181 results on '"Microwave power"'
Search Results
2. Drying kinetics and quality characteristics of microwave-assisted hot air dried beef chips
- Author
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Elif Aykın-Dinçer, Büşra Atlı, Ayşegül Çalışkan, Seda Canavar, and Özge Çakmak
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Materials science ,Microwave power ,Kinetics ,Spice ,Metals and Alloys ,Ceramics and Composites ,Electrical and Electronic Engineering ,Condensed Matter Physics ,Quality characteristics ,Pulp and paper industry ,Dried meat ,Microwave assisted ,Electronic, Optical and Magnetic Materials - Abstract
In this study, the drying kinetics and quality characteristics of microwave-assisted hot air dried beef chips were investigated. For this purpose, beef slices were treated with spice mixture (4 g/1...
- Published
- 2021
3. Effect of input microwave power and insulation on microstructure and tensile properties of cast Al 7039 alloy produced at 2.45 GHz
- Author
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Apurbba Kumar Sharma and Radha Raman Mishra
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Work (thermodynamics) ,Materials science ,Alloy ,Microwave power ,Metals and Alloys ,020206 networking & telecommunications ,Astrophysics::Cosmology and Extragalactic Astrophysics ,04 agricultural and veterinary sciences ,02 engineering and technology ,engineering.material ,Condensed Matter Physics ,Microstructure ,040401 food science ,Electronic, Optical and Magnetic Materials ,Power (physics) ,0404 agricultural biotechnology ,Casting (metalworking) ,Ultimate tensile strength ,0202 electrical engineering, electronic engineering, information engineering ,Ceramics and Composites ,engineering ,Electrical and Electronic Engineering ,Composite material ,Microwave - Abstract
In the present work, microwave energy was used for casting Al 7039 alloy at 2.45 GHz in the ambient cavity environment. Effects of input power and insulation of the mould assembly during irradiatio...
- Published
- 2020
4. Mathematical Modeling and Drying Characteristics Investigation of Black Mulberry Dried by Microwave Method
- Author
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İbrahim Doymaz and Azmi Seyhun Kipcak
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0106 biological sciences ,Materials science ,Ecology ,business.industry ,Microwave power ,Astrophysics::Cosmology and Extragalactic Astrophysics ,04 agricultural and veterinary sciences ,Plant Science ,Horticulture ,Microwave method ,01 natural sciences ,0405 other agricultural sciences ,Process engineering ,business ,Agronomy and Crop Science ,Physics::Atmospheric and Oceanic Physics ,Microwave ,010606 plant biology & botany ,040502 food science - Abstract
In this study, microwave drying characteristics of black mulberry were studied at microwave power levels of 90, 180 and 360 W. Obtained experimental drying results were applied to seven mathematica...
- Published
- 2020
5. Investigation of magnetron injection locking and cascaded locking by solid-state microwave power source
- Author
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Yang Yan, Wenjie Fu, and Xiaoyun Li
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Materials science ,business.industry ,Microwave power ,Metals and Alloys ,Solid-state ,020206 networking & telecommunications ,Cooker ,04 agricultural and veterinary sciences ,02 engineering and technology ,Condensed Matter Physics ,040401 food science ,Electronic, Optical and Magnetic Materials ,Injection locking ,0404 agricultural biotechnology ,Cavity magnetron ,0202 electrical engineering, electronic engineering, information engineering ,Ceramics and Composites ,Optoelectronics ,Electrical and Electronic Engineering ,business - Abstract
The investigation of injection locking of cooker magnetron by a solid-state microwave power source is reported. Experimental results show that a 2.45 GHz cooker magnetron can be locked in continuou...
- Published
- 2019
6. A promising pulse-spouted microwave freeze drying method used for Chinese yam cubes dehydration: quality, energy consumption, and uniformity
- Author
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Lequn Zhou, Min Zhang, and Linlin Li
- Subjects
Materials science ,Pulse (signal processing) ,General Chemical Engineering ,Microwave power ,04 agricultural and veterinary sciences ,02 engineering and technology ,Energy consumption ,medicine.disease ,040401 food science ,Freeze-drying ,0404 agricultural biotechnology ,Quality (physics) ,020401 chemical engineering ,medicine ,Dehydration ,0204 chemical engineering ,Physical and Theoretical Chemistry ,Composite material ,Microwave - Abstract
Pulse-spouted microwave freeze drying (PSMFD) used for Chinese yam cubes was evaluated at three microwave power levels (400, 600, and 800 W). The drying characteristics, energy consumption, and qua...
