Search

Our current understanding of early human settlements in North Africa relies on a few well-contextualized Oldowan and Acheulean sites (e.g., Ain Hanech, El Kherba, Ain Boucherit Lw and Up, Tighennif in Algeria; Thomas Quarry in Morocco). In particular, the site of Ain Hanech has documented for many decades the earliest evidence of human presence in North Africa (e.g., Sahnouni and de Heinzelin, 1998), until older stone tools were recently reported at the nearby Ain Boucherit locality (Sahnouni et al., 2018). While the Early Pleistocene antiquity of this Oldowan assemblage has never really been questioned, its exact age has, however, been discussed. In the early 2000s, a series of articles were published in this journal arguing either for an age of ~1.8 Ma (Sahnouni et al., 2002, 2004) or much younger, around 1.2 Ma (Geraads et al., 2004). Although subsequent chronostratigraphic studies have provided additional evidence for the older age (Pares et al., 2014 ; Sahnouni et al., 2018; Duval et al., 2021), Ain Hanech site had never been numerically dated until now. Moreover, beyond the archeological relevance of the site, Ain Hanech faunal association has also long been used as a reference for biochronological inferences and comparative studies with other paleontological localities of the region (e.g., Geraads, 2002; Sahnouni et al., 2002; Van der Made and Sahnouni, 2013; Van der Made et al., 2021). In other words, the accuracy of North African biochronology over the Early Pleistocene timescale partly relies on the age of Ain Hanech. In this context, we present here the dating results from electron spin resonance (ESR) and uranium-series (U-series) methods tentatively applied to optically bleached quartz grains and fossil teeth from Ain Hanech and the nearby stratigraphically equivalent site of El Kherba (Sahnouni and de Heinzelin, 1998).

The Aïn Beni Mathar-Guefaït Basin, in the High Plateau Region (Morocco), is dissected by the Za River, the main eastern tributary of the Moulouya, which incises more than 150 m into Plio-Pleistocene sediments. The main goal of the present study is to provide an initial geochronologic framework for such basin infill based on a combination of magnetostratigraphy and electron spin resonance (ESR). The combined results have implications on the age of the paleontological record, the evolution of the Moulouya River, and the activity of the faults that delimit the basin. We have studied sedimentary rocks that are essentially flat-lying and of an alluvial and lacustrine/palustrine origin. An approximately 140 m-thick section has been sampled at an average of 2.5 m per site, allowing to build a local magnetic polarity stratigraphy that includes nine geomagnetic reversals. Although no fold test is available, the presence of dual polarities and rockmagnetic analysis give us confidence that magnetization directions are primary. We then anchored the obtained magnetozones to the Geomagnetic Polarity Timescale (GPTS) using the biostratigraphic data as well as local geological observations. Our proposed magnetostratigraphy-based chronology reveals a Plio-Pleistocene sedimentary infill spanning from Gauss to Olduvai Chrons. The lower, detrital formations mostly fall within the normal Gauss Chron, whereas the upper lacustrine and palustrine carbonates, which are almost widespread to the top of the sedimentary fill, are Olduvai in age. These results provide the first chronological constraints for the basin fill in one of the largest intermontane basins of the High Plateaus. The new magnetostratigraphy also reveals that the major environmental change that triggered a switch from alluvial to lacustrine-palustrine conditions in Northern Maghreb occurred near the Gauss-Matuyama reversal, ca. 2.6 Ma. In addition, it shows that the age of the paleontological site Guefaït-4 is approximately

