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As a result of conventional wire-forming processes, the residual stress distribution in wires is frequently unfavorable for subsequent forming processes such as bending operations. High tensile residual stresses typically occur in the near-surface region of the wires and can limit further application and processability of the semi-finished products. This paper presents an approach for tailoring the residual stress distribution by modifying the forming process, especially with regard to the die geometry and the influence of the drawing velocity as well as the wire temperature. The aim is to mitigate the near-surface tensile residual stresses induced by the drawing process. Preliminary studies have shown that modifications in the forming zone of the dies have a significant impact on the plastic strain and deformation direction, and the approach can be applied to effectively reduce the process-induced near-surface residual stress distributions without affecting the diameter of the product geometry. In this first approach, the process variant using three different drawing die geometries was established for the metastable austenitic stainless steel X5CrNi18-10 (1.4301) using slow (20 mm/s) and fast (2000 mm/s) drawing velocities. The residual stress depth distributions were determined by means of incremental hole drilling. Complementary X-ray stress analysis was carried out to analyze the phase-specific residual stresses since strain-induced martensitic transformations occurred close to the surface as a consequence of the shear deformation and the frictional loading. This paper describes the setup of the drawing tools as well as the results of the experimental tests.

High-strength, high-conductivity copper/silver-alloyed materials were prepared by cold-spray (CS) manufacturing. For DC high-field application at room temperature, bulk Cu/Ag (5% vol. Ag) alloys with high mechanical properties and high electrical conductivity can be obtained by CS and post-heat treatments. For pulsed-field application at liquid nitrogen temperature, bulk Cu/Ag (5% vol. Ag) alloys serve as precursors for room-temperature wire drawing. The Cu/Ag-alloyed bulk CS deposit presents a high yield strength of about 510 MPa with a corresponding electrical resistivity of 1.92 µΩ·cm (at 293 K). The Cu/Ag-alloyed wires show a very high ultimate tensile strength (1660 MPa at 77 K or 1370 MPa at 293 K) and low electrical resistivity (1.05 µΩ·cm at 77 K or 2.56 µΩ·cm at 293 K). Microstructural studies via STEM allow us to understand this very high level of mechanical strength. The results evidence that materials developed by CS exhibit very high mechanical properties compared to materials prepared by other routes, due to the high velocity of the deposited particles, which leads to high initial deformation rates and specific microstructural features.

This investigation aims to analyze the effect of homogenization heat treatment at 1240 °C for 2 and 6 h on the hardness, distribution, morphology, and chemical composition of the δ-ferrite and sigma phases in 316L stainless steel cast billet. A field emission scanning electron microscope, combined with electron back-scattered diffraction, a field emission electron probe microanalyzer with a wavelength dispersive spectrometer, and a Vickers microhardness tester are applied to identify various phase evolutions in the cast billet. The morphology of the δ-ferrite and sigma phases in the austenite matrix of the 316L cast billet are strongly related to the subsequent hot and cold wire drawings. The homogenization heat treatment is expected to provide a driving force to form spheroid interdendritic δ-ferrite and to minimize the amount of the brittle sigma intermetallic compound in the austenite matrix. The homogenization heat treatment at 1240 °C effectively spheroidized all δ-ferrites into blunt ones in the cast billet. The transformation of δ-ferrite into sigma is dominated by temperature and cooling rate. The fast air cooling after homogenization between 1240 and 850 °C retards the precipitation of the sigma in the δ-ferrite. There are two δ-ferrite transformation mechanisms in this experiment. The direct transformation of the δ-ferrite into sigma is observed in the as-cast 316L stainless steel billet. In contrast, the eutectoid transformation of the δ-ferrite into the sigma and austenite dominates the 316L cast billet homogenized at 1240 °C, with a slow furnace cooling rate.

Temperature rise of a specimen is a significant issue in drawing industries for wire, rod, and bar products, because an excessive increase in temperature during the drawing process can deteriorate the product quality and die life. The influence of the strain hardening exponent (n) of a wire on the temperature and strain distributions during wire drawing is investigated to understand its effect and to improve the quality of drawn wire. Finite element analysis and experiments are conducted to analyze the temperature and strain distributions of wires with n values of 0.0, 0.1, 0.5, and 1.0. The temperature increase of the wire augments as the n of the wire increases, despite the same amount of ideal plastic deformation, which is associated closely with the redundant work. The shear strain increases with the n of the specimen, which generates redundant work, leading to a high temperature rise. Similarly, drawing force increases with the n of the specimen, owing to the increase in redundant work with the n of the wire. In addition, the drawing force presents a linear relationship with the temperature rise of the wire. The drawing speed should be reduced and/or the cooling of wire and die should be strengthened during wire drawing, with increasing n value of the wire, because product quality and die wear are highly associated with the temperature rise of the wire in the deformation zone.

