lightweight materials has been a key area of research. Magnesium-based commercial alloys (AZ and ZK series alloys) are the lightest among all structural metals. However, there is still a question about the replacement of Aluminum-based alloys due to HCP crystal structure. In this connection, MgAlCaMn (AXM) Mg alloy can be a choice as an alternative to the existing Mg-based commercial alloys for structural applications. It contains (Al, Mg)2Ca, Al2Ca, Mg2Ca, and Al8Mn5 as the secondary phases, contributing to the microstructural refinement and property enhancement. However, the formation of those precipitates depends on the amount of Al, Ca, and Mn, especially, the Ca/Al ratio. In addition, the secondary processes influence the grain refinement and property enhancement of texture modifications. Hence, this review article focuses on elaborating on the significance of the Ca/Al ratio for the precipitate formation, secondary process, and texture modifications. The co-segregation behavior of other micro-alloying elements like Cerium, Lanthanum, and Zinc in AXM Mg alloy systems has also been discussed for property enhancement.

The production of seamless hot‑deformed pipes from martensitic stainless steel with a high chromium content, used under the constant influence of aggressive environments, involves overcoming a series of technological challenges. These challenges are due to the metal’s structural features, such as relatively low plasticity, a narrow temperature range for hot deformation, a tendency to defect formation during rolling, and more intense wear on the rolling tools. The article discusses the main stages of research work on mastering the technology of producing seamless hot‑rolled pipes from stainless steel grade L80 type 13Cr at OJSC “BSW – Management Company of Holding “BMC”. It presents the results and complexities of mastering the technology for producing seamless stainless steel pipes, analyzes the results aimed at reducing the cost of finished products by increasing the durability of piercing mandrels, the resistance of disc saws for cutting blanks, eliminating metal adhesion to the piercing mill’s Dishar discs, increasing the productivity of the rolling line and heat treatment process.

Sunflower (Helianthus annuus L.), a vital crop for global vegetable oil production, encounters sustainability challenges in its cultivation. This study assesses the effects of incorporating a winter cover crop (CC), Avena sativa (L.), on the subsequent growth of sunflower crops and the vitality of their rhizosphere microbial communities over a two-year period. It examines the impact of two methods for suppressing winter CC--chemical suppression using glyphosate and mechanical suppression via rolling--both with and without the addition of phosphorus (P) starter fertilizer. These approaches are evaluated in comparison to the regional best management practices for sunflower cultivation, which involve a preparatory chemical fallow period and the subsequent application of starter P fertilizer. The methodology utilized Illumina sequencing for the analysis of rhizosphere bacterial 16S rRNA genes and fungal internal transcribed spacer (ITS) amplicons. Findings indicate a significant improvement (9-37%) in sunflower growth parameters (plant height, stem diameter, head diameter, and head dry weight) when cultivated after glyphosate-suppressed winter CC compared to the chemical fallows. Conversely, rolling of winter CC generally negatively affected sunflower growth. Rhizosphere bacterial communities following chemical suppression of winter CC showed greater Pielou's evenness, indicating a uniform distribution of species. In general, this treatment had more detrimental effects on beneficial sunflower rhizosphere bacteria such as Hymenobacter and Pseudarthrobacter than rolling of the winter CC, suggesting that the overall effect on sunflower growth may be mitigated by the redundancy within the bacterial community. As for fungal diversity, measured by the Chao-1 index, it increased in sunflowers planted after winter CC and receiving P fertilization, underscoring nutrient management's role in microbial community structure. Significant positive correlations between fungal diversity and sunflower growth parameters at the reproductive stage were observed (r = 0.41-0.72; p < 0.05), highlighting the role of fungal communities in plant fitness. The study underscores the positive effects of winter CC inclusion and management for enhancing sunflower cultivation while promoting beneficial microbes in the crop's rhizosphere. We advocate for strategic winter CC species selection, optimization of mechanical suppression techniques, and tailored phosphorus fertilization of sunflower to foster sustainable agriculture. [ABSTRACT FROM AUTHOR]

The aim of the work is to develop a physical and mathematical model of the process under complex asymmetric loading in conditions of single-area and two-area deformation zone during plastic processing of medium-thickness strips. The stress state in case of loss of stability during rolling of strips of medium thickness was investigated. The patterns of changes in the stress state of the strip under conditions of reach of the limiting deformation zone, as well as the effects of plastic shaping determined by a decrease in contact stresses under conditions of increasing deformation loading, are revealed. The described method is a visual approach to assessing the stress state of a plastic medium under conditions of complex interaction and asymmetric loading. [ABSTRACT FROM AUTHOR]