- Published
- 2019
7. Optimization of microwave-assisted extraction of bioactive compounds from pistachio (Pistacia vera L.) hull
- Author
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Fahrettin Göğüş, Sibel Fadıloğlu, Derya Koçak Yanık, and Hatice Neval Özbek
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General Chemical Engineering ,Filtration and Separation ,Astrophysics::Cosmology and Extragalactic Astrophysics ,02 engineering and technology ,010501 environmental sciences ,01 natural sciences ,Microwave assisted ,020401 chemical engineering ,Hull ,Response surface methodology ,Physics::Chemical Physics ,0204 chemical engineering ,Solvent extraction ,0105 earth and related environmental sciences ,Physics::Biological Physics ,Quantitative Biology::Biomolecules ,Chromatography ,Pistacia ,biology ,Chemistry ,Process Chemistry and Technology ,Microwave power ,Extraction (chemistry) ,General Chemistry ,biology.organism_classification ,Condensed Matter::Soft Condensed Matter ,Solvent - Abstract
Phenolic compounds were extracted from pistachio hull using microwave-assisted solvent extraction (MASE). The effects of four parameters, microwave power, extraction time, solvent to sample...
- Published
- 2019
8. Editor message: farewell to our friend Bob Schiffmann
- Author
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Juan Antonio Aguilar-Garib
- Subjects
Microwave power ,Metals and Alloys ,Ceramics and Composites ,Media studies ,Sociology ,Electrical and Electronic Engineering ,Condensed Matter Physics ,Electronic, Optical and Magnetic Materials - Abstract
Many people are part of the history of the International Microwave Power Institute (IMPI): Founders, board, and general members, as well as speakers, and paper authors, among others. They have ofte...
- Published
- 2021
9. Influence of microwave power on mechanical properties of microwave-cured polyethylene/coir composites
- Author
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Manoj Kumar Singh and Sunny Zafar
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Materials science ,Materials Science (miscellaneous) ,Microwave power ,02 engineering and technology ,010501 environmental sciences ,Polyethylene ,021001 nanoscience & nanotechnology ,01 natural sciences ,chemistry.chemical_compound ,chemistry ,High-density polyethylene ,Coir ,Composite material ,0210 nano-technology ,Microwave ,0105 earth and related environmental sciences - Abstract
The present work deals with investigating the influence of microwave power on mechanical properties of 20 wt.% coir reinforced high-density polyethylene (HDPE) composites. Chopped coir/HDPE composi...
- Published
- 2018
10. Microwave power detection using ferroelectric thin film varactors
- Author
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Samuel G. Hirsch, Michael R. Gasper, M. Ivill, Ryan C. Toonen, and Nitin Parsa
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Materials science ,Microwave signals ,Astrophysics::Cosmology and Extragalactic Astrophysics ,02 engineering and technology ,Condensed Matter::Materials Science ,0202 electrical engineering, electronic engineering, information engineering ,Materials Chemistry ,Physics::Atomic Physics ,Electrical and Electronic Engineering ,Thin film ,Astrophysics::Galaxy Astrophysics ,business.industry ,Microwave power ,Anharmonicity ,020206 networking & telecommunications ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,Electronic, Optical and Magnetic Materials ,Dipole ,Control and Systems Engineering ,Ceramics and Composites ,Ferroelectric thin films ,Barium strontium titanate ,Optoelectronics ,0210 nano-technology ,business - Abstract
Ferroelectric, barium strontium titanate thin film varactors have been used to rectify and detect microwave signals with frequencies ranging from 2 GHz to 3 GHz. Anharmonic dipolar resonant...
- Published
- 2018
11. AHP-based procedure for optimization of microwave-assisted blackberry sugar osmotic process
- Author
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Chunfang Song, G.S.V. Raghavan, Guiyi Luo, Zhenfeng Li, Wanxiu Xu, Haiying Chen, and Tian Sang
- Subjects
Composite score ,General Chemical Engineering ,Microwave power ,Analytic hierarchy process ,04 agricultural and veterinary sciences ,Pulp and paper industry ,040401 food science ,Microwave assisted ,Power level ,0404 agricultural biotechnology ,Scientific method ,Physical and Theoretical Chemistry ,Sugar ,Residence time (statistics) ,Mathematics - Abstract
Due to the limitations of single index analysis, the merits and demerits of microwave-assisted permeation process cannot be comprehensively evaluated. However, the analytical hierarchy process (AHP) was applied to optimize the conditions of microwave-assisted diffusion of sugar in blackberry. In this paper, the results of a single-factor experiment were compared with blackberry preserved after the treatment of microwave. An orthogonal rotation test procedure was designed to calculate the composite score of preserved blackberry fruit using AHP, and to determine the optimum processing conditions based on sugar osmosis characteristics. The results showed that the sugar content, vitamin C (VC) content, and color difference of treated blackberry increased with the increase of microwave power, the residence time, and the resulting sugar concentration. The composite grade points are listed to show that the optimum results were as follows: power level, the residence time, and the sugar concentration were,...
