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The A356 aluminum alloy is a very commonly used alloy in the automotive industry, for parts such as pistons, cylinder heads, and connecting rods, for which the mechanical properties can be effectively increased by anodizing. In this work, oxide layers were formed in oxalic acid solution with defined parameters on A356 aluminum alloy and then studied by using a novel combination of the scanning electron microscope (SEM) and in-situ nanoindentation. The purpose of this research is to understand the relationship between the substrate and the oxide layer by examining its microstructure and nanohardness. Based on the experimental results showing special composite microstructure and corresponding high hardness, this alloy seems to be a good alternative for replacing steel brake disks in an environmentally conscious manner. [ABSTRACT FROM AUTHOR]

Cyclic loading always results in great damage to the pore structure and fractal characteristics of soft soil. Scanning electron microscope (SEM) can help collect data to describe the microstructure of soft soil. This paper conducted a series of SEM tests to interpret the effect of consolidation confining pressure, circulating dynamic stress ratios and overconsolidation ratio on soil's micro-pore structure and fractal characteristics. The results demonstrate that fractal dimension can well represent the complex characteristics of the microstructure of the soil; the larger the consolidation confining pressure, the greater the cyclic dynamic stress ratio, and the greater the overconsolidation ratio, the smaller the fractal dimension number of soil samples. Finally, an empirical fitting formula for cumulative strain considering microstructure parameters is established through data fitting. [ABSTRACT FROM AUTHOR]

Featured Application: The geopolymer concrete comprising fly ash and fluid catalytic cracking residue could be applied for producing eco-friendly precast concrete products in Vietnam, which are precast wall, panel, or brick. The use of fluid catalytic cracking (FCC) by-products as aluminosilicate precursors in geopolymer binders has attracted significant interest from researchers in recent years owing to their high alumina and silica contents. Introduced in this study is the use of geopolymer concrete comprising FCC residue combined with fly ash as the requisite source of aluminosilicate. Fly ash was replaced with various FCC residue contents ranging from 0–100% by mass of binder. Results from standard testing methods showed that geopolymer concrete rheological properties such as yield stress and plastic viscosity as well as mechanical properties including compressive strength, flexural strength, and elastic modulus were affected significantly by the FCC residue content. With alkali liquid to geopolymer solid ratios (AL:GS) of 0.4 and 0.5, a reduction in compressive and flexural strength was observed in the case of geopolymer concrete with increasing FCC residue content. On the contrary, geopolymer concrete with increasing FCC residue content exhibited improved strength with an AL:GS ratio of 0.65. Relationships enabling estimation of geopolymer elastic modulus based on compressive strength were investigated. Scanning electron microscope (SEM) images and X-ray diffraction (XRD) patterns revealed that the final product from the geopolymerization process consisting of FCC residue was similar to fly ash-based geopolymer concrete. These observations highlight the potential of FCC residue as an aluminosilicate source for geopolymer products. [ABSTRACT FROM AUTHOR]

The presented paper aims to describe the influence of accelerating admixtures on the properties and microstructure of cement pastes and mortars. Blended slag cement CEM II/B-S containing two different clinkers (differing amounts of siliceous and aluminous phases) and four types of accelerators (calcium nitrate, sodium hydroxide, cement kiln dust, and crystal seeds) were used in research. Compressive strength tests (after 12, 24, 48 h of curing), Scanning Electron Microscope (SEM) observations together with an Energy Dispersive Spectroscopy (EDS) analysis, Mercury Intrusion Porosimetry (MIP) tests, and X-ray diffraction (XRD) analysis were conducted. Results have shown that SEM and EDS examination of the microstructure of cement pastes modified with accelerating admixtures at the observed points did not reveal differences that would be sufficient to explain the changes in compressive strength. Still, the increase in amorphous phase content indicates a faster hydration reaction rate for all pastes modified with accelerating admixture. It is backed up also by lower non-hydrated compounds content. All admixtures accelerate the hydration reaction of calcium silicate phases of cement, but only NaOH and cement kiln dust (CKD) influence the aluminate phase reaction rate. The pore volume is independent of the clinker type, while the pore size distribution is not. [ABSTRACT FROM AUTHOR]

In this study, to explore the microstructure deformation mechanism of marine soft marine soil under cyclic loading, we analyzed the dynamic properties of soft marine soil under cyclic loading via dynamic consolidation compression testing. Then, using Image-Pro Plus (IPP) 6.0 image analysis software, and according to the dynamic consolidation compression test results and the images from a scanning electron microscope (SEM), we determined the weakening effect of soft soils under different consolidation confining pressures, different cyclic stress ratios, and different over-consolidation ratios. After dynamic consolidation and compression, the pore structure of undisturbed soft marine soil tends to compact, the degree of soil particle fragmentation intensifies, small pores increase, large pores decrease, the pores become more regular, and the distribution of pores is directional. Subsequently, for undisturbed soft marine soil, the higher the consolidated confining pressure, cyclic dynamic stress ratio, and over-consolidation ratio, the greater the damage to the pore structure, and the more obvious the structural weakening effect exhibited under cyclic loading. [ABSTRACT FROM AUTHOR]

