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2. Biochar Derived from Water Hyacinth Biomass Chemically Activated for Dye Removal in Aqueous Solution

Author

Carneiro, Marcelo Teixeira, primary, Morais, Alan Ícaro Sousa, additional, de Carvalho Melo, André Luiz Ferreira, additional, Ferreira, Francisco José Lustosa, additional, Santos, Francisco Eroni Paz, additional, Viana, Bartolomeu Cruz, additional, Osajima, Josy Anteveli, additional, Bezerra, Roosevelt D. S., additional, Del Mar Orta Cuevas, Maria, additional, Peña-Garcia, Ramón Raudel, additional, Almeida, Luciano C., additional, and Silva-Filho, Edson C., additional

Published
2023
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3. Using Activated Biochar from Caryocar brasiliense Pequi Almonds for Removing Methylene Blue Dye in an Aqueous Solution.

Author

Melo, André Luiz Ferreira Carvalho, Carneiro, Marcelo Teixeira, Morais, Alan Ícaro Sousa, Viana, Bartolomeu Cruz, Santos, Francisco Eroni Paz, Osajima, Josy Anteveli, Bezerra, Roosevelt D. S., Peña-Garcia, Ramón Raudel, Almeida, Luciano C., Carrasco, Santiago Medina, and Silva-Filho, Edson C.

Subjects
METHYLENE blue, ADSORPTION capacity, BIOCHAR, COLOR removal in water purification, FOURIER transform infrared spectroscopy, AQUEOUS solutions, ALMOND
Abstract

Water pollution remains a global problem that urges researchers to develop new technologies aimed at environmental restoration. Here, this study aimed at obtaining an activated biochar from pequi almonds for dye removal. Before and after adsorption, the materials underwent characterization using techniques such as X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), Raman spectroscopy, and thermogravimetric analysis (TG). The biochar from the pequi almond was called BA, and the activated biochar from the pequi almond was called ABA. The influence of the pH, contact time, and adsorbate concentration on adsorption was investigated using the dye methylene blue. The morphological assessment revealed higher cracks and pores in the ABA than in the BA. The TG showed that the BA lost approximately 19% more mass than the ABA, indicating that activation occurred. The activation contributed to the decrease in the degree of disorder in the BA because of the increased number of graphitic carbon atoms (ordered) in the ABA, as observed via Raman. The adsorption kinetics followed a pseudo-second-order model, while the adsorption isotherms followed the Langmuir model. The BA adsorption capacity was 500.00 mg g−1, constituting a robust solution for dye removal from aqueous environments. Therefore, this implies the success of the process. [ABSTRACT FROM AUTHOR]

Published
2023
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4. Biochar Derived from Water Hyacinth Biomass Chemically Activated for Dye Removal in Aqueous Solution

Author

Universidad de Sevilla. Departamento de Química Analítica, Coordination Support in Higher Education (CAPES), National Council for Scientific and Technological Development (CNPq), Foundation of Support to Research of Piauí (FAPEPI), Carneiro, Marcelo Teixeira, Morais, Alan Ícaro Sousa, de Carvalho Melo, André Luiz Ferreira, Ferreira, Francisco José Lustosa, Santos, Francisco Eroni Paz, Viana, Bartolomeu Cruz, Orta Cuevas, María del Mar, Silva-Filho, Edson C., Universidad de Sevilla. Departamento de Química Analítica, Coordination Support in Higher Education (CAPES), National Council for Scientific and Technological Development (CNPq), Foundation of Support to Research of Piauí (FAPEPI), Carneiro, Marcelo Teixeira, Morais, Alan Ícaro Sousa, de Carvalho Melo, André Luiz Ferreira, Ferreira, Francisco José Lustosa, Santos, Francisco Eroni Paz, Viana, Bartolomeu Cruz, Orta Cuevas, María del Mar, and Silva-Filho, Edson C.

Abstract

Rapid industrial development has led to the use of numerous dyes responsible for significant water pollution worldwide. Adsorbents have been developed to treat these waters, mainly in the form of activated biochar, which has several advantages, one of which is its good surface characteristics, such as high surface area and pore volume. The objective of the investigation was to analyze the efficiency of removing the methylene blue model dye in aqueous solutions through the adsorption process using biochar chemically activated from the leaf and stem of water hyacinth (Eichhornio crassipes) as a bioadsorbent. This study carbonized the stem and leaf containing zinc chloride at 600 °C. The materials were characterized by different techniques and were tested for their ability to adsorb methylene blue. The activated stem and leaf biochars removed approximately 285.71 and 322.58 mg g−1 of the dye, respectively, indicating that the adsorption is more significant in the leaf. Pseudo-second-order kinetics was the most suitable model to describe dye adsorption on biochars, and the experimental isotherm data fit the Langmuir model. It is concluded that the application of activated water hyacinth biochar is a renewable resource with the potential for effluent treatment