• Role of Ca/Al ratio in AXM Mg alloy systems for the mechanical behavior. • Influence of amount of alloying elements like Al, Ca, and Mn on the formation of precipitation in AXM Mg alloy systems. • Significance of precipitate formation in monoatomic layer G.P zones for enhancing both strength and ductility. • Importance of co-segregation behavior to enhance the stretch formability of the AXM Mg alloy systems. Automobiles are the inevitable mode of transportation. However, increasing fuel prices and carbon dioxide emissions are posing a serious threat to automobile users and the environment. Thus, the development of new lightweight materials has been a key area of research. Magnesium-based commercial alloys (AZ and ZK series alloys) are the lightest among all structural metals. However, there is still a question about the replacement of Aluminum-based alloys due to HCP crystal structure. In this connection, Mg Al Ca Mn (AXM) Mg alloy can be a choice as an alternative to the existing Mg-based commercial alloys for structural applications. It contains (Al, Mg) 2 Ca, Al 2 Ca, Mg 2 Ca, and Al 8 Mn 5 as the secondary phases, contributing to the microstructural refinement and property enhancement. However, the formation of those precipitates depends on the amount of Al, Ca, and Mn, especially, the Ca/Al ratio. In addition, the secondary processes influence the grain refinement and property enhancement of texture modifications. Hence, this review article focuses on elaborating on the significance of the Ca/Al ratio for the precipitate formation, secondary process, and texture modifications. The co-segregation behavior of other micro-alloying elements like Cerium, Lanthanum, and Zinc in AXM Mg alloy systems has also been discussed for property enhancement. [Display omitted] [ABSTRACT FROM AUTHOR]

In this study, intermediate rolling processes, such as warm rolling (WR) before aging, hot rolling (HR) before quenching, and a combination of these processes, were used to process 7055 and 7075 alloys with solution and aging treatment. Intermediate rolling did not change the grain structure of 7055 alloy, but it refined the grain of 7075 alloy. Moreover, it led to the formation of dislocations in the alloys, thereby promoting the precipitation of η′ phases during subsequent aging. The low cooling rate resulted in the formation of η phases with large size and high-volume fraction in HR 7055 alloy. However, intermediate rolling did not seriously coarsen the precipitates of 7075 alloy due to its low Zn + Mg content, low Zn/Mg ratio, and high density of Cr-rich phases. WR before aging enhanced the strength of 7055 alloy, but other intermediate rolling processes seriously deteriorated its mechanical properties. The strength of 7075 alloy could be enhanced by all intermediate rolling processes, and the dislocation strengthening effect in 7075 alloy was more significant than its precipitation strengthening. [ABSTRACT FROM AUTHOR]

Copyright of Journal of Central South University is the property of Springer Nature and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Every year, almost 4 million patients received medical care for knee osteoarthritis. Osteoarthritis involves progressive deterioration or degenerative changes in the cartilage, leading to inflammation and pain as the bones and ligaments are affected. To enhance treatment and surgical outcomes, various studies analyzing the biomechanics of the human skeletal system by fabricating simulated bones, particularly those reflecting the characteristics of patients with knee osteoarthritis, are underway. In this study, we fabricated replicated bones that mirror the bone characteristics of patients with knee osteoarthritis and developed a skeletal model that mimics the actual movement of the knee. To create patient-specific replicated bones, models were extracted from computerized tomography (CT) scans of knee osteoarthritis patients. Utilizing 3D printing technology, we replicated the femur and tibia, which bear the weight of the body and support movement, and manufactured cartilage capable of absorbing and dispersing the impact of knee joint loads using flexible polymers. Furthermore, to implement knee movement in the skeletal model, we developed artificial muscles based on shape memory alloys (SMAs) and used them to mimic the rolling, sliding, and spinning motions of knee flexion. The knee movement was investigated by changing the SMA spring's position, the number of coils, and the applied voltage. Additionally, we developed a knee-joint-mimicking system to analyze the movement of the femur. The proposed artificial-skeletal-model-based knee-joint-mimicking system appears to be applicable for analyzing skeletal models of knee patients and developing surgical simulation equipment for artificial joint replacement surgery. [ABSTRACT FROM AUTHOR]

