Search

The human body constantly produces thermal electromagnetic radiation with a maximum of about 10 μm. This thermal radiation has a number of positive effects on the human body and, in addition, allows the insulation under clothing to be improved under extreme climatic conditions, causing a significant reduction in ambient temperature. With so-called far-infrared (FIR) textiles, it is possible to ensure the reflection of thermal radiation back to the human body. In the first part of this review, the generation of heat by the human body and its propagation by radiation through the skin are comprehensively explained. The thermal characteristics of the individual skin layers as an emitter of infrared radiation are given. The second part discusses the basic preparation methods of FIR textiles. Suitable particle systems are described based on metals and their oxides, porous carbon, and special ceramics. Modification of the fiber phase (especially the fineness of the fibers and the porosity of the fabric) in combination with the surface coating of metals is also used for their health-promoting effects. The main manufacturers of FIR textiles and their typical products are mentioned.

In this study, an algebraic model and its experimental verification was carried out to investigate the effect of moisture content on the heat loss that takes place due to conduction of sock fabrics. The results show that increasing moisture content in the studied socks caused a significant increase in their conductive heat loss. Plain knitted socks with different fiber composition were wetted to a saturated level, and then their moisture content was reduced stepwise. When achieving the required moisture content, the socks samples were characterized by the Alambeta testing instrument for heat transfer. Three different existing modified mathematical models for the thermal conductivity of wet fabrics were used for predicting thermal resistance of socks under wet conditions. The results from both ways are in very good agreement for all the socks at a 95% confidence level. In the above-mentioned models, the prediction of thermal resistance presents newly a combined effect of the real filling coefficient and thermal conductivity of the so-called “wet” polymers instead of dry polymers. With these modifications, the used models predicted the thermal resistance at different moisture levels. Predicted thermal resistance is converted into heat transfer (due to conduction) with a significantly high coefficient of correlation.

Nonwoven fabrics are widely used for thermal insulation and sound absorption purpose in construction and automobile fields. It is essential to investigate their thermal conductivity and sound absorption coefficient. Five cross-laid nonwoven fabrics are measured on the Alambeta device and Brüel & Kjær impedance tube. Bogaty and Bhattacharyya models are selected to predict the thermal conductivity, and Voronina and Miki models are used to predict the sound absorption coefficient. The predicted thermal conductivity shows a significant difference compared with the measured values. It is concluded that Bogaty and Bhattacharyya models are not suitable for high porous nonwoven fabric. In addition, the results of Voronina and Miki models for sound absorption prediction are acceptable, but Voronina model shows lower mean prediction error compared with Miki model. The results indicate that Voronina model can be used to predict the sound absorption of cross-laid nonwoven fabric.

By applying the simultaneous corona-temperature treatment, the effect of electret temperature on the structure and filtration properties of melt-blown nonwovens was investigated. Fiber diameter, pore size, thickness, areal weight, porosity, crystallinity, filtration efficiency, and pressure drop were evaluated. The results demonstrated that some changes occurred in the structure of electret fabrics after treatment under different temperatures. In the range of 20°C~105°C, the filtration efficiency of melt-blown nonwovens has a relationship with the change in crystallinity, and the pressure drop increased because of the change in areal weight and porosity. This work may provide a reference for further improving filtration efficiency of melt-blown nonwovens.

Thermal performance of aerogel-embedded polyester/polyethylene nonwoven fabrics in cross airflow was experimentally studied by using a laboratory-built dynamic heat transfer measuring device in which the fabric could be applied on a heating rod. Experiments were performed with different airflow velocities and heating conditions. The temperature–time histories of different materials were collected and compared. The temperature difference and convective heat transfer coefficient under continuous heating were analyzed and discussed. Results showed that under preheated conditions, the aerogel-embedded nonwoven fabrics had very small decrease in temperature and good ability to prevent against heat loss in cross flow. As for the continuous heating conditions, the heat transfer rate of each material showed an increasing trend with increase in the Reynolds number. The aerogel-treated nonwoven fabric with the least fabric thickness and aerogel content delivered a significantly increased heat transfer rate at higher Reynolds number. Thicker fabrics with higher aerogel content could provide better insulation ability in cross flow.

In this study, polypropylene meltblown nonwoven fabrics with different structure parameters such as fiber diameter, pore size, and areal density were prepared by the industrial production line. The morphology of meltblown nonwoven fibers was evaluated by using scanning electron microscope, and the diameter of fibers was analyzed by using image-pro plus software from at least 200 measurements. The pore size of nonwoven fabric was characterized by a CFP-1500AE type pore size analyzer. The filtration efficiency and pressure drop were evaluated by TSI8130 automatic filter. The results showed that the pressure drop of nonwoven fabrics decreased with the increase in pore size; the filtration efficiency and the pressure drop had a positive correlation with the areal density. However, when the areal density is in the range of 27–29 g/m2, both filtration efficiency and pressure drop decreased with the increase of areal density; when the areal density was kept constant, the filtration efficiency decreased as the pore size decreased; when the pore size of the meltblown nonwoven fabric is less than 17 μm, the filtration efficiency increased as the pore diameter decreased; when the pore diameter of the nonwoven fabric is larger than 17 μm. In a wide range, the pressure drop decreased as the fiber diameter decreased.