This paper describes research on the influence the technology of zinc-coated steel wire manufacturing has on the energy and force parameters of the drawing process, energy consumption and zinc expenditure. In the theoretical part of the paper, the theoretical work and drawing power were calculated. Calculations of the electric energy consumption have shown that usage of the optimal wire drawing technology results in a 37% drop in energy consumption, which in the course of a single year translates to savings equal to 13 TJ. This, in turn, results in the decrease of CO2 emissions by tons and a total decrease of the eco-costs by approximately EUR 0.5 mln. Drawing technology also influences the losses of the zinc coating and CO2 emissions. Properly adjusted parameters of the wire drawing technology allow obtaining a zinc-coating that is 100% thicker, translating to 265 tons of zinc, whose production generates 900 tons of CO2 and incurs eco-costs equal to EUR 0.6 mln. Optimal parameters for drawing, from the perspective of decreased CO2 emissions during the zinc-coated steel wire manufacturing, are as follows: usage of the hydrodynamic drawing dies, angle of the die reducing zone α = 5°, and drawing speed of 15 m/s.

In this paper, the effects of the skin pass technique on the residual stress and plastic strain fields generated in cold drawn pearlitic steel wires are analyzed. The aim is to find out the optimal conditions to be used in the design of a manufacturing process for obtaining more reliable structural components in terms of the main cause of failure: the hydrogen embrittlement (HE). To achieve this goal, diverse numerical simulations were performed by using finite elements (FE) and considering, on one hand, the first step of a real cold drawing chain, using (i) a conventional drawing die and (ii) modified drawing dies with different soft diameter reductions, and, on the other hand, numerical simulations by FE of the hydrogen diffusion assisted by stress and strain states to estimate the hydrogen distributions. Obtained results revealed the secondary reduction degree as a key parameter in the die design for reducing the drawing-induced residual stress. According to the results, low values of the reduction ratio cause radial distributions of residual stress with significant reductions at both the wire core and at the wire surface. In addition, the hydrogen accumulation at the prospective damage zone (near the wire surface) given by FE simulations is lower in the wires drawn with modified drawing dies including a skin pass zone.

Round-notched samples are commonly used for testing the susceptibility to hydrogen embrittlement (HE) of metallic materials. Hydrogen diffusion is influenced by the stress and strain states generated during testing. This state causes hydrogen-assisted micro-damage leading to failure that is due to HE. In this study, it is assumed that hydrogen diffusion can be controlled by modifying such residual stress and strain fields. Thus, the selection of the notch geometry to be used in the experiments becomes a key task. In this paper, different HE behaviors are analyzed in terms of the stress and strain fields obtained under diverse loading conditions (un-preloaded and preloaded causing residual stress and strains) in different notch geometries (shallow notches and deep notches). To achieve this goal, two uncoupled finite element (FE) simulations were carried out: (i) a simulation by FE of the loading sequences applied in the notched geometries for revealing the stress and strain states and (ii) a simulation of hydrogen diffusion assisted by stress and strain, for estimating the hydrogen distributions. According to results, hydrogen accumulation in shallow notches is heavily localized close to the wire surface, whereas for deep notches, hydrogen is more uniformly distributed. The residual stress and plastic strains generated by the applied preload localize maximum hydrogen concentration at deeper points than un-preloaded cases. As results, four different scenarios are established for estimating “a la carte” the HE susceptibility of pearlitic steels just combining two notch depths and the residual stress and strain caused by a preload.

The effect of the thermal properties of steels on wire drawing behavior has been investigated to understand and improve the wire drawing process. Finite element analysis and experimental tests were conducted to analyze the temperature distribution of the deformed specimens with different thermal properties. The thermal properties of twinning-induced plasticity (TWIP) steel were measured and compared with those of plain carbon steel. Based on the measurement of thermal properties, wire drawing behaviors were systematically compared with thermal conductivity of the specimen (k) using plain low-carbon steel with high k and TWIP steel with low k. The results revealed that the k of TWIP steel was approximately one third of that of low-carbon steel, and the thermal expansion coefficient of the TWIP steel was approximately 50% higher than that of low-carbon steel in the temperature range of 26–400 °C. The temperature distributions in the wire strongly depended on the k of the wire during wire drawing. TWIP steel exhibited higher maximum temperature, and took a longer time to attain the equilibrium temperature than low-carbon steel during wire drawing owing to the low k. The maximum temperature of the die increased with decreasing k of the wire, indicating that die wear can increase with decreasing k of the wire. Therefore, reducing the drawing speed is suggested for a wire with low k, such as high-alloyed metals, especially for TWIP steels.