During the sea launch of a launch vehicle in low sea state, a rolling phenomenon of the launch vehicle has been observed. In rough sea conditions, launch may failure. This study utilizes dimensionality reduction-driven spatial system projection methods and virtual prototype modeling technology to reveal that the launch vehicle's rolling is caused by differences in the motion paths of the center of mass. Additionally, during the prelaunch stage, the variation in the trajectory of the launch vehicle's center of mass caused by the rolling and pitching motions of the transportation vessel has a significant impact on the roll motion of the launch vehicle. The motion in other degrees of freedom has minimal influence on the launch vehicle's rolling. The minimum rocket rolling occurs when the dynamic coefficient of friction of the launchpad–launch vehicle contact is 0.05, and the dynamic coefficient of friction of the adapters and guideways is 0.4. The conclusions provide a theoretical foundation for optimizing the sea launch system and enhancing the reliability of sea launch in rough sea conditions. [ABSTRACT FROM AUTHOR]

The application of biodegradable Zn-based vascular alloy stents proves to be an ideal solution for addressing cardiovascular diseases. In this work, a Zn-0.8Li-0.4Mn alloy is designed with no biological toxicity, and optimized microstructure and properties through a hot rolling process. The resulting alloy shows a combined enhancement in both mechanical strength and resistance to corrosion. Noteworthy is the effectiveness of rolling deformation in refining alloy grains, promoting the uniform distribution of precipitates, and enhancing strength and ductility. After 90 % deformation, the Zn-0.8Li-0.4Mn alloy demonstrates excellent mechanical properties, with peak yield strength and ultimate tensile strength of 406.0 MPa and 449.1 MPa, respectively, and elongation exceeding 75 %. Corrosion studies indicate a relationship between the degradation rate increase and grain refinement, with the primary corrosion mechanism being pitting corrosion. The corrosion product Li2CO3 exhibits high stability, providing a passivation effect on the alloy surface. This work establishes a theoretical foundation and practical reference for the development of new biodegradable Zn-based alloys tailored for biomedical applications.

Micro-alloyed Zn–Mg alloys have attracted extensive attention in the field of medical implant due to their excellent biosafety and moderate degradation rate. The low Mg content could compromise the improvement of strength, therefore, the appropriate rolling process was investigated to enchance strength and inhibit strain softening behavior of Zn-0.06 Mg alloy. The observed changes in microstructures, mechanical properties, and strain softening behavior of the as-cast alloy after three different rolling processing were consistent with those exhibited by the solid-solution alloy. The cold rolled alloys showed excellent strength due to their small average grain size and high initial dislocation density, however, they also exhibited noticeable strain softening behavior. Hot rolling processing can result in coarsening of the grains, reduction in dislocation density and introducing a large number of twins, which inhibited strain softening behavior but also leaded to a decrease in the strength compared with cold rolling. The hot-cold rolling processing can induce the formation of heterostructure, wherein coarse grains encircled fine grains, while high density dislocation regions and low density dislocation regions were uniformly distributed, which effectively inhibited strain softening behavior on the basis of maintaining good mechanical properties.

In this work, Mg–7Y–5Zn-0.1V alloys were prepared by 1-D forging followed by multi-step rolling. The rolling reduction dependence of the microstructure and tensile properties of the Mg–7Y–5Zn-0.1V alloy was experimentally investigated. The results indicated that the bimodal matrix microstructures are formed, and the fibrous 18R long-period stacking ordered (LPSO) phase and kinked 14H-LPSO phase are observed after 1-D forging. As the rolling deformation increased, the fibrous 18R-LPSO fractured into block and distributed more homogeneous. The lamellar 14H-LPSO fractured more severely, and it re-precipitated within the matrix when the deformation reached 50 %. The average grain size decreased gradually with increasing rolling deformation, and the minimum was 5.07 μm. After rolling, the {0001} and {0001} textures disappeared. The grain refinement of rolling alloy was mainly due to the fact that dynamic recrystallization (DRX) and substructures were generated within some grains, while the forging alloy was mainly due to DRX. The mechanisms of DRX were discontinuous DRX (DDRX) and twin-induced DRX (TDRX) after forging, and continuous DRX (CDRX) and DDRX after rolling. The strength reached its maximum when the rolling deformation amount reached 60 %, with a yield strength (YS) of 350 MPa and an ultimate tensile strength (UTS) of 385 MPa. Compared to the as-cast Mg–7Y–5Zn-0.1V alloy, its strength increased by 56 % and 63 %, respectively. The improvement of mechanical properties was mainly attributed to fine grain strengthening and dislocation strengthening.