Polyvinylidene fluoride (PVDF) fibrous membranes with fiber diameter from nanoscale to microscale were prepared by electrospinning. The structural parameters of PVDF fibrous membrane in terms of fiber diameter, pore size and its distribution, porosity or packing density, thickness, and areal weight were tested. The relationship between solution concentration and structural parameters of fibrous membrane was analyzed. The filtration performance of PVDF fibrous membrane in terms of air permeability and filtration efficiency was evaluated. The results demonstrated that the higher solution concentration led to a larger fiber diameter and higher areal weight of fibrous membrane. However, no regular change was found in thickness, porosity, or pore size of fibrous membrane under different solution concentrations. The air permeability and filtration efficiency of fibrous membrane had positive correlations with pore size. The experimental results of filtration efficiency were compared with the predicted values from current theoretical models based on single fiber filtration efficiency. However, the predicted values did not have a good agreement with experimental results since the fiber diameter was in nanoscale and the ratio of particle size to fiber diameter was much larger than the value that the theoretical model requires.

Quality is the essence of any product for consumer satisfaction. However, different people have different perception of quality. Eventually the definition of quality varies from product to product and thus it is much more complex in textile clothing material evaluation. The end use application of a specific clothing material determines what should be the parameters of quality evaluation. Thus, the evaluation based on subjective assessment becomes unpredictable and unquantifiable. Quality for dress materials is not simply a physical parameter but something called as psycho-physical parameter. In recent times, many objective evaluation systems have been developed to evaluate the apparel grade textile materials with regard to their quality parameters. However, the evaluation does not involve enough statistical treatment of data so as to obtain a parametric weighted characterization of complex quality. The current work deals with parametric approach to complex quality evaluation based on multicriteria decision-making approach for ladies dress materials. The ladies dress materials are of numerous varieties and choices across the globe. The selection and marketing of these kinds of textile materials need to be given proper emphasis as it depends not only on physical parameters but also on climate, geography, ethnic group, market trend, age group, gender, and many such complex parameters, which are not quantifiable in absolute terms. In this study, woven fabrics used for ladies dress materials are collected from the market and they were evaluated for the consumer-oriented property parameters. A parametric approach is adopted to quantify the overall quality of these dress materials. Various objective techniques were used to evaluate the comfort and esthetic parameters. A complex quality index (CQI) was estimated with weighted combination of all the contributing parameters and total quality index was calculated. Selected consumers with different education level, age, and gender were interviewed to get a statistic of their opinion about quality parameters preferred by them. This complex quality index/degree of satisfaction shows very high correlation with subjective judgment. A CQI can be evaluated for each kind of clothing material looking into their applications.

The limitation of aramid fiber is its surface property, which results in its very poor interfacial adhesion to most of commercial resins. In order to improve the surface property of the aramid fiber, ozone treatment was carried out in this work. The aramid fabrics were evaluated in terms of surface morphology, wicking effect, tensile property, and ball bursting test. The results showed that the surface morphology of aramid fabrics did not undergo an obvious change; the wicking effect increased slightly with an increase in ozone treatment time; the tenacity and elongation of aramid fibers and fabrics did not significant change after ozone treatment, but the tenacity and elongation of aramid yarns showed significant improvement after ozone treatment, and increased with the increase of ozone treatment time; the ball bursting load and penetration displacement had a slight increase as well after ozone treatment. Therefore, ozone treatment could be one method to improve the surface property of the aramid fiber.

The air flow and conjugate heat transfer through the fabric was investigated numerically. The objective of this paper is to study the thermal insulation of fabrics under heat convection or the heat loss of human body under different conditions (fabric structure and contact conditions between the human skin and the fabric). The numerical simulations were performed in laminar flow regime at constant skin temperature (310 K) and constant air flow temperature (273 K) at a speed of 5 m/s. Some important parameters such as heat flux through the fabrics, heat transfer coefficient, and Nusselt number were evaluated. The results showed that the heat loss from human body (the heat transfer coefficient) was smallest or the thermal insulation of fabric was highest when the fabric had no pores and no contact with the human skin, the heat loss from human body (the heat transfer coefficient) was highest when the fabric had pores and the air flow penetrated through the fabric.