The inorganic structure formed at the stage of setting of the geopolymer binder ensures high durability of the material under high-temperature conditions. However, changes in the microstructure of the material are observed. The purpose of the study was to analyze changes in the structure of geopolymer mortar after exposure to high temperatures T = 200, 400, 600, 800, and 1000 °C. Mortars with a binder based solely on fly ash (FA) and mixed in the 1:1 ratio with a binder containing fly ash and ground granulated blast-furnace slag (GGBFS) were tested. The descriptions of their microstructures were prepared based on digital microscope observations, scanning electron microscope (SEM) observations, EDS (energy dispersive spectroscopy) analysis, and mercury intrusion porosimetry (MIP) porosity test results. Changes in the material due to high temperature were observed. The differences in the microstructure of the samples are also visible in the materials that were not exposed to temperature, which was influenced by the composition of the materials. Porosity increases with increasing annealing temperature. The distribution of individual pores also changes. In both materials, the proportion of pores larger than 1000 nm increases with the temperature increase. Moreover, the number of cracks and their width also increases, reaching 20 µm in the case of GGBFS. Furthermore, the color of geopolymers has changed. The obtained results extend the current state of knowledge in the field of changes in the microstructure of geopolymers subjected to high temperature. [ABSTRACT FROM AUTHOR]

In the South China Sea, calcareous sand, as a natural foundation, has the features of low mechanical properties, including its compressive strength. With the development of South China Sea islands, the problems of calcareous sand foundation are encountered in the process. However, the experience of traditional pile foundation engineering could not be applied to calcareous sand. In this study, different proportions of curing agents were added to calcareous sand to improve the compressive strength. The quantitative analysis of the relationship between the unconfined compressive strength and microstructure of solidified calcareous sand is discussed. The unconfined compressive strength was gauged from unconfined compressive strength tests. Microscopic images, acquired using a scanning electron microscope (SEM), were processed using the Image-Pro Plus (IPP) image processing software. The microscopic parameters, obtained using IPP, include the average equivalent particle size (Dp), the average equivalent aperture size (Db), and the plane pore ratio (e). This research demonstrates that the curing agent could improve the compressive strength, which has a relation with the three microstructure parameters. The curing agent, through hydration reaction, generates hydration products, i.e., calcium silicate hydrate, calcium hydroxide, and calcite crystals. They adhere to the surface of the particles or fill the space between the particles, which helps increase the compressive strength. In addition, there is a good linear relationship between the macroscopic mechanics and the microscopic parameters. Using the mathematical relation between the macroscopic and microscopic parameters, the correlation can be built for macro-microscopic research. [ABSTRACT FROM AUTHOR]

This study aimed to investigate the effect of different drying methods, namely ultrasound-assisted vacuum drying (USV), vacuum drying (VD), and freeze-drying (FD), on the drying kinetics and some quality parameters of dried minced meat. In this study, USV was for the first time applied to the drying of minced meat. The USV and VD methods were conducted at 25 °C, 35 °C, and 45 °C. The different drying methods and temperatures significantly affected the drying time (p < 0.05). The USV method showed lower drying times at all temperatures. The rehydration values of the freeze-dried minced meat samples were higher than those obtained by the USV and VD techniques. The samples prepared using USV showed higher rehydration values than the vacuum dried samples for all temperatures. The effects of the different drying techniques and drying conditions on the microstructural properties of the minced meat samples were investigated using scanning electron microscope (SEM). The USV method resulted in higher porosity and a more open structure than the VD method. Total color differences (ΔE) for VD, USV, and FD were 8.27–20.81, 9.58–16.42, and 9.38, respectively, and were significantly affected by the drying methods and temperatures (p < 0.05). Higher drying temperature increased the ΔE value. Peroxide values (PV) significantly increased after the drying process, and samples treated with USV showed lower PV values than the VD treated samples. This study suggests that USV could be used as an alternative drying method for minced meat drying due to lower drying times and higher quality parameters. [ABSTRACT FROM AUTHOR]

An in situ scanning electron microscope (SEM) study was conducted on a super duplex stainless steel (SDSS) containing 0%, 5% and 10% σ -phase. The material was heat treated at 850 °C for 12 min and 15 min, respectively, to achieve the different amounts of σ -phase. The specimens were investigated at room temperature and at −40 °C. The microstructure evolution during the deformation process was recorded using electron backscatter diffraction (EBSD) at different strain levels. Both σ -phase and χ -phase were observed along the grain boundaries in the microstructure in all heat treated specimens. Cracks started to form after 3–4% strain and were always oriented perpendicular to the tensile direction. After the cracks formed, they were initially arrested by the matrix. At later stages of the deformation process, cracks in larger σ -phase constituents started to coalesce. When the tensile test was conducted at −40 °C, the ductility increased for the specimen without σ -phase, but with σ -phase present, the ductility was slightly reduced. With larger amounts of σ -phase present, however, an increase in tensile strength was also observed. With χ -phase present along the grain boundaries, a reduction of tensile strength was observed. This reduction seems to be related to χ -phase precipitating at the grain boundaries, creating imperfections, but not contributing towards the increase in strength. Compared to the effect of σ -phase, the low temperature is not as influential on the materials performance. [ABSTRACT FROM AUTHOR]