Search

The evaluation of the impact of plasma-facing components damage on subsequent plasma operation is an important issue for ITER. During the first phase of the operation of WEST, a few ITER-like divertor plasma-facing units (PFUs) have been installed on the lower divertor. One PFU was pre-damaged under electron beam gun thermal loading, before its installation in WEST, and the subsequent evolution of the damage was studied after the WEST plasma exposure. This paper presents the procedure followed to get the pre-damaged PFU. It consists of the characterization of the response of tungsten samples representative of WEST PFU under high heat flux (HHF) loading, the selection of damage (namely, small cracks, crack network, crack network, and W melt droplets). Finally, according to the WEST plasma loading conditions, the blocks with damage within the PFU and the position of the pre-damaged PFU on the WEST lower divertor are attributed. The first results obtained after an initial plasma exposure in WEST lead to the assessment, as expected with regard to the heat loading conditions, that no major surface aspect modification was found. This result emphasized the possibility of implementing as pre-damaged small droplets of melted tungsten in a high heat-loaded zone for a future WEST experimental campaign.

Tungsten–tantalum (W-Ta) alloys for the application to fusion reactor divertor were developed to overcome the issues of W related to the low temperature brittleness, embrittlement by recrystallization, and embrittlement by neutron irradiation. In the present study, the response to cyclic thermal shock tests as well as the fundamental mechanical properties of W-3%Ta and pure W were investigated, which simulated a transient heat load event in the actual divertor environment. Because it was concerned that the effect of deuterium (D) plasma exposure might be much more pronounced in the Ta-alloyed materials, the thermal shock tests were performed under the background steady state D-plasma exposure. Based on the present study, W-3%Ta might be a competitive alloy system from the viewpoint of thermo-mechanical response in the actual divertor environment as well as the fundamental mechanical properties and resistance to recrystallization.

Six tungsten grades were irradiated in the Belgian material test reactor (BR2) and characterized by Vickers hardness tests in order to investigate the irradiation-induced hardening. These tungsten grades included: Plansee (Austria) ITER specification tungsten, ALMT (Japan) ITER specification tungsten, two products from KIT (Germany) produced by powder injection molding (PIM) and strengthened by 1% TiC and 2% Y2O3 dispersed particles, and rolled tungsten strengthened by 0.5% ZrC from ISSP (China). The materials were irradiated face-to-face at three temperatures equal to 600 °C, 1000 °C, and 1200 °C to the dose of ∼1 dpa. The Vickers hardness tests under 200 gf (HV0.2) were performed at room temperature. The Vickers hardness increases as the irradiation temperature increases from 600 to 1000 °C for all materials, except for the ZrC-reinforced tungsten, for which the increase of hardness does not depend on irradiation temperature. The irradiation-induced hardness decreases after irradiation at 1200 °C. This is a result of defect annealing enhanced by thermally activated diffusion. However, even at 1200 °C, the impact of neutron irradiation on the hardness increase remains significant; the hardness increases by ∼30 to 60% compared to the non-irradiated value. In the case of TiC-strengthened material, the irradiation hardening progressively raises with irradiation temperature, which cannot be explained by the accumulation of neutron irradiation defects solely.

High ductile-to-brittle transition temperature, recrystallization-induced embrittlement, and neutron-irradiation-induced embrittlement are potential drawbacks related to the mechanical properties of tungsten (W) for plasma facing materials of fusion reactor divertors. To improve the mechanical properties, resistance to recrystallization and neutron irradiation, W materials modified by potassium doping and alloying by rhenium have been developed. In this paper, thermal shock behaviors of these W materials under high heat flux tests were investigated, which simulated an edge localized mode of plasma occurring in fusion reactors as a transient event. The thermal shock tests were performed with an electron beam facility, JUDITH 1, and post-mortem analyses to evaluate the damage caused by the thermal shock tests were carried out.