The quest for sound-absorbing materials that are not only environmentally friendly, but also sustainable is the foremost reason for natural fibre-acoustic materials. Bark cloth is a natural non-woven fabric that is largely produced from Ficus trees. An exploratory investigation of bark cloth a non-woven material and its reinforcement in epoxy polymer composites has been fabricated and investigated for the sound absorption properties so as to find the most suitable applications and also to see whether bark cloth can be used in some applications in place of man-made fibres. Three types of material species were investigated with their respective composites. The fibre morphology showed bark cloth to be a porous fabric that showed promising sound absorption properties at higher frequencies. The sound absorption results of four-layer material selections of Ficus natalensis, Ficus brachypoda and Antiaris toxicaria bark cloth showed sound absorption coefficient of 0.7; 0.71 and 0.91 at f > 6400 Hz, respectively. The bark cloth reinforced laminar epoxy composites had reduced sound absorption coefficients, which ranged from 0.1 to 0.35, which was attributed to decreased porosity and vibration in the bark cloth fibre network.

Flex fatigue behaviour of plastic optical fibres (POFs) with the diameters of 0.2 and 0.3 mm under different pretensions is measured with fatigue life curve by flexometer. The fatigue sensitivity coefficient is calculated by the linear fitting curve of normalised stress versus logarithm of bending cycles. The residual modulus is investigated during the flex fatigue processes. The results exhibit the exponential relationship between applied pretension and numbers of bending cycles at break. It is indicated that the flex fatigue of POFs might be sensitive with high swing angle or swing speed. There is an evident loss of modulus for two POFs with pretensions of 4 and 10% of ultimate tensile strength during 10-times bending cycles. The values of residual modulus of two POFs almost keep constant after 10-times bending cycles.

CO2 laser treatment can increase the surface roughness of plastic optical fibres (POFs) with the diameter of 0.5 mm and enhance the input intensity and attenuation coefficient accordingly, which is supposed to weaken the side emission of POFs in long distance above 375 mm. TiO2 particles were applied to improve the increasing optical loss of POFs by laser treatment. POFs were first modified with fine TiO2 particles and then treated by CO2 laser with the pixel time from 30 to 120 ìs. The surface morphology was observed by scanning electron microscopy to investigate the changes of micro-structure before and after laser treatment and the distribution of TiO2 particles. The illumination intensity and attenuation coefficient were calculated and compared in two methods. It is visible that the evaluation by model LLF2 with two parts is more suitable for the fitting of experimental data and shows higher input intensity and lower attenuation than that by standard power function. Both the evaluation methods exhibit that the utilization of TiO2 particles could play an active role in the enhancement of side emission of POFs treated by CO2 laser.

Air permeability is one of the most important properties of non-woven fabrics in many applications. This paper aims to investigate the effects of thickness, porosity and density on the air permeability of needle-punched non-woven fabrics and compare the experimental values with two models which are based on hydraulic radius theory and drag theory, respectively. The air permeability of the samples was measured by an air permeability tester FX3300. The results showed that the air permeability of non-woven fabrics decreased with the increase in thickness and density of samples, increased with the increase of porosity, and the air permeability was not directly proportional to the pressure gradient. Meanwhile, the prediction model based on hydraulic radius theory had a better agreement with experimental values than the model based on drag theory, but the values were much higher than the experimental results, especially for higher porosity and higher pressure gradient.

Effective thermal conductivity (ETC) is a very important index for evaluating the thermal property of heterogeneous materials, which include more than two different kinds of materials. Several analytical models were proposed for predicting the ETC of heterogeneous materials, but in some cases, these models cannot provide very accurate predictions. In this work, several analytical models and numerical simulations were studied in order to investigate the differences among them. In addition, some factors which would influence the ETC of heterogeneous materials were investigated by numerical simulation. The results demonstrated that the numerical simulation can provide very accurate prediction, indicated that different analytical models should be selected to predict specific problems based on their assumptions, and suggested that more variables need to be considered in order to improve these analytical models, such as inclusion shape, inclusion size, distribution of inclusions and contact area. Besides, numerical method could be an effective and reliable way to obtain the ETC of heterogeneous materials with any kind of complicated structures.

Bacterial cellulose (BC) presents significant promise as a biomaterial, boasting unique qualities such as exceptional cellulose purity, robust mechanical strength, heightened crystalline structure, and biodegradability. Several studies have highlighted specific effects, such as the impact of dehydration/rehydration on BC tensile strength, the influence of polymer treatment methods on mechanical properties, the correlation between microorganism type, drying method, and Young's modulus value, and the relationship between culture medium composition, pH, and crystallinity. Drying methods are crucial to the structure, performance, and application of BC films. Research findings indicate that the method used for drying can influence the mechanical properties of BC films, including parameters such as tensile strength, Young's modulus, and water absorption capacity, as well as the micromorphology, crystallinity, and thermal characteristics of the material. Their versatility makes them potential biomaterials applicable in various fields, including thermal and acoustic insulation, owing to their distinct thermal and mechanical attributes. This review delves into the thermal and mechanical behavior of bacterial cellulose aerogels, which are profoundly impacted by their drying mechanism.