- Published
- 2018
12. Experimental investigation on drying characteristic of titanium slag using microwave heating
- Author
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Ruan Rongsheng, Guo Chen, Chandrasekar Srinivasakannan, Jin Chen, Jinhui Peng, and Feng Kanglu
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Work (thermodynamics) ,Materials science ,General Chemical Engineering ,Metallurgy ,Microwave power ,Sample mass ,04 agricultural and veterinary sciences ,02 engineering and technology ,Titanium slag ,021001 nanoscience & nanotechnology ,040401 food science ,0404 agricultural biotechnology ,Microwave heating ,Physical and Theoretical Chemistry ,0210 nano-technology - Abstract
Drying characteristic of titanium slag using microwave heating is attempted in the present work, so as to assess the effect of microwave power and sample mass, and to understand the mechani...
- Published
- 2018
13. Control of microwave assisted macadamia drying
- Author
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Pakonkiad Poogungploy, Nattapol Poomsa-ad, and Lamul Wiset
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Temperature control ,food.ingredient ,Materials science ,Water activity ,Microwave power ,Metals and Alloys ,04 agricultural and veterinary sciences ,Condensed Matter Physics ,040401 food science ,Microwave assisted ,Macadamia nut ,Electronic, Optical and Magnetic Materials ,0404 agricultural biotechnology ,food ,Drying time ,Thermal radiation ,Ceramics and Composites ,Air drying ,Electrical and Electronic Engineering ,Composite material - Abstract
We studied the microwave-assisted macadamia drying, using surface temperature control and without surface temperature control as well as hot air drying, and assessed the drying time, drying rate, colour values, hardness and water activity of nuts and efficiency. The surface temperature of macadamia nuts was controlled between 60 and 80 °C using a thermal radiation detector. For drying without the surface temperature control, drying temperatures in the range of 40–60 °C and microwave power were controlled in the range of 1.6–4.4 Wg−1. We found that increase in microwave power and temperature had a positive effect with shorter drying time and increased drying rate. Microwave assisted hot air drying by surface temperature control led to a better quality product in respect of kernel brightness and suitable aw for storage, but a harder kernel. In addition, drying without surface temperature control had the highest energy efficiency followed by surface temperature control and hot air only. Considering q...
- Published
- 2018
14. Comparison between isothermal and microwave gasification of lignite char for high syngas production
- Author
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Guanghua Wang, X.-Y. Wei, Liu Yang, Fu Liu, Qingdong Wang, and Shao Qiutong
- Subjects
Materials science ,Renewable Energy, Sustainability and the Environment ,020209 energy ,Microwave power ,Energy Engineering and Power Technology ,02 engineering and technology ,Isothermal process ,Fuel Technology ,Nuclear Energy and Engineering ,Chemical engineering ,0202 electrical engineering, electronic engineering, information engineering ,Char ,Microwave ,Syngas - Abstract
Using the water of lignite as gasification agent, this paper mainly studies the influence of microwave and isothermal gasification on the syngas production and H2/CO ratio to obtain the maximum pos...
- Published
- 2017
15. Assessing the moisture migration during microwave drying of coal using low-field nuclear magnetic resonance
- Author
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Yidu Hong, Wang Rui, Baiquan Lin, Zheng Wang, He Li, Huang Zhanbo, and Tong Liu
- Subjects
Moisture ,Chemistry ,business.industry ,020209 energy ,General Chemical Engineering ,Microwave power ,Analytical chemistry ,02 engineering and technology ,Low field nuclear magnetic resonance ,0202 electrical engineering, electronic engineering, information engineering ,Free water ,Bound water ,Coal ,Physical and Theoretical Chemistry ,Composite material ,business ,Microwave - Abstract
Microwave drying of coal has the advantage of volumetric and selective heating, which saves energy and time. However, comprehensive assessment of the moisture migration during microwave drying is lacking. In this study, the low-field nuclear magnetic resonance (LF-NMR) was used for moisture characterization during microwave drying. Moisture migration occurs first in larger pores, whereas the smaller pores appear to remain water-saturated. As the microwave power increases, the drying capacity and drying rate both increase because high-power microwave can open the blind pores to promote moisture seepage. Furthermore, moisture migration during microwave drying is usually directional (i.e., along the bedding plane). The LF-NMR method provides a framework for the determination of moisture migration of coals.