Systematic excavation and multidisciplinary research undertaken over three decades have deepened our understanding of the early Palaeolithic archaeology at Cueva Negra del Estrecho del Río Quípar (Caravaca de la Cruz, Murcia, Spain). New results from biochronology and combined ESR and U-series dating corroborate previous magnetostratigraphy, placing the entire excavated sequence between the Jaramillo sub-chron and the Matuyama-Brunhes boundary (i.e., ca. 990-772 thousand years ago [ka]); palaeontological and palynological findings reflect temperate environmental conditions. A bifacially-flaked limestone hand-axe was excavated one metre below the top of the Pleistocene sequence. The Equus cf. altidens tooth that provided the ESR estimate was excavated one metre below the hand-axe. Throughout its five-metre-deep sedimentary sequence, small nodules, fragments, and struck flakes make up the bulk of the Palaeolithic assemblage. Stratigraphical analysis points to undisturbed continuous sedimentary deposition above a layer of ashy sediment, encountered 4.5 m below the top of the Pleistocene sequence, which contained thermallyaltered bone and heat-shattered chert cores and flakes. Cueva Negra is among the earliest European sites with firm evidence of combustion.

This paper presents a reassessment of the archaeological record at Leang Burung 2, a key early human occupation site in the Late Pleistocene of Southeast Asia. Excavated originally by Ian Glover in 1975, this limestone rock-shelter in the Maros karsts of Sulawesi, Indonesia, has long held significance in our understanding of early human dispersals into 'Wallacea', the vast zone of oceanic islands between continental Asia and Australia. We present new stratigraphic information and dating evidence from Leang Burung 2 collected during the course of our excavations at this site in 2007 and 2011-13. Our findings suggest that the classic Late Pleistocene modern human occupation sequence identified previously at Leang Burung 2, and proposed to span around 31,000 to 19,000 conventional 14C years BP (~35-24 ka cal BP), may actually represent an amalgam of reworked archaeological materials. Sources for cultural materials of mixed ages comprise breccias from the rear wall of the rock-shelter-remnants of older, eroded deposits dated to 35-23 ka cal BP-and cultural remains of early Holocene antiquity. Below the upper levels affected by the mass loss of Late Pleistocene deposits, our deep-trench excavations uncovered evidence for an earlier hominin presence at the site. These findings include fossils of now-extinct proboscideans and other 'megafauna' in stratified context, as well as a cobble-based stone artifact technology comparable to that produced by late Middle Pleistocene hominins elsewhere on Sulawesi.

A limestone cave on the lower slopes of the southeastern Australian high country reveals a deep, stratified deposit dated from ca. 14,000 to 2000 cal. BP and rich in predominantly non-cultural faunal remains. Located in a sensitive ecological area between the Australian Alps and the Southern Tablelands, the site provides a valuable chronological archive for the interpretation of local environmental change using the faunal record as a proxy, in particular native rodents and other small mammals. Inferred palaeoenvironmental trends include the cessation of periglacial conditions in the surrounding ranges during the Terminal Pleistocene; a shift to warmer conditions and the establishment of forest and wetland habitats from around 13,500 to 10,000 cal. BP, with a significant decline in cold-adapted species at ca. 11,500 cal. BP and a period of significant taxon fluctuation and extinctions corresponding to a possible peak in warm and moist conditions (a ‘Holocene Optimum’), beginning around 8000 cal. BP and lasting perhaps 1500 to 2000 years. Complications to the relatively steady and continuous chronostratigraphy, formed from an AMS radiocarbon sequence from sedimentary charcoal, arose from the presence of several teeth of extinct sthenurine megafauna. These were resolved with direct U-series analysis to establish their much greater antiquity and comparison of the sthenurine teeth with teeth of extant macropodids from the same deposit through fluoride absorption analysis, which also identified the megafauna teeth as anomalous to the sequence. The site provides an important case study for the interpretation of megafauna remains in stratified sedimentary deposits, especially for sites that appear to contain evidence for the co-occurrence of megafauna and humans in primary contexts.