This research provides an in-depth assessment of two paper yarn variants, examining their structural, functional, and performance characteristics. These yarns demonstrated favorable properties, including suitable linear density, twist, typical cellulosic functional groups as confirmed by Infrared spectroscopy, minimal hairiness, moisture transfer, and creditable mechanical strength. These yarns have flat layered cross-sections and grooved longitudinal surfaces. In addition, a low hairiness index (1.3-1.33) further acknowledged their smooth surface. Their remarkable evenness (15.86% and 7.08%) supported their effective wicking properties. Despite average breaking strength (0.77 cN/dTex and 1.05 cN/dTex) and moderate elongation, these yarns exhibited exceptional water-washing resistance and retained over 89% breaking strength after 15 washes. This study ranks these paper yarns as highly suitable for durable clothing fabrics, providing promising sustainable alternatives in the textile industry., Competing Interests: The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper., (© 2024 The Authors.)

Given their exceptional attributes, aerogels are viewed as a material with immense potential. Being a natural polymer, cellulose offers the advantage of being both replenishable and capable of breaking down naturally. Cellulose-derived aerogels encompass the replenish ability, biocompatible nature, and ability to degrade naturally inherent in cellulose, along with additional benefits like minimal weight, extensive porosity, and expansive specific surface area. Even with increasing appreciation and acceptance, the undiscovered possibilities of aerogels within the textiles sphere continue to be predominantly uninvestigated. In this context, we outline the latest advancements in the study of cellulose aerogels' formulation and their diverse impacts on textile formations. Drawing from the latest studies, we reviewed the materials used for the creation of various kinds of cellulose-focused aerogels and their properties, analytical techniques, and multiple functionalities in relation to textiles. This comprehensive analysis extensively covers the diverse strategies employed to enhance the multifunctionality of cellulose-based aerogels in the textiles industry. Additionally, we focused on the global market size of bio-derivative aerogels, companies in the industry producing goods, and prospects moving forward.

In this paper, copper deposited graphene was fabricated through electroless plating. A novel and facile pretreatment method is introduced based on ultrasonic treatment with nickel nano-particles as the catalytic core. This method abandons the sensitization and activation process in the traditional pretreatment that reduces the time and economic cost dramatically. The static contact angle was determined by an Olympus BX51M optical microscope. The surface morphology and plating composition were characterized via scanning electron microscope (SEM) and energy dispersive spectroscopy (EDS), the infrared radiation (IR) transmittance spectra of the copper plated graphene were measured by Fourier transform infrared spectroscopy (FTIR), the layer structure was measured by Raman spectrum, the phase identification was identified by X-ray diffraction (XRD), the thermogravimetric analysis (TGA) (Q5000 TA instruments, USA) was carried out to detect the thermal characteristics. The electrical resistivity of copper-plated graphene was performed in an especially designed apparatus. The results show that the surface of graphene is coarsened, and the size is reduced after ultrasonic treatment, which can facilitate the nucleation and fine particle distribution of metal. The electroless plated efficiency of copper of the nickel pretreatment copper-plated graphene is 64.27 wt%, higher than that of generic copper-plated graphene at 58.62 wt%. The resistivity decreases rapidly from 1.69 × 10 -2  Ω cm of the original Gr to 0.79 × 10 -2  Ω cm of Cu/Ni@Gr due to the large number of fine copper particles scattered around the graphene., (© 2022. The Author(s).)

In the current study, a sustainable approach was adopted for the green synthesis of silver nanoparticles, green synthesis of copper nanoparticles, and the investigation of the phytochemical and biological screening of bark, leaves, and fruits of Ehretia acuminata (belongs to the family Boraginaceae). Subsequently, the prepared nanoparticles and extracted phytochemicals were loaded on cotton fibres. Surface morphology, size, and the presence of antimicrobial agents (phytochemicals and particles) were analysed by scanning electron microscopy, dynamic light scattering, and energy-dispersive X-ray spectroscopy. The functional groups and the presence of particles (copper and silver) were found by FTIR and XRD analyses. The coated cotton fibres were further investigated for antibacterial (qualitative and quantitative), antiviral, and antifungal analysis. The study revealed that the herb-encapsulated nanoparticles can be used in numerous applications in the field of medical textiles. Furthermore, the utility of hygienic and pathogenic developed cotton bandages was analysed for the comfort properties regarding air permeability and water vapour permeability. Finally, the durability of the coating was confirmed by measuring the antibacterial properties after severe washing.

High thermostability of phase change materials is the critical factor for producing phase change thermoregulated fiber (PCTF) by melt spinning. To achieve the production of PCTF from melt spinning, a composite phase change material with high thermostability was developed, and a sheath-core structure of PCTF was also developed from bicomponent melt spinning. The sheath layer was polyamide 6, and the core layer was made from a composite of polyethylene and paraffin. The PCTF was characterized by scanning electron microscopy (SEM), thermal analysis (TG), Fourier Transform Infra-Red (FTIR), X-ray diffraction (XRD), differential scanning calorimetry (DSC) and fiber strength tester. The results showed that the core material had a very high thermostability at a volatilization temperature of 235 °C, the PCTF had an endothermic and exothermic process in the temperature range of 20-30 °C, and the maximum latent heat of the PCTF reached 20.11 J/g. The tenacity of the PCTF gradually decreased and then reached a stable state with the increase of temperature from -25 °C to 80 °C. The PCTF had a tenacity of 343.59 MPa at 0 °C, and of 254.63 MPa at 25 °C, which fully meets the application requirements of fiber in textiles.