- Published
- 2017
16. Study on microwave coherent power combining based on 20-kW S-band CW power-adjustable magnetrons
- Author
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Xiaojie Chen, Changjun Liu, Heping Huang, and Wan Jiang
- Subjects
010302 applied physics ,Materials science ,business.industry ,Microwave power ,Electrical engineering ,General Physics and Astronomy ,Power capacity ,Astrophysics::Cosmology and Extragalactic Astrophysics ,02 engineering and technology ,021001 nanoscience & nanotechnology ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Power (physics) ,0103 physical sciences ,Cavity magnetron ,S band ,Electrical and Electronic Engineering ,0210 nano-technology ,business ,Telecommunications ,Absorption (electromagnetic radiation) ,Microwave ,Power control - Abstract
In order to meet the requirements of large-power capacity in microwave-energy industry, the microwave coherent power combining by multiple magnetrons is a valid method to gain a large-power and high efficiency microwave source. In microwave energy applications, microwave absorption of industrial materials is varying in the heating duration and dependent on the dynamic change of materials. It is the first time that a 20-kW continuously power-adjustable injection-locked magnetron source has been achieved, and according to the experiment results, the maximum microwave coherent power combining output reaches 33.1 kW, and the coherent power combining efficiency is higher than 93%. The experiments show that the unbalanced output power between the two magnetrons does not affect greatly on the microwave coherent power combining efficiency. It is a great progress to develop the microwave power source which satisfies the power capacity requirement of microwave energy industry with the real-time power adjust...
- Published
- 2017
17. Microwave power absorption profile of detergent surfactant agglomerates during microwave heating
- Author
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Nigel Patrick Somerville Roberts, Muhammad Y. Sandhu, Qari Khalid, Ian Hunter, and Sharjeel Afridi
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Materials science ,General Chemical Engineering ,Microwave power ,Analytical chemistry ,04 agricultural and veterinary sciences ,02 engineering and technology ,Dielectric ,040401 food science ,Bulk density ,0404 agricultural biotechnology ,020401 chemical engineering ,Pulmonary surfactant ,Agglomerate ,Microwave heating ,0204 chemical engineering ,Physical and Theoretical Chemistry ,Absorption (electromagnetic radiation) ,Microwave - Abstract
The microwave energy absorption behavior of the linear alkylbenzene sulfonate (LAS) surfactant detergent agglomerates was studied while considering changes in the physical properties of the samples. Microwave heating was used to change the internal structure of the agglomerates to make a reduced density (fluffy) product. The absorption of energy within LAS samples indicated fluctuating trends as microwave heating progressed. This was associated with the dielectric properties of the material which are strongly dependent upon the nature (“free” or “bound”) and quantity of water present in them at any instant which changes during heating. Therefore, complete profiles of the energy absorbed by the samples have been recorded to determine their actual power absorption behavior/total energy consumption over time. The bulk density of the agglomerates decreased significantly when exposed to microwave fields. Hot air drying can be combined with microwave heating to reduce the total heating time. It has been...
- Published
- 2017
18. Update on Cooling for the ITER ECH Waveguide Transmission Line
- Author
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Timothy Jones, C.R. Luttrell, C. R. Schaich, D. N. Hill, Arnold Lumsdaine, Greg Hanson, and Ethan Coffey
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Nuclear and High Energy Physics ,Waveguide (electromagnetism) ,Materials science ,business.industry ,020209 energy ,Mechanical Engineering ,Cyclotron ,Microwave power ,02 engineering and technology ,Electron ,01 natural sciences ,010305 fluids & plasmas ,law.invention ,Power (physics) ,Electric power transmission ,Optics ,Nuclear Energy and Engineering ,law ,Transmission line ,Gyrotron ,0103 physical sciences ,0202 electrical engineering, electronic engineering, information engineering ,General Materials Science ,business ,Civil and Structural Engineering - Abstract
The ITER Electron Cyclotron Heating (ECH) system provides 20 MW of microwave power from 24 gyrotron sources. The power is transmitted through evacuated, corrugated waveguide transmission lines. The...