16th International Conference on Plasma-Facing Materials and Components for Fusion Applications

In the experimental fusion reactor ITER, beryllium will be applied as first wall armor material. However, the ITER-like wall project at JET already experienced that the relatively low melting temperature of beryllium can easily be exceeded during plasma operation. Therefore, a detailed study was carried out on S-65 beryllium under various transient, ITER-relevant heat loads that were simulated in the electron beam facility JUDITH 1. Hereby, the absorbed power densities were in the range of 0.15–1.0 GW m−2 in combination with pulse durations of 1–10 ms and pulse numbers of 1–1000. In metallographic cross sections, the emergence of a transition region in a depth of ~70–120 µm was revealed. This transition region was characterized by a strong segregation of oxygen at the grain boundaries, determined with energy dispersive x-ray spectroscopy element mappings. The oxide segregation strongly depended on the maximum temperature reached at the end of the transient heat pulse in combination with the pulse duration. A threshold for this process was found at 936 °C for a pulse duration of 10 ms. Further transient heat pulses applied to specimens that had already formed this transition region resulted in the overheating and melting of the material. The latter occurred between the surface and the transition region and was associated with a strong decrease of the thermal conductivity due to the weakly bound grains across the transition region. Additionally, the transition region caused a partial separation of the melt layer from the bulk material, which could ultimately result in a full detachment of the solidified beryllium layers from the bulk armor. Furthermore, solidified beryllium filaments evolved in several locations of the loaded area and are related to the thermally induced crack formation. However, these filaments are not expected to account for an increase of the beryllium net erosion.

Surface damage and structure evolution of the full tungsten ITER divertor under transient heat loads is a key concern for component lifetime and plasma operations. Recrystallization caused by transients and steady-state heat loads can lead to degradation of the material properties and is therefore one of the most serious issues for tungsten armor. In order to investigate the thermal response of the recrystallized tungsten under edge localized mode-like transient thermal loads, fully recrystallized tungsten samples with different average grain sizes are exposed to cyclic thermal shocks in the electron beam facility JUDITH 1. The results indicate that not only does the microstructure change due to recrystallization, but that the surface residual stress induced by mechanical polishing strongly influences the surface cracking behavior. The stress-free surface prepared by electro-polishing is shown to be more resistant to cracking than the mechanically polished one. The resulting surface roughness depends largely on the loading conditions instead of the recrystallized-grain size. As the base temperature increases from room temperature to 400 °C, surface roughening mainly due to the shear bands in each grain becomes more pronounced, and sub-grains (up to 3 μm) are simultaneously formed in the sub-surface. The directions of the shear bands exhibit strong grain-orientation dependence, and they are generally aligned with the traces of {1 1 2} twin habit planes. The results suggest that twinning deformation and dynamic recrystallization represent the predominant mechanism for surface roughening and related microstructure evolution.

ITER first wall (FW) panels are irradiated by energetic neutrons during the nuclear phase. Thus, an irradiation and high heat flux testing programme is undertaken by the ITER organization in order to evaluate the effects of neutron irradiation on the performance of enhanced heat flux (EHF) FW components. The test campaign includes neutron irradiation (up to 0.6–0.8 dpa at 200 °C–250 °C) of mock-ups that are representative of the final EHF FW panel design, followed by thermal fatigue tests (up to 4.7 MW m−2). Mock-ups were manufactured by the same manufacturing process as proposed for the series production. After a pre-irradiation thermal screening, eight mock-ups will be selected for the irradiation campaigns. This paper reports the preparatory work of HHF tests and neutron irradiation, assessment results as well as a brief description of mock-up manufacturing and inspection routes.

The broad array of expected loading conditions in a fusion reactor such as ITER necessitates high requirements on the plasma facing materials (PFMs). Tungsten, the PFM for the divertor region, the most affected part of the in-vessel components, must thus sustain severe, distinct exposure conditions. Accordingly, comprehensive experiments investigating sequential and simultaneous thermal and particle loads were performed on double forged pure tungsten, not only to investigate whether the thermal and particle loads cause damage but also if the sequence of exposure maintains an influence. The exposed specimens showed various kinds of damage such as roughening, blistering, and cracking at a base temperature where tungsten could be ductile enough to compensate the induced stresses exclusively by plastic deformation (Pintsuk et al 2011 J. Nucl. Mater. 417 481–6). It was found out that hydrogen has an adverse effect on the material performance and the loading sequence on the surface modification.

Powder injection molding (PIM) was used to produce pure and particle reinforced W materials to be qualified for the use as plasma facing material. As alloying elements La2O3, Y2O3, TiC, and TaC were chosen with a particle size between 50 nm and 2.5 μm, depending on the alloying element. The fabrication of alloyed materials was done for different compositions using powder mixtures. Final sintering was performed in H2 atmosphere at 2400 °C resulting in plates of 55 × 22 × 4 mm3 with ~98% theoretical density. The qualification of the materials was done via high heat flux testing in the electron beam facility JUDITH-1. Thereby, ELM-like 1000 thermal shock loads of 0.38 GW m−2 for 1 ms and 100 disruption like loads of 1.13 GW m−2 for 1 ms at a base temperature of 1000 °C were applied. The obtained damage characteristics, i.e. surface roughening and crack formation, were qualified versus an industrially manufactured pure reference tungsten material and linked to the material's microstructure and mechanical properties.

