1. Comprehensive and Comparative Heat Treatment of Additively Manufactured Inconel 625 Alloy and Corresponding Microstructures and Mechanical Properties
- Author
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Victoria Luna, Leslie Trujillo, Ariel Gamon, Edel Arrieta, Lawrence E. Murr, Ryan B. Wicker, Colton Katsarelis, Paul R. Gradl, and Francisco Medina
- Subjects
Inconel 625 ,additive manufacturing techniques ,post-process heat treatment ,microstructures ,microindentation hardness ,tensile properties ,Production capacity. Manufacturing capacity ,T58.7-58.8 - Abstract
This study examines and compares the microstructures, Vickers microindentation hardness, and mechanical properties for additively manufactured (AM) samples built by a variety of AM processes: wire arc AM (WAAM), electron beam powder bed fusion (EB-PBF), laser wire direct energy deposition (LW-DED), electron beam direct energy deposition (EB-DED), laser-powered direct energy deposition (LP-DED), and laser powder bed fusion (L-PBF). These AM process samples were post-processed and heat-treated by stress relief annealing at 1066 °C, HIP at 1163 °C, and solution annealing treatment at 1177 °C. The resulting microstructures and corresponding microindentation hardnesses were examined and compared with the as-built AM process microstructures and hardnesses. Fully heat-treated AM process samples were mechanically tested to obtain tensile properties and were also evaluated and compared. Principal findings in this study were that high-temperature heat treatment >1100 °C of AM process-built samples was dominant and exhibited recrystallized, equiaxed grains containing fcc {111} annealing twins and second phase particles independent of the AM process, in contrast to as-built columnar/dendritic structures. The corresponding yield stress values ranged from 285 MPa to 371 MPa, and elongations ranged from 52% to 70%, respectively. Vickers microindentation hardnesses (HV) over this range of heat-treated samples varied from HV 190 to HV 220, in contrast to the as-built samples, which varied from HV 191 to HV 304.
- Published
- 2022
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