Conventional conductive homopolymers such as polypyrrole and poly-3,4-ethylenedioxythiophene (PEDOT) have poor mechanical properties, for the solution to this problem, we tried to construct hybrid composites with higher electrical properties coupled with high mechanical strength. For this purpose, Kevlar fibrous waste, conductive carbon particles, and epoxy were used to make the conductive composites. Kevlar waste was used to accomplish the need for economics and to enhance the mechanical properties. At first, Kevlar fibrous waste was converted into a nonwoven web and subjected to different pretreatments (chemical, plasma) to enhance the bonding between fiber-matrix interfaces. Similarly, conductive carbon particles were converted into nanofillers by the action of ball milling to make them homogeneous in size and structure. The size and morphological structures of ball-milled particles were analyzed by Malvern zetasizer and scanning electron microscopy. In the second phase of the study, the conductive paste was made by adding the different concentrations of ball-milled carbon particles into green epoxy. Subsequently, composite samples were fabricated via a combination of prepared conductive pastes and a pretreated Kevlar fibers web. The influence of different concentrations of carbon particles into green epoxy resin for electrical conductivity was studied. Additionally, the electrical conductivity and electromagnetic shielding ability of conductive composites were analyzed. The waveguide method at high frequency (i.e., at 2.45 GHz) was used to investigate the EMI shielding. Furthermore, the joule heating response was studied by measuring the change in temperature at the surface of the conductive composite samples, while applying a different range of voltages. The maximum temperature of 55 °C was observed when the applied voltage was 10 V. Moreover, to estimate the durability and activity in service the ageing performance (mechanical strength and moisture regain) of developed composite samples were also analyzed.

To function as source control, a fabric mask must be able to filter micro-droplets (≥5 µm) in expiratory secretions and still allow the wearer to breathe normally. This study investigated the effects of fabric structural properties on the filtration efficiency (FE) and air permeability (AP) of a range of textile fabrics, using a new method to measure the filtration of particles in the described conditions. The FE improved significantly when the number of layers increased. The FE of the woven fabrics was generally higher, but double-layer weft knitted fabrics, especially when combined with a third (filter) layer, provided a comparable FE without compromising on breathability. This also confirmed the potential of nonwoven fabrics as filter layers in masks. None of the physical fabric properties studied affected FE significantly more than the others. The variance in results achieved within the sample groups show that the overall performance properties of each textile fabric are a product of its combined physical or structural properties, and assumptions that fabrics which appear to be similar will exhibit the same performance properties cannot be made. The combination of layers of fabric in the design of a mask further contributes to the product performance.

A textile material's electromagnetic interference (EMI) shielding effectiveness mainly depends on the material's electrical conductivity and porosity. Enhancing the conductivity of the material surface can effectively improve the electromagnetic shielding effectiveness. However, the use of highly conductive materials increases production cost, and limits the enhancement of electromagnetic shielding effectiveness. This work aims to improve the EMI shielding effectiveness (EMSE) by using an ultrathin multilayer structure and the air-permeable textile MEFTEX. MEFTEX is a copper-coated non-woven ultrathin fabric. The single-layer MEFTEX SE test results show that the higher its mass per unit area (MEFTEX 30), the better its SE property between 56.14 dB and 62.53 dB in the frequency band 30 MHz-1.5 GHz. Through comparative testing of three groups samples, a higher electromagnetic shielding effect is obtained via multilayer structures due to the increase in thickness and decrease of volume electrical resistivity. Compared to a single layer, the EMI shielding effectiveness of five layers of MEFTEX increases by 44.27-83.8%. Due to its ultrathin and porous structure, and considering the balance from porosity and SE, MEFTEX 10 with three to four layers can still maintain air permeability from 2942 L/m 2 /s-3658 L/m 2 /s.

In this study, we developed multifunctional and durable textile sensors. The fabrics were coated with metal in two steps. At first, pretreatment of fabric was performed, and then copper and silver particles were coated by the chemical reduction method. Hence, the absorbance/adherence of metal was confirmed by the deposition of particles on microfibers. The particles filled the micro spaces between the fibers and made the continuous network to facilitate the electrical conduction. Secondly, further electroplating of the metal was performed to make the compact layer on the particle- coated fabric. The fabrics were analyzed against electrical resistivity and electromagnetic shielding over the frequency range of 200 MHz to 1500 MHz. The presence of metal coating was confirmed from the surface microstructure of coated fabric samples examined by scanning electron microscopy, EDS, and XRD tests. For optimized plating parameters, the minimum surface resistivity of 67 Ω, EMI shielding of 66 dB and Ohmic heating of 118 °C at 10 V was observed. It was found that EMI SH was increased with an increase in the deposition rate of the metal. Furthermore, towards the end, the durability of conductive textiles was observed against severe washing. It was observed that even after severe washing there was an insignificant increase in electrical resistivity and good retention of the metal coating, as was also proven with SEM images.

