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Measuring temperature in complex two-phase flows is crucial for understanding the dynamics of heat and mass transfer. In this Letter, we introduce a novel, to the best of our knowledge, optical approach based on the combination of two-photon laser-induced fluorescence (2p-LIF) imaging and two-color laser-induced fluorescence (2CLIF) for instantaneous temperature mapping of complex liquid media. Using Kiton Red (KR) and Rhodamine 560 (R560), a temperature sensitivity of 1.54 % / ∘ C has been achieved over a range of 17-60°C. The monitoring of two-dimensional transient temperature dynamics in the heating and degassing of water shows the efficiency of the 2p-2CLIF. This new approach contributes to the toolkit of optical temperature measurement techniques, providing a robust solution for studying transient scattering media and high-speed two-phase flows.

Previous research has shown that the polarization ratio technique allows the characterization of the surface mean diameter, D 21 , of droplets forming dilute sprays. However, its application to optically dense sprays has posed significant challenges due to the presence of multiple light scattering. Additionally, errors in measurement can arise from the angular dependence of the signal. In this Letter, we present a novel, to the best of our knowledge, method that addresses these challenges. Our approach combines the use of a telecentric objective with structured laser illumination, to both optimize light detection and suppress the unwanted intensity from multiple scattering. This approach enables the utilization of the polarization ratio technique for measuring the droplet size of challenging atomizing sprays. The method offers a promising solution for accurate and comprehensive spray characterization. It is applied, here, to a hollow-cone water spray running at 30, 50, and 70 bar injection pressure, reaching an optical depth up to three.