The impact on the deuterium retention of simultaneous exposure of tungsten to a steady-state plasma and transient cyclic heat loads has been studied in the linear PSI-2 facility with the main objective of qualifying tungsten (W) as plasma-facing material. The transient heat loads were applied by a high-energy laser, a Nd:YAG laser (λ = 1064 nm) with an energy per pulse of up to 32 J and a duration of 1 ms. A pronounced increase in the D retention by a factor of 13 has been observed during the simultaneous transient heat loads and plasma exposure. These data indicate that the hydrogen clustering is enhanced by the thermal shock exposures, as seen on the increased blister size due to mobilization and thermal production of defects during transients. In addition, the significant increase of the D retention during the simultaneous loads could be explained by an increased diffusion of D atoms into the W material due to strong temperature gradients during the laser pulse exposure and to an increased mobility of D atoms along the shock-induced cracks. Only 24% of the retained deuterium is located inside the near-surface layer (d

Stress-relieved pure tungsten received three damage levels (0.10, 0.25 and 0.50 dpa) by self-tungsten ion beam irradiation at room temperature. Positron annihilation spectroscopy showed the formation of mono-vacancies and vacancy clusters after ion beam exposure. In the first irradiation step (0–0.10 dpa) some splitting up of large vacancy clusters occurred which became more numerous. For increasing dose to 0.25 dpa, growth of the vacancy clusters was seen. At 0.50 dpa a change in the defect formation seems to occur leading to a saturation in the lifetime signal obtained from the positrons. Nano-indentation on the cross-sections showed a flat damage depth distribution profile. The nano-indentation hardness increased for increasing damage dose without any saturation up to 0.50 dpa. This means that other defects such as dislocation loops and large sized voids seem to contribute.

The experimental fusion reactor ITER, currently under construction in Cadarache, France, is transferring the nuclear fusion research to the power plant scale. ITER's first wall (FW), armoured by beryllium, is subjected to high steady state and transient power loads. Transient events like edge localized modes not only deposit power densities of up to 1.0 GW m−2 for 0.2–0.5 ms in the divertor of the machine, but also affect the FW to a considerable extent. Therefore, a detailed study was performed, in which transient power loads with absorbed power densities of up to 1.0 GW m−2 were applied by the electron beam facility JUDITH 1 on beryllium specimens at base temperatures of up to 300 °C. The induced damage was evaluated by means of scanning electron microscopy and laser profilometry. As a result, the observed damage was highly dependent on the base temperatures and absorbed power densities. In addition, five different classes of damage, ranging from 'no damage' to 'crack network plus melting', were defined and used to locate the damage, cracking, and melting thresholds within the tested parameter space.

Experimental simulations of ITER-like transient events with relevant surface heat load parameters (energy density up to 1.1 MJ/m2 and the pulse duration of 0.25 ms) as well as particle loads (varied in wide range from 1023 to 1027 ion/m2 s) were carried out with a quasistationary plasma accelerator QSPA Kh-50. Particular attention was paid to elaboration of damage of tungsten as a main candidate material for ITER divertor surfaces and also as prospective material for DEMO design. Erosion features, cracks evolution and changes in their thickness with increasing exposition dose are studied for different W grades, including deformed material with elongated grains, as well as WTa5 and sintered tungsten.

This paper presents the results of tungsten irradiation experiments performed with three plasma facilities: the QSPA Kh-50 quasi-steady-state plasma accelerator, the PPA pulsed plasma gun and the magneto-plasma compressor. Targets made of different kinds of tungsten (sintered, rolled and deformed) were irradiated with powerful plasma streams at heat fluxes relevant to edge-localized modes in ITER. The irradiated targets were analyzed and two different meshes of cracks were identified. It has been shown that the major cracks do not depend on the tungsten grade. This has been attributed to ductile-to-brittle transition effects. Meshes of inter-granular micro-cracks were detected for energy loads above the melting threshold and these were probably caused by the re-solidification process. The blister-like and cellular-like structures were observed on sample surfaces exposed to helium and hydrogen plasmas.