To date, the earliest modern human fossils found outside of Africa are dated to around 90,000 to 120,000 years ago at the Levantine sites of Skhul and Qafzeh. A maxilla and associated dentition recently discovered at Misliya Cave, Israel, was dated to 177,000 to 194,000 years ago, suggesting that members of the Homo sapiens clade left Africa earlier than previously thought. This finding changes our view on modern human dispersal and is consistent with recent genetic studies, which have posited the possibility of an earlier dispersal of Homo sapiens around 220,000 years ago. The Misliya maxilla is associated with full-fledged Levallois technology in the Levant, suggesting that the emergence of this technology is linked to the appearance of Homo sapiens in the region, as has been documented in Africa.

Strontium isotope ratios (⁸⁷Sr/⁸⁶Sr) of archaeological samples (teeth and bones) can be used to track mobility and migration across geologically distinct landscapes. However, traditional interpolation algorithms and classification approaches used to generate Sr isoscapes are often limited in predicting multiscale ⁸⁷Sr/⁸⁶Sr patterning. Here we investigate the suitability of plant samples and soil leachates from the IRHUM database (www.irhumdatabase.com) to create a bioavailable ⁸⁷Sr/⁸⁶Sr map using a novel geostatistical framework. First, we generated an ⁸⁷Sr/⁸⁶Sr map by classifying ⁸⁷Sr/⁸⁶Sr values into five geologically-representative isotope groups using cluster analysis. The isotope groups were then used as a covariate in kriging to integrate prior geological knowledge of Sr cycling with the information contained in the bioavailable dataset and enhance ⁸⁷Sr/⁸⁶Sr predictions. Our approach couples the strengths of classification and geostatistical methods to generate more accurate ⁸⁷Sr/⁸⁶Sr predictions (Root Mean Squared Error = 0.0029) with an estimate of spatial uncertainty based on lithology and sample density. This bioavailable Sr isoscape is applicable for provenance studies in France, and the method is transferable to other areas with high sampling density. While our method is a step forward in generating accurate ⁸⁷Sr/⁸⁶Sr isoscapes, the remaining uncertainty also demonstrates that fine-modelling of ⁸⁷Sr/⁸⁶Sr variability is challenging and requires more than geological maps for accurately predicting ⁸⁷Sr/⁸⁶Sr variations across the landscape. Future efforts should focus on increasing sampling density and developing predictive models to further quantify and predict the processes that lead to ⁸⁷Sr/⁸⁶Sr variability.

This paper presents a reassessment of the archaeological record at Leang Burung 2, a key early human occupation site in the Late Pleistocene of Southeast Asia. Excavated originally by Ian Glover in 1975, this limestone rock-shelter in the Maros karsts of Sulawesi, Indonesia, has long held significance in our understanding of early human dispersals into 'Wallacea', the vast zone of oceanic islands between continental Asia and Australia. We present new stratigraphic information and dating evidence from Leang Burung 2 collected during the course of our excavations at this site in 2007 and 2011-13. Our findings suggest that the classic Late Pleistocene modern human occupation sequence identified previously at Leang Burung 2, and proposed to span around 31,000 to 19,000 conventional 14C years BP (~35-24 ka cal BP), may actually represent an amalgam of reworked archaeological materials. Sources for cultural materials of mixed ages comprise breccias from the rear wall of the rock-shelter-remnants of older, eroded deposits dated to 35-23 ka cal BP-and cultural remains of early Holocene antiquity. Below the upper levels affected by the mass loss of Late Pleistocene deposits, our deep-trench excavations uncovered evidence for an earlier hominin presence at the site. These findings include fossils of now-extinct proboscideans and other 'megafauna' in stratified context, as well as a cobble-based stone artifact technology comparable to that produced by late Middle Pleistocene hominins elsewhere on Sulawesi.