- Published
- 2017
19. Optimization of microwave-assisted fluidized-bed drying of carrot slices
- Author
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Yvan Gariepy, Xue Hu, Vijaya Raghavan, and Jiby Kurian
- Subjects
0106 biological sciences ,Chromatography ,Blanching ,General Chemical Engineering ,Microwave power ,04 agricultural and veterinary sciences ,040401 food science ,01 natural sciences ,Microwave assisted ,chemistry.chemical_compound ,0404 agricultural biotechnology ,Drying time ,chemistry ,Fluidized bed drying ,010608 biotechnology ,Air temperature ,Physical and Theoretical Chemistry ,Sugar ,Citric acid - Abstract
The drying of carrot slices in a microwave-assisted fluidized-bed drying (MWFBD) system was investigated. The drying conditions such as the initial microwave power density and the inlet air temperature were optimized. The effects of different pretreatment processes such as water blanching, osmotic drying with 20% sugar solution, and 1% citric acid solution on the drying of carrot slices were investigated under the optimized drying conditions. The drying kinetics and the physical properties of the dried carrot slices were analyzed. Different mathematical models of the drying process were explored and fitted to the drying of carrot slices in MWFBD. The pretreatment of the carrot slices reduced the drying time required and improved the qualities such as color and textural strength of the dried carrot slices.
- Published
- 2016
20. Biodiesel production from castor oil using potassium hydroxide as a catalyst: Simulation and validation
- Author
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A. Agatheeshwaren, V. Sivakumar, K. Thirugnanasambandham, and K. Shine
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Potassium hydroxide ,Biodiesel ,Materials science ,ASTM D6751 ,Waste management ,Renewable Energy, Sustainability and the Environment ,020209 energy ,Microwave power ,Energy Engineering and Power Technology ,02 engineering and technology ,Pulp and paper industry ,Catalysis ,chemistry.chemical_compound ,Fuel Technology ,020401 chemical engineering ,Nuclear Energy and Engineering ,chemistry ,Biodiesel production ,Castor oil ,0202 electrical engineering, electronic engineering, information engineering ,medicine ,Response surface methodology ,0204 chemical engineering ,medicine.drug - Abstract
The key objective of the present research is to optimize and investigate the biodiesel production from ricinuscommunis (castor) oil using microwave-assisted hybrid transesterfication process under various conditions such as microwave power, treatment time, ethanol:oil ratio and catalyst concentration (KOH). Response surface methodology (RSM) coupled with four factors with a three-level Box–Behnken response surface design (BBD) was employed to model the transesterfication technique. The obtained results were analyzed by analysis of variance (ANOVA) and a second-order polynomial model was developed to study the interactive effect of process factors on biodiesel production. Derringer’s desired function methodology was used for the optimization and optimum conditions for maximizing the biodiesel production. Under optimum conditions, the predicted biodiesel production was found to be 95% with a desirability value of 0.998. The fuel properties of the produced biodiesel were compared with the ASTM D6751 ...
- Published
- 2016
21. Ultrasonication as pretreatment for drying of tomato slices in a hot air–microwave hybrid oven
- Author
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Erhan Horuz, Hawar Jawdat Jaafar, and Medeni Maskan
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0106 biological sciences ,Waste management ,Vitamin C ,General Chemical Engineering ,Sonication ,Microwave power ,04 agricultural and veterinary sciences ,040401 food science ,01 natural sciences ,Lycopene ,chemistry.chemical_compound ,0404 agricultural biotechnology ,chemistry ,Drying time ,010608 biotechnology ,Food science ,Physical and Theoretical Chemistry ,Microwave - Abstract
This study aims to investigate the effect of ultrasonic pretreatment on drying time and quality properties of tomato slices dried by microwave combined with hot air at 60°C. The influence of ultrasound pretreatment (0, 20, and 40 min) and microwave power (120, 150, and 180 W) on drying time, color, total phenolic content, lycopene, vitamin C, and rehydration capacity of dried slices of tomato was studied. Results showed that as the microwave power level increased, drying time decreased significantly (about 46.4%). Ultrasound pretreatment decreased the drying time by 7.38% only at 120 W microwave power and 40 min of pretreatment compared to those without ultrasound pretreatment at the same microwave power. Depending on drying conditions, vitamin C and lycopene contents reduced from 433.94 to 81.89 mg AA/100 g dry solids and 3920.57 to 415.40 mg/100 g dry solids, respectively. The change in total phenolic content was not severe as much as vitamin C contents. Rehydration capacity of pretreated sample...