In this article, a mathematical model of the wire’s average temperature change in the process of multiple drawing on high-speed straight-line drawing machines has been developed. The calculation results showed that the average temperature of the wire during a drawing at a speed of up to 45 m/s on straight-line drawing machines could reach 400 °C. Deformation heating of the wire during drawing does not exceed 60 °C, and heating due to sliding friction can reach 300 °C, depending on the friction coefficient, which ranges from 0.05 to 0.15. The average strain rates under the conditions of the modern high-speed drawing process reach 7000 s−1. Over the course of the research, it was found that there are no conditions for the occurrence of dynamic deformation aging due to impurity atoms of carbon, nitrogen and oxygen. At the same time, at the temperature and speed parameters of the high-speed wire drawing, conditions are created for the onset of the dynamic strain aging of steel in the presence of hydrogen atoms. Therefore, during heat treatment and pickling, it is necessary to exclude the hydrogenation of steel. It has been established that in order to exclude static strain aging of steel during drawing, it is necessary to prevent heating the wire above 180–200 °C.

The different behaviors of the mechanical properties of drawn and caliber-rolled wires with applied strain were investigated to determine the appropriate process between wire drawing and caliber rolling with consideration of materials and process conditions. Ferritic, pearlitic, and TWIP steels were drawn and caliber-rolled under the same process conditions. Caliber-rolled wires exhibited a hardening behavior in the early deformation stage and softening behavior in the later deformation stage compared with the drawn wires, regardless of the steel. The hardening behavior of the caliber-rolled wires was explained by the higher strain induced by caliber rolling compared with wire drawing, especially the higher amount of redundant work in caliber-rolled wire. The caliber-rolled wire had approximately 36% higher strain than the drawn wire and approximately 85% higher strain than nominal strain. The softening behavior of the caliber-rolled wire in later deformation stages was related to the Bauschinger effect or low-cycle fatigue effect caused by the roll geometries and loading conditions during caliber rolling. The different intersection points of the tensile strength between drawn and caliber-rolled wires with the steels were attributed to the different strain hardening rates of each steel. Between the options of the caliber rolling and wire drawing processes, the appropriate process should be selected according to the strain hardening rate of the material and the amount of plastic deformation. For instance, when the wires need to deform at high levels, wire drawing is the better process because of the appearance of the Bauschinger effect in caliber-rolled wire.

This paper describes the relations between microstructure, mechanical properties, and electromagnetic behavior of carbon steel wires submitted to different thermomechanical treatments. The electrical resistivity and bulk magnetic properties are determined through resistivity measurements down to 2 K and magnetic hysteresis loop measurements. In addition, magnetic domains are imaged by magnetic force microscopy despite the complex microstructures. The electromagnetic properties are mainly related to changes in the volume fraction, morphology, and distribution of the cementite phase within the α-ferrite matrix. Electrical conductivity and magnetic permeability increase in the order of martensite, tempered martensite, pearlite, proeutectoid ferrite-pearlite, spheroidite, and ferrite microstructures. The increase in carbon concentration enhances the electrons localization at atomic sites, assisting the covalent character of Fe–C interatomic bonds and thereby reducing conductivity. Moreover, the α-Fe3C interfaces that act as a physical barrier for dislocation slip in ferrite, affecting also the main free-paths for conductive electrons and magnetic domain walls displacements within the materials. As the electromagnetic behavior of steels results from individual contributions of microstructural elements that are often intrinsically related to one another, a careful interpretation of both electrical and magnetic responses is critical for a proper application of quality and process monitoring methods of carbon steel wires.

