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1. Repetitive Two-Step Method for o,o,p- and o,p-Oligophenylene Synthesis through Pd-Catalyzed Cross-Coupling of Hydroxyterphenylboronic Acid

Author

Miyuki Yamaguchi, Takeshi Kimura, Naomi Shinohara, and Kei Manabe

Subjects
palladium, Suzuki-Miyaura coupling, oligoarene, nonaflate, Organic chemistry, QD241-441
Abstract

A repetitive two-step method involving the Pd-catalyzed Suzuki-Miyaura coupling of hydroxyterphenylboronic acid and the subsequent nonaflation of the hydroxy group has been developed for the synthesis of oligophenylenes. This method readily afforded o,o,p- and o,p-oligophenylenes with defined chain lengths. X-ray crystallography was employed to obtain the structure of the o,p-oligophenylene 9-mer.

Published
2013
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