- Published
- 2016
22. Degradation of carotenoids in pumpkin (Cucurbita maximaL.) slices as influenced by microwave vacuum drying
- Author
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Lili Meng, Xiaoping Wang, Dajing Li, Jiangfeng Song, and Chunquan Liu
- Subjects
0301 basic medicine ,chemistry.chemical_classification ,030109 nutrition & dietetics ,biology ,organic chemicals ,Microwave power ,food and beverages ,04 agricultural and veterinary sciences ,biology.organism_classification ,040401 food science ,biological factors ,Vacuum drying ,03 medical and health sciences ,0404 agricultural biotechnology ,chemistry ,Color changes ,Botany ,Degradation (geology) ,Air drying ,Food science ,Carotenoid ,Cucurbita maxima ,Microwave ,Food Science - Abstract
The aim of this study was to investigate the influence of microwave vacuum drying on carotenoids in pumpkin (Cucurbita maxima L.) slices. Carotenoids were measured using the reverse-phase high-performance liquid chromatography technique. It was shown that compared with hot air drying, microwave vacuum drying inhibited color changes and significantly (p < 0.05) improved total carotenoid retention (89.1%) in pumpkin slices. During the microwave vacuum drying process, microwave power had an important effect on total carotenoid and all-trans carotenoids. As microwave power increased, the total carotenoid content significantly decreased (p < 0.05), and the levels of individual carotenoids, including all-trans-α-carotene, all-trans-β-carotene, and all-trans-lutein, generally decreased. However, there was an overall upward trend for the levels of 13-cis-β-carotene, 15-cis-β-carotene, 9-cis-β-carotene, and 9-cis-α-carotene. The trans carotenoid quality of the finished products was improved within a certai...
- Published
- 2016
23. Drying behavior of lignite under microwave heating
- Author
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Chuanming Jing, Zhanlong Song, Xiqiang Zhao, Wenlong Wang, Chunyuan Ma, and Liansheng Yao
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Thermogravimetric analysis ,Materials science ,Moisture ,Waste management ,020209 energy ,General Chemical Engineering ,Microwave power ,Metallurgy ,02 engineering and technology ,Inner mongolia ,Microwave heating ,0202 electrical engineering, electronic engineering, information engineering ,Particle size ,Physical and Theoretical Chemistry ,Water content ,Microwave - Abstract
Because of lignite’s high moisture content, it must be dried before most applications. Microwave radiation may be suitable for efficient drying because of its special heating properties. This study investigated the drying behavior of lignite samples from eastern Inner Mongolia by microwave thermogravimetric analysis. Three stages of microwave drying were observed: preheating, fast weight loss, and falling rate drying periods. Samples’ surface temperatures increased dramatically during preheating, dropped slightly in the second period, and rose again in the final period. The measured surface temperature was
- Published
- 2016
24. Testing microwave dewatering as a solution for reducing clay disposal pond areas
- Author
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Ayman A. El-Midany and Hassan El-Shall
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inorganic chemicals ,Engineering ,Flocculation ,Waste management ,Research areas ,business.industry ,General Chemical Engineering ,Microwave power ,04 agricultural and veterinary sciences ,complex mixtures ,040401 food science ,Dewatering ,0404 agricultural biotechnology ,Physical and Theoretical Chemistry ,Processing plants ,business ,Porosity ,Solid content ,Microwave - Abstract
Phosphate processing plants produce an excessive amount of phosphatic clay. This clay represents a serious environmental problem due to their disposal in huge ponds. Finding a feasible method to reduce the clay disposal area is needed. Although the flocculation process, in the presence of fibrous material, seems to be a good dewatering process for phosphatic clay wastes, the maximum solid percentage of flocculated clay does not exceed 18% (starting from 3 to 4%). Recently, the microwave proved a better performance in several research areas as compared to the conventional drying. In this study, clay dewatering by microwave was investigated. Several factors affecting the dewatering process were studied such as heating time, microwave power efficiency, and fiber percentage. Using the microwave, the solid content significantly increases in a reasonably short time. The time and power are the most significant among the studied factors. In addition, sand–clay mix was tested to improve the solid percentag...
