1. Effect of Initial Grain Size on Microstructure and Mechanical Properties of In Situ Hybrid Aluminium Nanocomposites Fabricated by Friction Stir Processing
- Author
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Ghasem Azimiroeen, Seyed Farshid Kashani-Bozorg, Martin Nosko, and Saeid Lotfian
- Subjects
AA1050 ,reactive friction stir processing ,in situ nanocomposites ,grain refinement ,EBSD ,annealing ,Technology ,Engineering (General). Civil engineering (General) ,TA1-2040 ,Biology (General) ,QH301-705.5 ,Physics ,QC1-999 ,Chemistry ,QD1-999 - Abstract
Friction stir processing (FSP) offers a unique opportunity to tailor the microstructure and improve the mechanical properties due to the combination of extensive strains, high temperatures, and high-strain rates inherent to the process. Reactive friction stir processing was carried out in order to produce in situ Al/(Al13Fe4 + Al2O3) hybrid nanocomposites on wrought/as-annealed (673 K) AA1050 substrate. The active mixture of pre-ball milled Fe2O3 + Al powder was introduced into the stir zone by pre-placing it on the substrate. Microstructural characterisation showed that the Al13Fe4 and Al2O3 formed as the reaction products in a matrix of the dynamically restored aluminium matrix. The aluminium matrix means grain size was found to decrease markedly to 3.4 and 2 μm from ~55 μm and 40–50 μm after FSP using wrought and as-annealed substrates employing electron backscattered diffraction detectors, respectively. In addition, tensile testing results were indicative that the fabricated surface nanocomposite on the as-annealed substrate offered a greater ultimate tensile strength (~160 MPa) and hardness (73 HV) than those (146 MPa, and 60 HV) of the nanocomposite formed on the wrought substrate.
- Published
- 2023
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