The augmented demands of textile materials over time have brought challenges in the disposal of substantial volumes of waste generated during the processing and end of life of such materials. Taking into consideration environmental safety due to discarding of textile waste, it becomes critical to recuperate useful products from such waste for economic reasons. The present work deals with the preparation of porous and electrically conductive activated carbon fabric by a novel single stage method of simultaneous carbonization and physical activation of Kevlar feedstock material procured from local industries, for effective electromagnetic (EM) shielding applications. The Kevlar fabric waste was directly carbonized under a layer of charcoal without any intermediate stabilization step at 800 °C, 1000 °C, and 1200 °C, with a heating rate of 300 °C/h and without any holding time. The physical and morphological properties of the activated carbon, influenced by carbonization process parameters, were characterized from EDX, X-ray diffraction, SEM analysis, and BET analysis. Furthermore, the electrical conductivity was analyzed. Finally, the potential application of the activated material for EM shielding effectiveness was analyzed at low (below 1.5 GHz) and high (2.45 GHz) frequencies. The phenomena of multiple internal reflections and absorption of electromagnetic radiations was found dominant in the case of activated carbon fabric produced at higher carbonization temperatures.

In the current research, we present a single-step, one-pot, room temperature green synthesis approach for the development of functional poly(tannic acid)-based silver nanocomposites. Silver nanocomposites were synthesized using only tannic acid (plant polyphenol) as a reducing and capping agent. At room temperature and under mildly alkaline conditions, tannic acid reduces the silver salt into nanoparticles. Tannic acid undergoes oxidation and self-polymerization before the encapsulating of the synthesized silver nanoparticle and forms silver nanocomposites with a thick capping layer of poly(tannic acid). No organic solvents, special instruments, or toxic chemicals were used during the synthesis process. The results for the silver nanocomposites prepared under optimum conditions confirmed the successful synthesis of nearly spherical and fine nanocomposites (10.61 ± 1.55 nm) with a thick capping layer of poly(tannic acid) (~3 nm). With these nanocomposites, iron could be detected without any special instrument or technique. It was also demonstrated that, in the presence of Fe 3+ ions (visual detection limit ~20 μM), nanocomposites aggregated using the coordination chemistry and exhibited visible color change. Ultraviolet-visible (UV-vis) and scanning electron microscopy (SEM) analysis also confirmed the formation of aggregate after the addition of the analyte in the detection system (colored nanocomposites). The unique analytic performance, simplicity, and ease of synthesis of the developed functional nanocomposites make them suitable for large-scale applications, especially in the fields of medical, sensing, and environmental monitoring. For the medical application, it is shown that synthesized nanocomposites can strongly inhibit the growth of Escherichia coli and Staphylococcus aureus . Furthermore, the particles also exhibit very good antifungal and antiviral activity.

The fabrics with electromagnetic interference (EMI) have been used in various fields. However, most studies related to the EMI fabrics focused on the improvement of the final electromagnetic shielding effectiveness (EM SE ) by adjusting the preparation parameters while the breathability of the EMI fabrics was affected and the visible surficial patterns on the EMI fabric was limited. In this work, the two samples based on the Song Brocade structure were fabricated with surficial visible pattern ''. One was fabricated with silver-plated polyamide (Ag-PA) yarns and the silk yarns, the another with polyester (PET) yarns and the silk yarns. The weaving structure of the two samples were investigated by scanning electronic microscopy (SEM) and laser optical microscopy (LOM). The resistance against the EM radiation near field communication (NFC) and the ultraviolet (UV) light was also evaluated. Besides, the surface resistance, the air permeability and the water evaporation rate were investigated. The results revealed that the '' appeared successfully on the surface of the two samples with stable weaving structure. The Ag-PA yarn-incorporated Song Brocade fabric had the EMI shielding effectiveness value around 50 dB, which was supported by the low surface resistance less than 40 Ω. The excellent NFC shielding of the Ag-PA yarn-incorporated Song Brocade was also found. The ultraviolet protection factor (UPF) value of the Ag-PA yarn-incorporated Song Brocade fabric was higher than 190. The air permeability and the evaporation rate of the Ag-PA yarn-incorporated Song Brocade fabric was higher than 99 mm/s, and 1.4 g/h, respectively. As a result, the Ag-PA yarn-incorporated Song Brocade fabrics were proposed for both the personal and the industrial scale utilization.