The article contains experimental evaluation of technological possibilities of the wave-shaped profiles and confirmation of classical metal flow on profiles of wheel rims with toroidal flanges. The following parameters are recorded during the experiments: temperature in the finishing gauge, rolling force in the 2nd, 4th, 6th and 7th passes, current, voltages and motor speeds. The analysis of experimental data of rolling profiles 7.0-20-03, 8.5-20-03 and 228G-020-01 shows that technological capabilities of special rolled products for the truck wheel rims with wavy central part are much higher than serial profiles, where the central zone is of rectangular shape. It is possible to reduce the mass of profiles without changing the process parameters, i.e., rolling force and torque. This indicates the influence of additional and kinematic effects on the deformation zone in real production conditions. [ABSTRACT FROM AUTHOR]

The physical and mechanical properties and structural condition of flexible graphite foils produced by processing natural graphite with nitric acid, hydrolysis, thermal expansion of graphite and subsequent rolling were studied. The processes of obtaining materials and changing their characteristics has been thoroughly described and demonstrated. The structural transformations of graphite in the manufacture of foils were studied by X-ray diffraction analysis (XRD) and transmission electron microscopy (TEM). A decrease in the average size of the coherent scattering regions (CSR) of nanocrystallites was revealed during the transition from natural graphite to thermally expanded graphite from 57.3 nm to 20.5 nm at a temperature of 900 °C. The rolling pressure ranged from 0.05 MPa to 72.5 MPa. The thickness of the flexible graphite foils varied from 0.11 mm to 0.75 mm, the density—from 0.70 to 1.75 g/cm3. It was shown that with an increase in density within these limits, the compressibility of the graphite foil decreased from 65% to 9%, the recoverability increased from 5% to 60%, and the resiliency decreased from 10% to 6%, which is explained by the structural features of nanocrystallites. The properties' anisotropy of graphite foils was studied. The tensile strength increased with increasing density from 3.0 MPa (ρ = 0.7 g/cm3) to 14.0 MPa (ρ = 1.75 g/cm3) both in the rolling direction L and across T. At the same time, the anisotropy of physical and mechanical properties increased with an increase in density along L and T to 12% with absolute values of 14.0 MPa against 12.5 MPa at a thickness of 200 μm. Expressed anisotropy was observed along L and T when studying the misorientation angles of nanocrystallites: at ρ = 0.7 g/cm3, it was from 13.4° to 14.4° (up to 5% at the same thickness); at ρ = 1.3 g/cm3—from 11.0° to 12.8° (up to 7%); at ρ = 1.75 g/cm3—from 10.9° to 12.4° (up to 11%). It was found that in graphite foils, there was an increase in the coherent scattering regions in nanocrystallites with an increase in density from 24.8 nm to 49.6 nm. The observed effect can be explained by the coagulation of nanocrystallites by enhancing the Van der Waals interaction between the surface planes of coaxial nanocrystallites, which is accompanied by an increase in microstrains. The results obtained can help discover the mechanism of deformation of porous graphite foils. The obtained results can help discover the deformation mechanism of porous graphite foils. We assume that this will help predict the material behavior under industrial operating conditions of products based flexible graphite foils. [ABSTRACT FROM AUTHOR]

The paper analyzes the occurrence of evenly spaced cracks on the surface of lamellar specimens of Fe-28Mn-6Si-5Cr (mass %) shape-memory alloy (SMA), during cold rolling. The specimens were hot rolled and normalized and developed cold rolling cracks with an approximate spacing of about 1.3 mm and a depth that increased with the thickness-reduction degree. At normalized specimens, X-ray diffraction patterns revealed the presence of multiple crystallographic variants of brittle α′ body-bcc martensite, which could be the cause of cold-rolling cracking. Both normalized and cold-rolled specimens were analyzed using scanning electron microscopy SEM. SEM micrographs revealed the presence of several crystallographic variants of α′-body-centered cubic (bcc) and ε hexagonal close-packed (hcp) martensite plates within a γ-face-centered cubic (fcc) austenite matrix in a normalized state. High-resolution SEM, recorded after 25% thickness reduction by cold-rolling, emphasized the ductile character of the cracks by means of an array of multiple dimples. After additional 33% cold-rolling thickness reduction, the surface of crack walls became acicular, thus revealing the fragile character of failure. It has been argued that the specimens cracked in the neutral point but preserved their integrity owing to the ductile character of γ-fcc austenite matrix. [ABSTRACT FROM AUTHOR]