14th International Conference on Plasma-Facing Materials and Components for Fusion Applications Foreword

Cracking thresholds and crack patterns in tungsten targets after repetitive ITER-like edge localized mode (ELM) pulses have been studied in recent simulation experiments by laser irradiation. The tungsten specimens were tested under selected conditions to quantify the thermal shock response. A Nd:YAG laser capable of delivering up to 32 J of energy per pulse with a duration of 1 ms at the fundamental wavelength λ = 1064 nm has been used to irradiate ITER-grade tungsten samples with repetitive heat loads. The laser exposures were performed for targets at room temperature (RT) as well as for targets preheated to 400 °C to measure the effects of the ELM-like loading conditions on the formation and development of cracks. The magnitude of the heat loads was 0.19, 0.38, 0.76 and 0.90 MJ m−2 (below the melting threshold) with a pulse duration of 1 ms. The tungsten surface was analysed after 100 and 1000 laser pulses to investigate the influence of material modification by plasma exposures on the cracking threshold. The observed damage threshold for ITER-grade W lies between 0.38 and 0.76 GW m−2. Continued cycling up to 1000 pulses at RT results in enhanced erosion of crack edges and crack edge melting. At the base temperature of 400 °C, the formation of cracks is suppressed.

Experimental simulations of ITER edge-localized mode have been performed with a Kh-50 quasi-stationary plasma accelerator. Heat loads exceeded the tungsten melting threshold. Droplet splashing and the solid dust ejection were observed. Droplets were emitted during the plasma exposure and dust generation dominated after the end of a plasma pulse, at the time of the material cooling. A decrease in the droplet velocity at an increase in the surface heat load was observed. It could be attributed to growing sizes of the droplets at higher energy loads. After one hundred pulses were performed at loads below the tungsten melting and above the cracking threshold, some porosity appeared. Such defects achieved dimensions of several tens of ?m. A heat load amounting to half the cracking threshold (0.3?MJ?m?2) could lead to the appearance of fatigue cracks after 100 plasma pulses. In this case the appearance of cracks could be caused by the accumulation and redistribution of linear defects (dislocations) in the affected tungsten layer.

Transient thermal loads in magnetic confinement experiments such as ITER have a strong impact on the material degradation of the plasma-facing components. In particular, the thermal loads for plasma-facing components in nuclear fusion devices are extraordinarily high. Within the ITER-like wall project, realized at JET, some of the plasma-facing components in the divertor region are made of tungsten-coated carbon fiber composite (CFC). These tungsten coatings were tested under ELM (edge-localized modes)-like loading conditions in an electron beam material testing facility to determine the thermal shock resistance. The failure occurrence and damage thresholds depending on base temperature and absorbed power density with special emphasis on the microstructure of the underlying CFC substrate are described in detail.

The thermal shock performances of two new tungsten grades with 1 and 5 wt% of tantalum were characterized with the electron beam facility JUDITH 1. As a reference material, ultra-high-purity tungsten (W-UHP) with a purity of 99.9999 wt% was used. The induced thermal shock crack networks and surface modifications were analysed by a scanning electron microscope, light microscopy and laser profilometry. Damage and cracking thresholds were defined for all materials as a function of absorbed power density and base temperature. The materials showed significantly different thermal shock behaviour, which is, among others, expressed by differences in cracking patterns, i.e. crack distance and depth. These results allow us to quantify the influence of the materials' mechanical and thermal properties on the thermal shock performance. Furthermore, the specific grain structure of the materials has a significant influence on crack propagation towards the bulk material.

Plasma facing components in future thermonuclear fusion devices will be subjected to intense transient thermal loads due to type I edge localized modes (ELMs), plasma disruptions, etc. To exclude irreversible damage to the divertor targets, local energy deposition must remain below the damage threshold for the selected wall materials. For monolithic tungsten (pure tungsten and tungsten alloys) power densities above ≈0.3 GW m−2 with 1 ms duration result in the formation of a dense crack network. Thin tungsten coatings for the so-called ITER-like wall in JET, which have been deposited on a two-directional carbon–fibre composite (CFC) material, are even less resistant to thermal shock damage; here the threshold values are by a factor of 2 lower. First ELM-simulation experiments with high cycle numbers up to 104 cycles on actively cooled bulk tungsten targets do not reveal any cracks for absorbed power densities up to 0.2 GW m−2 and ELM-durations in the sub-millisecond range (0.8 ms); at somewhat higher power densities (0.27 GW m−2, Δt = 0.5 ms) cracks have been detected for 106 cycles.