Published
2023

6. Electrospun Poly(butylene-adipate-co-terephthalate)/Nano-hyDroxyapatite/Graphene Nanoribbon Scaffolds Improved the In Vivo Osteogenesis of the Neoformed Bone

Author

Vasconcellos, Luana Marotta Reis, primary, Santana-Melo, Gabriela F., additional, Silva, Edmundo, additional, Pereira, Vanessa Fernandes, additional, Araújo, Juliani Caroline Ribeiro, additional, Silva, André Diniz Rosa, additional, Furtado, André S. A., additional, Elias, Conceição de Maria Vaz, additional, Viana, Bartolomeu Cruz, additional, Marciano, Fernanda Roberta, additional, and Lobo, Anderson Oliveira, additional

Published
2021
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7. Morphological analysis of the TiN thin film deposited by CCPN technique

Author

e Silva, Heurison de Sousa, primary, Marciano, Fernanda Roberta, additional, de Menezes, Alan Silva, additional, Costa, Thercio Henrique de Carvalho, additional, de Almeida, Larissa Solano, additional, Rossino, Luciana Sgarbi, additional, Nascimento, Igor Oliveira, additional, de Sousa, Rômulo Ribeiro Magalhães, additional, and Viana, Bartolomeu Cruz, additional

Published
2020
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9. TiO2 Immobilized on Fibrous Clay as Strategies to Photocatalytic Activity

Author

Oliveira, Wemerson Vieira de, primary, Morais, Alan Ícaro Sousa, additional, Honorio, Luzia Maria Castro, additional, Trigueiro, Pollyana Aragão, additional, Almeida, Luciano Costa, additional, Garcia, Ramón Raudel Peña, additional, Viana, Bartolomeu Cruz, additional, Furtini, Marcelo B., additional, Silva-Filho, Edson Cavalcanti, additional, and Osajima, Josy Anteveli, additional

Published
2020
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10. High loads of nano-hydroxyapatite/graphene nanoribbon composites guided bone regeneration using an osteoporotic animal model

Author

Oliveira,Francilio Carvalho, Carvalho,Jancineide Oliveira, Gusmão,Suziete Batista Soares, Gonçalves,Licia de Sousa, Soares Mendes,Liana Martha, Freitas,Sérgio Antonio Pereira, Gusmão,Gustavo Oliveira de Meira, Viana,Bartolomeu Cruz, Marciano,Fernanda Roberta, Lobo,Anderson Oliveira, Oliveira,Francilio Carvalho, Carvalho,Jancineide Oliveira, Gusmão,Suziete Batista Soares, Gonçalves,Licia de Sousa, Soares Mendes,Liana Martha, Freitas,Sérgio Antonio Pereira, Gusmão,Gustavo Oliveira de Meira, Viana,Bartolomeu Cruz, Marciano,Fernanda Roberta, and Lobo,Anderson Oliveira

Abstract

Francilio Carvalho Oliveira,1,2,* Jancineide Oliveira Carvalho,1,2,* Suziete Batista Soares Gusmão,3 Licia de Sousa Gonçalves,2 Liana Martha Soares Mendes,4 Sérgio Antonio Pereira Freitas,2 Gustavo Oliveira de Meira Gusmão,5 Bartolomeu Cruz Viana,3,6 Fernanda Roberta Marciano,1,7,8 Anderson Oliveira Lobo1,3,8 1Institute of Science and Technology, Brasil University, Itaquera 08230-030, São Paulo, Brazil; 2University Center for Health, Humanities and Technology of Piauí, (UNINOVAFAPI), Teresina, Piauí, Brazil; 3LIMAV-Interdisciplinary Laboratory for Advanced Materials, Materials Science and Engineering Graduate Program, Technological Center, UFPI-Federal University of Piauí, Teresina 64049-550, Piaui, Brazil; 4Department of Specialized Medicine, Federal University of Piauí, Teresina 64017-775, Piaui, Brazil; 5Department of Physics, State University of Piaui, Teresina 64002-150, Piaui, Brazil; 6Department of Physics, Federal University of Piauí, Teresina 64049-550, Brazil; 7Nanomedicine Lab, Department of Chemical Engineering, Northeastern University, Boston, MA 02115, USA; 8Department of Chemistry, Massachusetts Institute of Technology, Cambridge, MA 02139, USA *These authors contributed equally to this work Background: It has been difficult to find bioactive compounds that can optimize bone repair therapy and adequate osseointegration for people with osteoporosis. The nano-hydroxyapatite (nHAp)/carbon nanotubes with graphene oxides, termed graphene nanoribbons (GNR) composites have emerged as promising materials/scaffolds for bone regeneration due to their bioactivity and osseointegration properties. Herein, we evaluated the action of nHAp/GNR composites (nHAp/GNR) to promote bone regeneration using an osteoporotic model.Materials and methods: First, three different nHAp/GNR (1, 2, and 3 wt% of GNR) were produced and characterized. For in vivo analys