The paper describes the capability of magnetic softening of a coarse-grained bulk material by a severe deformation technique. Connecting the microstructure with magnetic properties, the coercive field decreases dramatically for grains smaller than the magnetic exchange length. This makes the investigation of soft magnetic properties of severely drawn pearlitic wires very interesting. With the help of the starting two-phase microstructure, it is possible to substantially refine the material, which allows the investigation of magnetic properties for nanocrystalline bulk material. Compared to the coarse-grained initial, pearlitic state, the coercivities of the highly deformed wires decrease while the saturation magnetization values increase—even beyond the value expectable from the individual constituents. The lowest coercivity in the drawn state is found to be 520 A m−1 for a wire of 24-µm thickness and an annealing treatment has a further positive effect on it. The decreasing coercivity is discussed in the framework of two opposing models: grain refinement on the one hand and dissolution of cementite on the other hand. Auxiliary measurements give a clear indication for the latter model, delivering a sufficient description of the observed evolution of magnetic properties.

The present study investigates, experimentally and numerically, the tensile behavior of copper-clad aluminum composite wires. Two fiber-matrix configurations, the conventional Al-core/Cu-case and a so-called architectured wire with a continuous copper network across the cross-section, were considered. Two different fiber arrangements with 61 or 22 aluminum fibers were employed for the architectured samples. Experimentally, tensile tests on the two types of composites show that the flow stress of architectured configurations is markedly higher than that of the linear rule of mixtures’ prediction. Transverse stress components and processing-induced residual stresses are then studied via numerical simulations to assess their potential effect on this enhanced strength. A set of elastic-domain and elastoplastic simulations were performed to account for the influence of Young’s modulus and volume fraction of each phase on the magnitude of transverse stresses and how theses stresses contribute to the axial stress-strain behavior. Besides, residual stress fields of different magnitude with literature-based distributions expected for cold-drawn wires were defined. The findings suggest that the improved yield strength of architectured Cu-Al wires cannot be attributed to the weak transverse stresses developed during tensile testing, while there are compelling implications regarding the strengthening effect originating from the residual stress profile. Finally, the results are discussed and concluded with a focus on the role of architecture and residual stresses.

The effects of die radius in a streamlined die on design factors, such as the distribution of strain, stress, temperature, damage, and drawing force of a wire, were investigated during wire drawing for a better understanding of streamlined die and improvement in drawing quality of the wire. A numerical simulation was performed with the die radius of the streamlined die. The behavior of the design factors of the drawn wire fabricated by the streamlined die was different from that of the conventional die and was highly dependent on the die radius. The different behaviors of the design factors with the die radius can be explained by the frictional work and redundant work of the wire with die angle. The temperature rise and drawing force were high at a greater die radius because of the great frictional stress and heating effect stemming from the high contact length of the wire and die. Meanwhile, the higher redundant work at the surface area with decreasing die radius led to higher strain inhomogeneity, effective stress, damage value, temperature rise, and drawing force due to the abrupt change in the metal flow of the wire stemming from the high die angle. After the optimization of several design factors with die radius, it was concluded that the optimum IDR values ranged from 0.14 to 0.18, indicating that a streamlined die with a radius of 70 to 90 mm was the most suitable in the present process condition. In particular, the damage value of the wire was reduced in this range of die radii compared to the conventional die.

The effect of changing the strain path on texture development, twin kinetics, and mechanical properties in twinning-induced plasticity steel was investigated to understand twinning behavior in more detail. Among the various plastic deformation processes, the wire drawing process was selected to achieve the aims of the study. Specimens of cold-drawn TWIP steel wire under the same effective strain but with different crystallographic textures were successfully fabricated using the effect of the wire drawing direction. Electron backscatter diffraction results showed that the drawn wires using both unidirectional (UD) and reverse-directional (RD) wire drawing processes were characterized as duplex fiber textures of major and minor . It was found that the RD wire had a higher fraction of component at both the center and surface areas compared to the UD wire, because the metal flow of the RD wire was beneficial for the development of a orientation. The pronounced crystallographic orientation of the RD wire activated the twinning rate and geometrically necessary dislocation density, leading to an increase in strength but a decrease in ductility. The strain path is as important as the amount of strain for strengthening the materials, especially those that are deformed by twinning.

The efforts to increase the operating speed of the wire drawing process play a crucial role regarding the industrial productivity. The problem is closely related to various features such as heat generation, material plastic deformation, as well as the friction at the wire/die interface. For instance, the introduction of specific lubricants at the interface between the die and the wire may efficiently reduce the friction or in another context, induce a difference in friction among different regimes, as for the case of hydrodynamic lubrication. The present study systematically explores various aspects concerning the drawing process of an electrolytic tough pitch copper wire. To be specific, the drawing speed, drawing force, die temperature, lubricant temperature, and stress distributions are analysed by using experimental as well as numerical approaches. The obtained results demonstrate how the drawing stress and temperature are affected by the variation of the friction coefficient, die geometry, and drawing speed. It is argued that such a study might help in optimizing the operational parameters of the wire drawing process, which further leads to the improvement of the lubrication conditions and product quality while minimizing the energy consumption during the process.