In this study, the effects of chemical composition and process routes on the microstructure and mechanical properties of high-Zn-content Al-Zn-Mg-Sc alloys were investigated. Aging led to the formation of nano-sized Zn phases in the grain interior and large Zn phases at the grain boundary (GB) or Al/Al3Sc interfaces in the Al-20Zn-0.5Mg-0.5Sc (20Zn-0.5Mg) alloy, and cold rolling before aging (Pre-CR) could accelerate this precipitation. Compared with the 20Zn-0.5Mg alloy, the Al-15Zn-1Mg-0.5Sc (15Zn-1Mg) alloy exhibited a more difficult Zn phase precipitation during aging, and only pre-CR could lead to the formation of intracrystalline Zn phases in this alloy during artificial aging. The transition of the η′ phases into η phases without coarsening of Zn phases occurred at the GB or Al/Al3Sc interfaces of the 15Zn-1Mg alloy during artificial aging. Pre-CR could improve the mechanical properties of high-Zn-content Al-Zn-Mg-Sc alloys, and the significant evolution of Zn phases in the 20Zn-0.5Mg alloy during processing in different routes conferred this alloy a wider range of mechanical properties than the 15Zn-1Mg alloy. [ABSTRACT FROM AUTHOR]

This article investigated the formability of aluminum/copper bimetal sheets during single-point incremental forming. First, the two-layer sheets were produced by the explosive welding process; then, the rolling process was performed with 50% strain on two-layer samples. Considering the importance of examining the mechanical and metallurgical properties on the formability of the two-layer samples, the mechanical properties were first examined, including the uniaxial tensile and micro-hardness tests. Then, metallurgical tests were performed, including scanning electron microscopy equipped with energy-dispersive X-ray spectroscopy (SEM-EDX) to investigate the fracture surface and penetration depth and an X-ray diffraction (XRD) test to check the secondary phase particles in the penetration zone of Al and Cu in five different annealing temperature conditions. Considering that the forming limit diagram (FLD) is dependent on the strain path, to study the effect of the strain path, the two-layer samples were formed by three geometries: pyramid, cone, and straight groove. Simulations of FLD by Abaqus software 6.14-4 with four different methods were studied: FLDCRT, effective strain rate (ESR), second derivation of thinning (SDT), and maximum strain rate (MSR). The results showed that the FLDCRT criterion provided a more accurate estimate of the necking time. In the following, the values of the thickness distribution were carried out by experimental and numerical methods, and the results between the methods were in good agreement. [ABSTRACT FROM AUTHOR]

Sunflower (Helianthus annuus L.), a vital crop for global vegetable oil production, encounters sustainability challenges in its cultivation. This study assesses the effects of incorporating a winter cover crop (CC), Avena sativa (L.), on the subsequent growth of sunflower crops and the vitality of their rhizosphere microbial communities over a two-year period. It examines the impact of two methods for suppressing winter CC—chemical suppression using glyphosate and mechanical suppression via rolling—both with and without the addition of phosphorus (P) starter fertilizer. These approaches are evaluated in comparison to the regional best management practices for sunflower cultivation, which involve a preparatory chemical fallow period and the subsequent application of starter P fertilizer. The methodology utilized Illumina sequencing for the analysis of rhizosphere bacterial 16S rRNA genes and fungal internal transcribed spacer (ITS) amplicons. Findings indicate a significant improvement (9–37%) in sunflower growth parameters (plant height, stem diameter, head diameter, and head dry weight) when cultivated after glyphosate-suppressed winter CC compared to the chemical fallows. Conversely, rolling of winter CC generally negatively affected sunflower growth. Rhizosphere bacterial communities following chemical suppression of winter CC showed greater Pielou’s evenness, indicating a uniform distribution of species. In general, this treatment had more detrimental effects on beneficial sunflower rhizosphere bacteria such as Hymenobacter and Pseudarthrobacter than rolling of the winter CC, suggesting that the overall effect on sunflower growth may be mitigated by the redundancy within the bacterial community. As for fungal diversity, measured by the Chao-1 index, it increased in sunflowers planted after winter CC and receiving P fertilization, underscoring nutrient management’s role in microbial community structure. Significant positive correlations between fungal diversity and sunflower growth parameters at the reproductive stage were observed (r = 0.41–0.72; p