Published
2019

11. Behavior and biocompatibility of rabbit bone marrow mesenchymal stem cells with bacterial cellulosic membrane

Author

Alencar, Marcello Silva, Carvalho, Yulla Klinger, Carvalho, Camila Ernanda, Feitosa, Matheus Tajra, Alves, Michel Muálem, Carvalho, Fernando Aécio de Amorim, Viana, Bartolomeu Cruz, Miglino, Maria Angélica, Jozala, Ângela Faustino, and Carvalho, Maria Acelina

Abstract

Background. Tissue engineering has been shown to exhibit great potential for the creation of biomaterials capable of developing into functional tissues. Cellular expansion and integration depends on the quality and surface-determinant factors of the scaffold, which are required for successful biological implants. The objective of this research was to characterize and evaluate the in vitro characteristics of rabbit bone marrow mesenchymal stem cells (BM-MSCs) associated with a bacterial cellulose membrane (BCM). We assessed the adhesion, expansion, and integration of the biomaterial as well as its ability to induce macrophage activation. Finally, we evaluated the cytotoxicity and toxicity of the BCM. Methods. Samples of rabbit bone marrow were collected. Mesenchymal stem cells were isolated from medullary aspirates to establish fibroblast colony-forming unit assays. Osteogenic, chondrogenic, and adipogenic differentiation was performed. Integration with the BCM was assessed by scanning electron microscopy at 1, 7, and 14 days. Cytotoxicity was assessed via the production of nitric oxide, and BCM toxicity was assessed with the MTT assay; phagocytic activity was also determined. Results. The fibroblastoid colony-forming unit (CFU-F) assay showed cells with a fibroblastoid morphology organized into colonies, and distributed across the culture area surface. In the growth curve, two distinct phases, lag and log phase, were observed at 15 days. Multipotentiality of the cells was evident after induction of osteogenic, chondrogenic, and adipogenic lineages. Regarding the BM-MSCs’ bioelectrical integration with the BCM, BM-MSCs were anchored in the BCM in the first 24 h. On day 7 of culture, the cytoplasm was scattered, and on day 14, the cells were fully integrated with the biomaterial. We also observed significant macrophage activation; analysis of the MTT assay and the concentration of nitric oxide revealed no cytotoxicity of the biomaterial. Conclusion. The BCM allowed the expansion and biointegration of bone marrow progenitor cells with a stable cytotoxic profile, thus presenting itself as a biomaterial with potential for tissue engineering.

Published
2018
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13. Photoelectrodes with titanate nanotubes sensitized by mesoporphyrin derivative from cashew nut shell

Author

Souza, Antonio Paulo Santos, primary, Almeida, Ana Fabíola Leite, additional, Conegero, Leila de Souza, additional, Viana, Bartolomeu Cruz, additional, Ferreira, Odair Pastor, additional, Alencar, Francisco Klayton Marques de, additional, Mazzetto, Selma Elaine, additional, Fechine, Pierre Basílio Almeida, additional, Graça, Manuel Pedro Fernandes, additional, and Freire, Francisco Nivaldo Aguiar, additional

Published
2019
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14. High loads of nano-hydroxyapatite/graphene nanoribbon composites guided bone regeneration using an osteoporotic animal model

Author

Oliveira, Francilio Carvalho, primary, Carvalho, Jancineide Oliveira, additional, Gusmão, Suziete Batista Soares, additional, Gonçalves, Licia de Sousa, additional, Soares Mendes, Liana Martha, additional, Freitas, Sérgio Antonio Pereira, additional, Gusmão, Gustavo Oliveira de Meira, additional, Viana, Bartolomeu Cruz, additional, Marciano, Fernanda Roberta, additional, and Lobo, Anderson Oliveira, additional

Published
2019
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15. Understanding the impact of crosslinked PCL/PEG/GelMA electrospun nanofibers on bactericidal activity

Author

De Paula, Mirian Michelle Machado, primary, Bassous, Nicole Joy, additional, Afewerki, Samson, additional, Harb, Samarah Vargas, additional, Ghannadian, Paria, additional, Marciano, Fernanda Roberta, additional, Viana, Bartolomeu Cruz, additional, Tim, Carla Roberta, additional, Webster, Thomas Jay, additional, and Lobo, Anderson Oliveira, additional

Published
2018
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18. Spectroscopic Analysis of a Theropod Dinosaur (Reptilia, Archosauria) from the Ipubi Formation, Araripe Basin, Northeastern Brazil

Author

da Silva, João Hermínio, primary, de Sousa Filho, Francisco Eduardo, additional, Saraiva, Antônio Álamo Feitosa, additional, Andrade, Nádia Amanda, additional, Viana, Bartolomeu Cruz, additional, Sayão, Juliana Manso, additional, Abagaro, Bruno Tavares de Oliveira, additional, Freire, Paulo de Tarso Cavalcante, additional, and Saraiva, Gilberto Dantas, additional

Published
2013
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