P-aminophenol is a hazardous environmental pollutant that can remain in water in the natural environment for long periods due to its resistance to microbiological degradation. In order to decompose p-aminophenol in water, manganese oxide/polytetrafluoroethylene (PTFE) hollow fiber membranes were prepared. MnO 2 and Mn 3 O 4 were synthesized and stored in PTFE hollow fiber membranes by injecting MnSO 4 ·H2O, KMnO 4 , NaOH, and H 2 O 2 solutions into the pores of the PTFE hollow fiber membrane. The resultant MnO 2 /PTFE and Mn 3 O 4 /PTFE hollow fiber membranes were characterized using scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), and thermal analysis (TG). The phenol catalytic degradation performance of the hollow fiber membranes was evaluated under various conditions, including flux, oxidant content, and pH. The results showed that a weak acid environment and a decrease in flux were beneficial to the catalytic degradation performance of manganese oxide/PTFE hollow fiber membranes. The catalytic degradation efficiencies of the MnO 2 /PTFE and Mn 3 O 4 /PTFE hollow fiber membranes were 70% and 37% when a certain concentration of potassium monopersulfate (PMS) was added, and the catalytic degradation efficiencies of MnO 2 /PTFE and Mn 3 O 4 /PTFE hollow fiber membranes were 50% and 35% when a certain concentration of H 2 O 2 was added. Therefore, the manganese oxide/PTFE hollow fiber membranes represent a good solution for the decomposition of p-aminophenol.

Electromagnetically shielding textile materials, especially in professional or ordinary clothing, are used to protect an implanted pacemaker in the body. Alternatively, traditional textiles are known for their non-conductivity and transparency to an electromagnetic field. The main goal of this work was to determine whether the high moisture content (sweat) of the traditional textile structure significantly affects the resulting ability of the material to shield the electromagnetic field. Specifically, whether sufficient wetting of the traditional textile material can increase its electrical conductivity to match the electrically conductive textiles determined for shielding of the electromagnetic field. In this study, cotton and polyester knitted fabric samples were used, and two liquid medias were applied to the samples to simulate human sweating. The experiment was designed to analyse the factors that have a significant effect on the shielding effectiveness that was measured according to ASTM D4935. The following factors have a significant effect on the electromagnetic shielding effectiveness of moisturised fabric: squeezing pressure, drying time and type of liquid media. Additionally, the increase of electromagnetic shielding was up to 1 dB at 1.5 GHz frequency at the highest level of artificial sweat moisturised sample.

The versatile one-pot green synthesis of a highly concentrated and stable colloidal dispersion of silver nanoparticles (Ag NPs) was carried out using the self-assembled tannic acid without using any other hazardous chemicals. Tannic acid (Plant-based polyphenol) was used as a reducing and stabilizing agent for silver nitrate in a mild alkaline condition. The synthesized Ag NPs were characterized for their concentration, capping, size distribution, and shape. The experimental results confirmed the successful synthesis of nearly spherical and highly concentrated (2281 ppm) Ag NPs, capped with poly-tannic acid (Ag NPs-PTA). The average particle size of Ag NPs-PTA was found to be 9.90 ± 1.60 nm. The colloidal dispersion of synthesized nanoparticles was observed to be stable for more than 15 months in the ambient environment (25 °C, 65% relative humidity). The synthesized AgNPs-PTA showed an effective antimicrobial activity against Staphylococcus Aureus (ZOI 3.0 mM) and Escherichia coli (ZOI 3.5 mM). Ag NPs-PTA also exhibited enhanced catalytic properties. It reduces 4-nitrophenol into 4-aminophenol in the presence of NaBH 4 with a normalized rate constant (K nor = K/m) of 615.04 mL·s -1 ·mg -1 . For comparison, bare Ag NPs show catalytic activity with a normalized rate constant of 139.78 mL·s -1 ·mg -1 . Furthermore, AgNPs-PTA were stable for more than 15 months under ambient conditions. The ultra-high catalytic and good antimicrobial properties can be attributed to the fine size and good aqueous stability of Ag NPs-PTA. The unique core-shell structure and ease of synthesis render the synthesized nanoparticles superior to others, with potential for large-scale applications, especially in the field of catalysis and medical.

COVID-19, classified as SARS-CoV-2, is causing an ongoing global pandemic. The pandemic has resulted in the loss of lives and has caused economic hardships. Most of the devices used to protect against the transmission of the novel COVID-19 disease are related to textile structures. Hence, the challenge for textile professionals is to design and develop suitable textile structures with multiple functionalities for capturing viruses, passivating them, and, at the same time, having no adverse effects on humans during the complete period of use. In addition to manufacturing efficient, biocompatible, and cost-effective protective face masks, it is also necessary to inform the public about the benefits and risks of protective face mask materials. The purpose of this article is to address the concerns of efficiency and efficacy of face masks by primarily reviewing the literature of research conducted at the Technical University of Liberec. The main focus is on the presentation of problems related to the specification of aims of face mask applications, mechanisms of capture, durability, and modes of sterilization. The recommendations, instead of conclusions, are addressed to the whole textile society because they should be leading players in the design, creation, and proper treatment of face masks due to their familiarity with the complex behavior of textile structures and targeted changes of structural hierarchy starting from polymeric chains (nano-level) and ending in planar textile structures (millimeter level) due to action by mechanical, physical and chemical fields. This becomes extremely critical to saving hundreds of thousands of lives from COVID-19.