New ages for flowstone, sediments and fossil bones from the Dinaledi Chamber are presented. We combined optically stimulated luminescence dating of sediments with U-Th and palaeomagnetic analyses of flowstones to establish that all sediments containing Homo naledi fossils can be allocated to a single stratigraphic entity (sub-unit 3b), interpreted to be deposited between 236 ka and 414 ka. This result has been confirmed independently by dating three H. naledi teeth with combined U-series and electron spin resonance (US-ESR) dating. Two dating scenarios for the fossils were tested by varying the assumed levels of 222Rn loss in the encasing sediments: a maximum age scenario provides an average age for the two least altered fossil teeth of 253 +82/-70 ka, whilst a minimum age scenario yields an average age of 200 +70/-61 ka. We consider the maximum age scenario to more closely reflect conditions in the cave, and therefore, the true age of the fossils. By combining the US-ESR maximum age estimate obtained from the teeth, with the U-Th age for the oldest flowstone overlying Homo naledi fossils, we have constrained the depositional age of Homo naledi to a period between 236 ka and 335 ka. These age results demonstrate that a morphologically primitive hominin, Homo naledi, survived into the later parts of the Pleistocene in Africa, and indicate a much younger age for the Homo naledi fossils than have previously been hypothesized based on their morphology.

Molluscs incorporate negligible uranium into their skeleton while they are living, with any uranium uptake occurring post-mortem. As such, closed-system U-series dating of molluscs is unlikely to provide reliable age constraints for marine deposits. Even the application of open-system U-series modelling is challenging, because uranium uptake and loss histories can affect time-integrated uranium distributions and are difficult to constrain. We investigate the chemical and isotopic distribution of uranium in fossil Tridacna gigas (giant clams) from Marine Isotope Stage (MIS) 5e (128–116 ka) and MIS 11 (424–374 ka) reefs at Huon Peninsula in Papua New Guinea. The large size of the clams enables detailed chemical and isotopic mapping of uranium using LA-ICPMS and LA-MC-ICPMS techniques. Within each fossil Tridacna specimen, marked differences in uranium concentrations are observed across the three Tridacna growth zones (outer, inner, hinge), with the outer and hinge zones being relatively enriched. In MIS 5e and MIS 11 Tridacna, the outer and hinge zones contain approximately 1 ppm and 5 ppm uranium respectively. In addition to uptake of uranium, loss of uranium appears prevalent, especially in the MIS 11 specimens. The effect of uranium loss is to elevate measured [230Th/238U] values with little effect on [234U/238U] values. Closed-system age estimates are on average 50% too young for the MIS 5e Tridacna, and 25% too young for the MIS 11 Tridacna. A complex, multi-stage uptake and loss history is interpreted for the fossil Tridacna and we demonstrate that they cannot provide independent, reliable geochronological controls on the timing of past reef growth at Huon Peninsula.

Wallacea, the zone of oceanic islands separating the continental regions of Southeast Asia and Australia, has yielded sparse evidence for the symbolic culture of early modern humans. Here we report evidence for symbolic activity 30,000-22,000 y ago at Leang Bulu Bettue, a cave and rock-shelter site on the Wallacean island of Sulawesi. We describe hitherto undocumented practices of personal ornamentation and portable art, alongside evidence for pigment processing and use in deposits that are the same age as dated rock art in the surrounding karst region. Previously, assemblages of multiple and diverse types of Pleistocene "symbolic" artifacts were entirely unknown from this region. The Leang Bulu Bettue assemblage provides insight into the complexity and diversification of modern human culture during a key period in the global dispersal of our species. It also shows that early inhabitants of Sulawesi fashioned ornaments from body parts of endemic animals, suggesting modern humans integrated exotic faunas and other novel resources into their symbolic world as they colonized the biogeographically unique regions southeast of continental Eurasia.

