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Students’ learning experience and their engagement in online learning environments are becoming increasingly important as blended learning grows more prevalent in tertiary education. In this study, asynchronous lectures for applied sciences courses, offered to polytechnic students of Applied Chemistry and Pharmaceutical Science at Nanyang Polytechnic, were designed using the Community of Inquiry framework. Students’ perceptions of their learning experience and cognitive, emotional, and behavioral engagement in asynchronous lectures were determined through a survey study. The results showed that students were engaged and had positive learning experiences. Through an educational design research methodology, this survey study also determined and provided design features important for designing asynchronous lectures. Further research could explore the possibility of expanding the scope of the research to other institutions with students of different cultural backgrounds, learning preferences, and learning abilities.