Metalworking is an essential process for the manufacture of machinery and equipment components. The design of the die geometry is an essential aspect of metalworking, and directly affects the resultant product’s quality and cost. As a matter of fact, a comprehensive understanding of the die bearing geometry plays a vital role in the die design process. For the specific case of wire drawing, however, few efforts have been dedicated to the study of the geometry of the bearing zone. In this regard, the present paper involves an attempt to investigate the effects of different geometries of the die bearing. For different forms of reduction as well as bearing zones, measurements are carried out for the wire-drawing process. Subsequently, by extracting the friction coefficients from the electrolytic tough pitch copper wire in cold-drawn essays, the numerical simulations are also implemented. We present the results on both the superficial and center radial tensions obtained by finite element methods. It is observed that the reduction of the friction coefficient leads to an increase in radial stress, while for a given friction coefficient, the substitution of the C-type die by the R-type one results in a decrease in the superficial radial stress of up to 93.27%, but an increase at the center of the material. Moreover, the die angle is found to play a less significant role in the resultant center radial stress, but it significantly affects the superficial radial stress. Lastly, R-type dies result in smaller superficial radial stress, with a change of up to 34.48%, but a slightly larger center radial stress up to 6.55% for different die angles. The implications of the present findings are discussed.

Owing to significant advantages of bioactivity and biodegradability, biodegradable metallic materials such as magnesium, iron, and zinc and their alloys have been widely studied over recent years. Metallic wires with superior tensile strength and proper ductility can be fabricated by a traditional metalworking process (drawing). Drawn biodegradable metallic wires are popular biodegradable materials, which are promising in different clinical applications such as orthopedic fixation, surgical staples, cardiovascular stents, and aneurysm occlusion. This paper presents recent advances associated with the application of biodegradable metallic wires used in dental and orthopedic fields. Furthermore, the effects of some parameters such as the surface modification, alloying elements, and fabrication process affecting the degradation rate as well as biocompatibility, bioactivity, and mechanical stability are reviewed in the most recent works pertaining to these materials. Finally, possible pathways for future studies regarding the production of more efficient biodegradable metallic wires in the regeneration of bone defects are also proposed.

Vibration power and amplitude are essential factors in ultrasonic drawing processes, especially for difficult-to-draw materials like titanium and its alloys. This paper presents a new composite power-superimposed ultrasonic vibrator for wire drawing which was driven by three separate ultrasonic transducers. The transducers were uniformly distributed around the circular cross section of the vibrator, with their axes along the radial direction and pointing to the center. The vibrator can concentrate the vibrational energy of multiple transducers and transform the radial vibration into a longitudinal vibrator because of the Poisson effect and therefore output larger vibration power and amplitude. In the paper, the four-terminal network method was used to establish the vibration equations of the vibrator. The FE model was established in ANSYS to investigate its characteristics under various excitation conditions. A prototype was manufactured and measurements were performed to verify the validation of FEA results. The results matched well with the theoretical results. It was found that the composite vibrator achieved an amplitude of about 40 μm when driven by square wave signals with 120° in phase difference, which implies a potential way of applying ultrasonic vibration to the processing of difficult-to-draw materials.

The paper describes the capability of magnetic softening of a coarse-grained bulk material by a severe deformation technique. Connecting the microstructure with magnetic properties, the coercive field decreases dramatically for grains smaller than the magnetic exchange length. This makes the investigation of soft magnetic properties of severely drawn pearlitic wires very interesting. With the help of the starting two-phase microstructure, it is possible to substantially refine the material, which allows the investigation of magnetic properties for nanocrystalline bulk material. Compared to the coarse-grained initial, pearlitic state, the coercivities of the highly deformed wires decrease while the saturation magnetization values increase-even beyond the value expectable from the individual constituents. The lowest coercivity in the drawn state is found to be 520 A m -1 for a wire of 24-µm thickness and an annealing treatment has a further positive effect on it. The decreasing coercivity is discussed in the framework of two opposing models: grain refinement on the one hand and dissolution of cementite on the other hand. Auxiliary measurements give a clear indication for the latter model, delivering a sufficient description of the observed evolution of magnetic properties.