We present here the results of a technological and typological analysis of the Acheulian and early Middle Paleolithic assemblages from Torre in Pietra (Latium, Italy) together with comparisons with the Acheulian small tools of Castel di Guido. The assemblages were never chronometrically dated before. We have now 40Ar/39Ar dates and ESR-U-series dates, within a geomorphological framework, which support correlations to marine isotope stages. The Acheulian (previously correlated to MIS 9) is now dated to MIS 10 while the Middle Paleolithic is dated to MIS 7. Lithic analyses are preceded by taphonomic evaluations. The Levallois method of the Middle Paleolithic assemblage is an innovation characterized by the production of thin flake blanks without cortex. In contrast, the small tool blanks of the Acheulian were either pebbles or thick flakes with some cortex. They provided a relatively easy manual prehension. The choice of Levallois thin flake blanks in the Middle Paleolithic assemblage suggest that the new technology is most likely related to the emergence of hafting. Accordingly, the oldest direct evidence of hafting technology is from the site of Campitello Quarry in Tuscany (Central Italy) where birch-bark tar, found on the proximal part of two flint flakes, is dated to the end of MIS 7. Nevertheless, a peculiar feature of the Middle Paleolithic at Torre in Pietra is the continuous presence of small tool blanks on pebbles and cores and on thick flake albeit at a much lower frequency than in the older Acheulian industries. The adoption of the new technology is thus characterized by innovation combined with a degree of stability. The persistence of these habits in spite of the introduction of an innovative technique underlies the importance of cultural transmission and conformity in the behavior of Neandertals.

Lancefield Swamp, south-eastern Australia, was one of the earliest sites to provoke interest in Pleistocene faunal extinctions in Sahul (Pleistocene Australia-New Guinea). The systematic investigation of the deposit in the early 1970s identified megafaunal remains dominated by the 100–200 kg kangaroo Macropus giganteus titan. Associated radiocarbon ages indicated that the species was extant until c.30,000 BP, suggesting significant overlap with human settlement of Sahul. This evidence was inconsistent with contemporary models of rapid human-driven extinctions. Instead, researchers inferred ecological tethering of fauna at Lancefield Swamp due to intense drought precipitated localised mass deaths, consistent with Late Pleistocene climatic variability. Later investigations in another part of the swamp, the Mayne Site, remote to the initial investigations, concluded that mass flow disturbed this area, and Electron Spin Resonance (ESR) analyses on megafauna teeth returned wide-ranging ages. To clarify site formation processes and dating of Lancefield Swamp, we excavated new test-pits next to previous trenches in the Classic and Mayne Sites. We compared absolute chronologies for sediments and teeth, sedimentology, palaeo-topography, taphonomy, and macropod age at death across the swamp. Luminescence dating of sediments and ESR analysis of teeth returned ages between c.80,000 and 45,000 years ago. We found no archaeological remains in the bone beds, and evidence of carnivore activity and fluvial action, in the form of reactivated spring flow. The latter disturbed limited parts of the site and substantial areas of the bone beds remained intact. The faunal assemblage is dominated by megafaunal adult Macropus, consistent with mass die-offs due to severe drought. Such droughts appear to have recurred over millennia during the climatic variability of Marine Isotope Stages 4 and 3. These events began tens of millennia before the first appearance of Aboriginal people in Sahul an

Na monografía clásica de Puig y Larraz (1896: 250-252) amiéntense delles cavidaes del Conceyu de Piloña2 , pero non la Cueva d’El Sidrón (Fig. 1). Esta conocíase, ensin dulda, dende la Guerra Civil y el maquis al servir d’abellugu a persiguíos políticos, y guarda una alcordanza imborrable nuna de les sos múltiples entraes, yá qu’ellí ta enterrada Olvido Otero González (1908-1938). Per El Sidrón pasaron munches persones a lo llargo de los años, pero en 1994 prodúxose’l descubrimientu per parte d’unos espeleólogos xixoneses d’unos güesos humanos que dieron un importante xiru a la conocencia de los nuesos antepasaos neandertales