- Published
- 2016
25. Continuous tubular microwave heating of homogeneous foods: evaluation of heating uniformity
- Author
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Yngve Hamnerius, Sven Isaksson, Andreas Fhager, Birgitta Wäppling Raaholt, and Lars Hamberg
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0106 biological sciences ,Materials science ,Microwave power ,Metals and Alloys ,04 agricultural and veterinary sciences ,Condensed Matter Physics ,040401 food science ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Cross section (physics) ,0404 agricultural biotechnology ,Homogeneous ,010608 biotechnology ,Excited state ,Microwave heating ,Dielectric heating ,Ceramics and Composites ,Tube (fluid conveyance) ,Electrical and Electronic Engineering ,Composite material ,Microwave - Abstract
A pilot-scale process for continuous in-flow microwave processing of foods, designed and implemented at SP Food and Bioscience, was evaluated for heat treatment of a homogeneous model food for high-temperature short-time (HTST) conditions, at constant total input microwave power, at 2450 MHz. The microwave system has three consecutive cavities, one excited by the TM020 microwave mode that heats primarily in the tube centre, and two TM120 mode cavities that heat primarily in the tube periphery. The temperature uniformity of the homogeneous model food after microwave heating is here evaluated in terms of spatial distribution, for different set-ups of input microwave power in each cavity and for different order of the placement of the cavities, while maintaining the total input microwave power. The microwave heating uniformity is evaluated, based on measured and calculated radial temperature profiles. Combined TM020 and TM120 heating was found to result in more uniform heating by means of spatial temperature uniformity over the tube cross section. Furthermore, appropriately selected microwave power distribution between the centre and periphery heating cavities results in a stable heating profile in the studied food, that differs only about 10 °C or less between highest and lowest average values directly after microwave heating.
- Published
- 2016
26. Optimization and evaluation of microwave-assisted synthesis of magnetite as a carrier for targeted drug delivery system
- Author
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Tushar Raut, Sagar Rahane, Paraag Gide, Birendra Shriwastava, Pankaj Sharma, Gitanjali Deokar, and Kiran Erande
- Subjects
010302 applied physics ,Ferrous sulphate ,Materials science ,General Chemical Engineering ,Metallurgy ,Microwave power ,02 engineering and technology ,Factorial experiment ,021001 nanoscience & nanotechnology ,01 natural sciences ,Microwave assisted ,chemistry.chemical_compound ,Chemical engineering ,Targeted drug delivery ,chemistry ,0103 physical sciences ,Particle size ,0210 nano-technology ,Microwave ,Magnetite - Abstract
The present research work is a novel cost-effective method for synthesis of magnetite. Magnetite is a carrier which is used in the targeted drug delivery system. The conventional methods of preparation of magnetite take around 6–7 h for the completion of reaction; moreover, the particle size of magnetite which we get by the conventional methods is above 5 µm, so the present work aims at preparing magnetite with microwave assistance which has found to reduce reaction time with particle size obtained below 5 µm. The aim of this study was to optimize magnetite synthesis using 23 factorial design by Design-Expert software. Magnetites were synthesized using oxidation of ferrous sulfate. In the next step, the effects of different variables on particle size are studied, including the stirring speed, microwave power (W), and stirring time. Based on the type and the variables studied, eight formulations were designed using factorial design method, and were then prepared, and their particle size was determi...
- Published
- 2015
27. Physical Chemical Properties of Leachate in the Process of Improving Vanadium Leaching From Petroleum Coke: Part II
- Author
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Huang Wenqiang, X. G. Tian, and Yunyun Zhang
- Subjects
Materials science ,General Chemical Engineering ,Microwave power ,Metallurgy ,Petroleum coke ,Energy Engineering and Power Technology ,Vanadium ,chemistry.chemical_element ,General Chemistry ,Raw material ,Geotechnical Engineering and Engineering Geology ,Anode ,Fuel Technology ,chemistry ,Physical chemical ,Leachate ,Leaching (metallurgy) - Abstract
Petroleum coke is the main raw material to produce carbon anode. The content of vanadium in petroleum coke seriously affects the quality of carbon anode. Physical chemical properties of leachate in the process of improving vanadium leaching from petroleum coke were investigated. The effects of different parameters on vanadium removal were chiefly introduced. Systematic studies indicate that the high removal can be achieved under the following conditions: 10 g of petroleum coke, 20 mL of oxidation, 3 h of leaching time, 500 W of microwave power, and 400 mg/L of surfactant amount. Physical chemical properties of leachate changed along with the parameters. This is one reason for the leaching amount of change.
