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1. A convenient, rapid, conventional heating route to MIDA boronates

Author

Andrew McGown, Anthony K. Edmonds, Daniel Guest, Verity L. Holmes, Chris Dadswell, Ramón González-Méndez, Charles A. I. Goodall, Mark C. Bagley, Barnaby W. Greenland, and John Spencer

Subjects
Heating, Molecular Structure, Chemistry (miscellaneous), boronic acid, MIDAs, heterocycles, Organic Chemistry, Drug Discovery, Molecular Medicine, Pharmaceutical Science, Physical and Theoretical Chemistry, Boronic Acids, Analytical Chemistry
Abstract

A cheap, conventional, sealed heating reactor proved to be a useful alternative to a microwave reactor in the synthesis of a >20-member MIDA boronate library (MIDA = N-methyliminodiacetic acid). Reaction times were 10 min and work-ups were minimal, saving on energy and solvent usage.

Published
2022

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