Sulawesi is the largest and oldest island within Wallacea, a vast zone of oceanic islands separating continental Asia from the Pleistocene landmass of Australia and Papua (Sahul). By one million years ago an unknown hominin lineage had colonized Flores immediately to the south1, and by about 50 thousand years ago, modern humans (Homo sapiens) had crossed to Sahul2, 3. On the basis of position, oceanic currents and biogeographical context, Sulawesi probably played a pivotal part in these dispersals4. Uranium-series dating of speleothem deposits associated with rock art in the limestone karst region of Maros in southwest Sulawesi has revealed that humans were living on the island at least 40 thousand years ago (ref. 5). Here we report new excavations at Talepu in the Walanae Basin northeast of Maros, where in situ stone artefacts associated with fossil remains of megafauna (Bubalus sp., Stegodon and Celebochoerus) have been recovered from stratified deposits that accumulated from before 200 thousand years ago until about 100 thousand years ago. Our findings suggest that Sulawesi, like Flores, was host to a long-established population of archaic hominins, the ancestral origins and taxonomic status of which remain elusive.

The last interglacial maximum (Marine Isotope Substage 5e [MIS 5e], 128¿116 ka) is a distinctive event in recent Earth history. Shoreline successions of this age are important for calibrating climate models and defining the overall behaviour of the crust¿mantle system to fluctuating ice and ocean-water volumes. In a global context, the recently intensified interest in last interglacial shoreline successions has revealed considerable variability in the magnitude of sea-level rise during this time interval and highlighted the need to examine paleosea-level evidence from tectonically stable, far-field settings. Situated in the far-field of continental ice sheets and on the tectonically stable Gawler Craton, the 300 km coastal sector of western Eyre Peninsula between Fowlers Bay and Lake Newland in southern Australia represents an important region for defining the glacio-eustatic (ice-equivalent) sea-level attained during the last interglacial maximum based on the relative sea-level observations from this region. Low-energy, shoaling upward, peritidal bioclastic carbonate successions of the last interglacial (locally termed Glanville Formation) formed within back-barrier, estuarine¿lagoonal environments in the lee of eolianite barrier complexes (locally termed Bridgewater Formation) along this coastline. The well-preserved shelly successions (coquinas) contain diverse molluscan fossil assemblages including species no longer living in the coastal waters of South Australia (e.g. the Sydney cockle Anadara trapezia and the benthic foraminifer Marginopora vertebralis). The extent of amino acid racemisation (a measure of fossil age based on increasing d/l value) in a range of species, and in particular A. trapezia and Katelysia sp., confirms the time equivalence of the isolated embayment-fill successions, correlated with the informal type section of the Glanville Formation at Dry Creek, north of Adelaide. Preliminary U-series analyses on A. trapezia also suggest a correlation

Dating is basic for archaeological and paleontological investigations and results of different dating methods used in Azokh caves are described in this chapter. Fossils from Azokh were not dated by any method previously. Lithic technology and taxonomy suggested a middle Pleistocene age for Unit V (from where Acheulian industries and a human mandible fragment were recovered) while Units III and II yielded Mousterian industries indicating middle Paleolithic ages. Dates from Azokh by Electron Spin Resonance (ESR) previously published elsewhere were given before final calculations and they slightly differ from those given in this Appendix, which are the definitive dating results.

Recent excavations at the early Middle Pleistocene site of Mata Menge in the So'a Basin of central Flores, Indonesia, have yielded hominin fossils1 attributed to a population ancestral to Late Pleistocene Homo floresiensis2. Here we describe the age and context of the Mata Menge hominin specimens and associated archaeological findings. The fluvial sandstone layer from which the in situ fossils were excavated in 2014 was deposited in a small valley stream around 700 thousand years ago, as indicated by 40Ar/39Ar and fission track dates on stratigraphically bracketing volcanic ash and pyroclastic density current deposits, in combination with coupled uranium-series and electron spin resonance dating of fossil teeth. Palaeoenvironmental data indicate a relatively dry climate in the So'a Basin during the early Middle Pleistocene, while various lines of evidence suggest the hominins inhabited a savannah-like open grassland habitat with a wetland component. The hominin fossils occur alongside the remains of an insular fauna and a simple stone technology that is markedly similar to that associated with Late Pleistocene H. floresiensis.