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Air-coupled ultrasonic testing (ACUT) technique has been viewed as a viable solution in defect detection of advanced composites used in aerospace and aviation industries. However, the giant mismatch of acoustic impedance in air–solid interface makes the transmission efficiency of ultrasound low, and leads to poor signal-to-noise (SNR) ratio of received signal. The utilisation of signal-processing techniques in non-destructive testing is highly appreciated. This paper presents a wavelet filtering and phase-coded pulse compression hybrid method to improve the SNR and output power of received signal. The wavelet transform is utilised to filter insignificant components from noisy ultrasonic signal, and pulse compression process is used to improve the power of correlated signal based on cross-correction algorithm. For the purpose of reasonable parameter selection, different families of wavelets (Daubechies, Symlet and Coiflet) and decomposition level in discrete wavelet transform are analysed, different Barker codes (5–13 bits) are also analysed to acquire higher main-to-side lobe ratio. The performance of the hybrid method was verified in a honeycomb composite sample. Experimental results demonstrated that the proposed method is very efficient in improving the SNR and signal strength. The applicability of the proposed method seems to be a very promising tool to evaluate the integrity of high ultrasound attenuation composite materials using the ACUT. [ABSTRACT FROM AUTHOR]