Electromagnetic (EM) radiation is everywhere in this world and galaxy in different forms and levels. In some cases, human beings need to protect themselves from electromagnetic radiations and the same thing is also recommended for electronic devices as well. Lots of studies are there on the shielding of electromagnetic radiation interference using metals, polymers, and minerals. For protecting the human being, textile structures are playing the main role. In the textile material structure itself many types are there; each one is having its unique geometrical shape and design. In this work, the copper/nickel-coated ultrathin nonwoven fabric is prepared like a strip. The 3, 6, and 9 mm thick strips are prepared and laid at different gaps, angles, and layered to study the effect of factors on EM shielding effectiveness as per ASTM D4935-10 standard. The design of experiment has been done to analyze the three factors and three levels of the strip properties having an influence on electromagnetic shielding results. From the findings of the design of experiment (DoE) screening design, the factors are the thickness of the strips, the gap between the strips, and the strips laid angle having a statistically significant effect on electromagnetic shielding effectiveness.

Resistance against penetration of various rays including electromagnetic waves (EM), infrared rays (IR), and ultraviolet rays (UV) has been realized by using copper (Cu)-coated fabrics. However, the corrosion of the Cu on coated fabrics influenced the shielding effectiveness of the various rays. Besides, the metal-coated fabrics have high density and are unbreathable. This work aims to solve the problem by incorporating nickel (Ni) into the Cu coating on the ultra-light polyester fibrous materials (Milife ® composite nonwoven fabric-10 g/m 2 , abbreviation Milife) via electroless plating. The electromagnetic interference (EMI), IR test, ultraviolet protection factor (UPF), water contact angle, and air permeability of the Cu/Ni-coated Milife fabric were measured. All the samples were assumed as ultra-light and breathable by obtaining the similar fabric density (~10.57 g/m 2 ) and large air permeability (600-1050 mm/s). The Cu/Ni deposition on the Milife fabrics only covered the fibers. The EM shielding effectiveness ( SE ) decreased from 26 to 20 dB, the IR reflectance ( R infrared ) decreased from 0.570 to 0.473 with increasing w Ni from 0 to 19.5 wt %, while the w Ni improved the UPF from 9 to 48. Besides, addition of Ni changed the Cu/Ni-coated Milife fabric from hydrophilicity to the hydrophobicity by observing WCA from 77.7° to 114°.

Polytetrafluoroethylene (PTFE) is a synthetic fluoropolymer known for its excellent hydrophobic properties. In this work, samples from PTFE dispersions with different combinations of water and carbon microparticles were prepared using an electrospraying method. The morphologies and sizes of carbon particles were investigated and the properties of layers including roughness, hydrophobicity and electrical resistivity were investigated. The non-conductive carbon microparticles were selected as a model particle to check the compatibility and electrospraying ability, and it had no effect on the hydrophobic and electrical properties. Carbon microparticles in polymer solution increased the degree of ionization and was found to be beneficial for the shape control of materials. The results showed that PTFE dispersion with the composition of water and carbon microparticles produced fine sphere particles and the layer fabricated with increased roughness. It was also found that the electrical resistivity and hydrophobicity of all the layers comparatively increased. The fabricated microporous layers can be used in various applications like interlining layer in multilayer textile sandwiches.

The commercial availability of inorganic/organic precursors for sol-gel formulations is very high and increases day by day. In textile applications, the precursor-synthesized sol-gels along with functional chemicals can be deposited onto textile fabrics in one step by rolling, padding, dip-coating, spraying or spin coating. By using this technology, it is possible to provide fabrics with functional/multi-functional characteristics including flame retardant, anti-mosquito, water- repellent, oil-repellent, anti-bacterial, anti-wrinkle, ultraviolet (UV) protection and self-cleaning properties. These surface properties are discussed, describing the history, basic chemistry, factors affecting the sol-gel synthesis, progress in sol-gel technology along with various parameters controlling sol-gel technology. Additionally, this review deals with the recent progress of sol-gel technology in textiles in addressing fabric finishing, water repellent textiles, oil/water separation, flame retardant, UV protection and self-cleaning, self-sterilizing, wrinkle resistance, heat storage, photochromic and thermochromic color changes and the improvement of the durability and wear resistance properties.

This review analyzes thermal and electrically conductive properties of composites and how they can be influenced by the addition of special nanoparticles. Composite functional characteristics-such as thermal and electrical conductivity, phase changes, dimensional stability, magnetization, and modulus increase-are tuned by selecting suitable nanoparticle filler material. The conductivity of composites can be related to the formation of conductive pathways as nanofiller materials form connections in the bulk of a composite matrix. With increasing use of nanomaterial containing composites and relatively little understanding of the toxicological effects thereof, adequate disposal and recyclability have become an increasing environmental concern.