After closure, voids need to be healed through bonding and interface dissolution to restore the mechanical properties and produce a sound product. For the prediction of void healing and the respective process optimization, a void healing criterion, spanning all three phases is needed. While hot rolling is generally suited for void healing, with large deformations at hydrostatic pressure as well as high temperatures, not all regions in the workpiece offer the same void healing conditions. Due to gradients of these metrics e. g. along the normal direction, a space-resolved approach is needed. Previously, a practical void healing criterion combining void closure and subsequent recrystallization has been proposed and applied to exemplary hot rolling processes. Besides a broader application of the criterion, adding the process parameters roll diameter and temperature, the present paper mainly aims for the experimental validation of this criterion. In bonding trials, a positive influence of temperature and strain on the bond strength has been found. While no clear correlation of the holding time on the bond strength was detectible without concurrent contact pressure the experiments suggested a saturation strain as an indicator for void healing instead. Accordingly, the criterion has been revised and a strain-based criterion proposed, applied, and compared to the previously introduced recrystallization-based void healing criterion.

In this research, corrosion behavior and discharge capabilities of the AZ61-In alloy experiencing hot rolling process have been discussed in detail. The results reveal that the introduction of indium to magnesium facilitates the dissolution of magnesium by augmenting a quantity of secondary phases, generating less-protective products. The corrosion resistance of AZI plus 50 % rolling reduction is improved attributed to the preferred basal orientation and further recrystallization. Moreover, the average discharge potentials of AZI-50 % can respectively reach −1.551 V and −1.234 V at 10 mA cm−2 and 50 mA cm−2, showing potential for application in seawater activated batteries.

The aging precipitated phases are of great significance for the strengthening and toughening of Al–Zn–Mg alloys. In this work, pre-precipitating was realized through equal channel angular pressing (ECAP) immediately followed by solid solution treatment at 475 °C for 6 h. Its corresponding strengthening and toughening effect on the room temperature (RT)-rolled Al–6Zn–1Mg alloy was systematically studied. The results indicate that pre-precipitating by ECAP can effectively improve the strength of the RT-rolled Al–6Zn–1Mg alloy and circumvent the strength-ductility trade-off. Microstructure characterization reveals that ECAP induces a large number of microshear bands, which can not only encourage recrystallization but also effectively promote the precipitation of the η′ phase. The synergistic effect of precipitation strengthening and dislocation strengthening contributes to the high strength of Al–6Zn–1Mg alloy, with UTS and YS increasing to ∼522 MPa and ∼400 MPa, respectively. Meanwhile, the ductility remains almost unchanged mainly due to the coordinated grain boundary sliding and the uniform and finely dispersed second phase particles. As a result, the strength-ductility trade-off is effectively avoided. The findings shed some light on optimizing the traditional aging treatment.

This paper presents research on the changes in the mechanical and structural properties of the commercial aluminum alloy EN-AW 7075 during thermomechanical processing. The processing involved artificial aging of the alloy at a temperature of 150°C for 30 minutes, followed by cold rolling after aging. Changes in hardness and impact toughness during the experiment were monitored. Hardness was measured using the Leeb method, while impact toughness was measured using the Charpy method. In the annealed state, the lowest hardness values were recorded, while the highest-impact toughness value was achieved in the as-quenched state. By applying cold plastic deformation after artificial aging, the hardness of the alloy significantly increased, while the impact toughness continuously decreased. After deformation of 20%, cracks appearance prevented further deformation. Optical microscopy was used to follow microstructural changes during the applied processing regime. Precipitates of various sizes and morphologies were observed in the structure. The annealed state results in poorly defined grain boundaries and formation of large precipitates relatively evenly distributed throughout the matrix. Cold plastic deformation after aging has resulted in elongated grain structure aligned with the rolling direction, along with crushing of secondary phase particles.

In this work, finite element simulation of the rolling-pressing process with horizontal and vertical rolls was carried out. To analyze the efficiency of metal processing, the main parameters of the stress-strain state were considered: equivalent strain, equivalent stress, average hydrostatic pressure, deformation force. Aluminum alloy Al6063 was chosen as the workpiece material. For variational simulation, models with a change in the heating temperature of the workpiece and the rolls rotation speed were constructed. The most optimal option is a model in which the workpiece was heated to 100 °C and deformation was carried out at a circumferential speed of the first pair of rolls of 60 rpm. Variants with a single temperature reduction to 20 °C, or rotation speed reduction to 35 rpm also give acceptable results to all the indicators considered. However, rotation speed reduction to 10 rpm makes it impossible to carry out a stable process at any temperature.