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Iron vanadate (FeVO4) nanoparticles (NPs) were synthesized using the sol‐gel auto‐combustion technique, yielding a triclinic nanostructure as revealed by X‐ray diffraction (XRD). The average size, crystalline structure, and morphology of the nanoparticles were analyzed using field emission scanning electron microscopy (FESEM). Energy‐dispersive X‐ray spectroscopy (EDX) was used to investigate the elemental content and purity of the FeVO4 NPs. Fourier transform infrared spectroscopy (FTIR) confirmed the surface stretching frequency of the FeVO4 NPs. Using a doctor blade, the produced FeVO4 NPs were applied to the surface of a stainless steel (SS) substrate. The fabricated electrode was examined using GCD, EIS, and CV techniques. The absorption spectra exhibited strong absorbance in the visible range, with a band gap of 3.43 eV. Additionally, the FeVO4 electrode showed supercapacitor properties, with a maximum specific capacitance of 1151.05 F/g in a 1 M KOH electrolyte at a scan rate of 5 mV/s. These results indicate that the prepared FeVO4 electrode is promising for supercapacitor application due to their excellent electrochemical performance. [ABSTRACT FROM AUTHOR]

Supercapacitors are the cutting-edge, high performing, and emerging energy storage devices in the future of energy storage technology. It delivers high energy and produces higher specific capacitances. This research study provides insights into supercapacitor materials and their potential applications by examining different battery technologies compared with supercapacitors' advantages and disadvantages. Transition metal hydroxides (cobalt hydroxides) have been studied to develop electrodes for supercapacitors and their use in various fields of energy and conversion devices. Cobalt-based metal oxides and hydroxides provide high-capacitance electrodes for supercapacitors. Metal hydroxides combine high electrical conductivity and excellent stability over time. The metal oxides used to prepare the electrodes for supercapacitors are cobalt-based metal oxides and hydroxides. It is stronger than most of the other oxides and has tremendous electrical conductivity. Cobalt hydroxides are also used in supercapacitors instead of other metal hydroxides, such as aluminum hydroxide, copper hydroxide, and nickel hydroxide. This study gives a complete overview of the preparation, synthesis, analysis, and characterization of cobalt hydroxide thin film electrodes by using the electrochemical deposition technique, parameters measurements, important characteristics, material properties, various applications, and future enhancement in supercapacitors. [ABSTRACT FROM AUTHOR]