- Published
- 2015
28. Studying different design parameters of a microwave preheating system in solar desalination
- Author
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H. Khafajeh, Ahmad Banakar, and Mohammad Hadi Khoshtaghaza
- Subjects
Chemistry ,Microwave power ,Analytical chemistry ,Ocean Engineering ,02 engineering and technology ,Factorial experiment ,010501 environmental sciences ,Saline water ,01 natural sciences ,Pollution ,Salinity ,020401 chemical engineering ,Volume (thermodynamics) ,0204 chemical engineering ,Solar desalination ,Heating time ,Microwave ,0105 earth and related environmental sciences ,Water Science and Technology - Abstract
An increasing number of microwave radiation applications have led to a large body of research on the effects of microwave radiation on heating. The effect of different design parameters was analyzed on the microwave-induced heating of saline water. In a completely randomized factorial experiment with three replications, effects of four salinity levels (0, 1,000, 10,000, and 30,000 ppm), three volume levels (100, 300, and 500 ml), and three power levels (200, 600, and 1,000 W) on heating time were studied. ANOVA results showed that the effects of power, volume, and salinity as well as all interactions were significant at the 1% level. The heating rate was calculated for heating water from 20 to 90°C. Heating rate varied from 0.0183 to 1.531°C/s, depending on the microwave power, volume and salinity. Results demonstrated that heating rate decreased with increasing salinity and increased with increasing microwave power and volume.
- Published
- 2015
29. Mathematical model for intermittent microwave convective drying of food materials
- Author
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Mohammad U. H. Joardder, Graeme J. Millar, Azharul Karim, Troy W. Farrell, and Chandan Kumar
- Subjects
Physics ,Convection ,business.industry ,General Chemical Engineering ,Microwave power ,Thermodynamics ,04 agricultural and veterinary sciences ,040401 food science ,law.invention ,0404 agricultural biotechnology ,law ,Intermittency ,Heat generation ,Fruits and vegetables ,Mass transfer ,Food material ,Physical and Theoretical Chemistry ,Process engineering ,business ,Microwave - Abstract
Intermittent microwave convective drying (IMCD) is an advanced technology that improves both energy efficiency and food quality in drying. Modelling of IMCD is essential to understand the physics of this advanced drying process and to optimize the microwave power level and intermittency during drying. However, there is still a lack of modelling studies dedicated to IMCD. In this study, a mathematical model for IMCD was developed and validated with experimental data. The model showed that the interior temperature of the material was higher than the surface in IMCD, and that the temperatures fluctuated and redistributed due to the intermittency of the microwave power. This redistribution of temperature could significantly contribute to the improvement of product quality during IMCD. Limitations when using Lambert's Law for microwave heat generation were identified and discussed.
- Published
- 2015
30. Drying Kinetics and Bioactivity of Beetroot Slices Pretreated in Concentrated Chokeberry Juice and Dried with Vacuum Microwaves
- Author
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Małgorzata Serowik, Aneta Wojdyło, Krzysztof Lech, Adam Figiel, Małgorzata Korzeniowska, and Marian Szarycz
- Subjects
Chromatography ,Drying time ,Chemistry ,General Chemical Engineering ,Specific surface area ,Microwave power ,Kinetics ,Physical and Theoretical Chemistry ,Lower temperature ,Microwave - Abstract
Beetroot slices 18 mm in diameter and with a thickness of 9.6, 6.3, 3.35, or 2.6 mm were pretreated in 40°Bx chokeberry juice at a temperature of 50°C for 2 h and then dried by a vacuum-microwave (VM) method at different microwave power levels, such as 120, 240, 360, 480, and 480/120 W. The drying kinetics were described by a fitted model that incorporated contributions from the surface area of the samples, microwave power, and VM processing time. As the microwave power during VM drying increased, the bioactive potential decreased for untreated samples and increased for pretreated samples. Increasing the samples' specific surface area resulted in shorter drying time, lower temperature of the material during drying, and enhanced quality of the dried product. For osmotically pretreated beetroot slices with a specific surface area of 827 ± 18 m2m−3, a final VM drying step at 240 W is recommended to produce high quality vegetable snacks.
- Published
- 2015
31. Microwave drying of wastewater sludge: Experimental and modeling study
- Author
-
Muhammad T. Afzal, Lyes Bennamoun, and Zhenyu Chen
- Subjects
Materials science ,Moisture ,General Chemical Engineering ,Microwave power ,Environmental engineering ,04 agricultural and veterinary sciences ,Thermal diffusivity ,Pulp and paper industry ,040401 food science ,Power level ,Constant rate ,0404 agricultural biotechnology ,Volume (thermodynamics) ,Physical and Theoretical Chemistry ,Microwave ,Shrinkage - Abstract
This study investigates experimentally and using mathematical modeling the microwave drying of wastewater sludge with determination of moisture diffusivity at different drying conditions. The drying behavior was observed at different power levels (480, 840, and 1,080 W) and different initial masses (90, 120, and 150 g). The observed drying kinetics were divided into three parts: a short adaptation period, a long constant drying rate period, and a falling drying rate period. The maximum drying rate was observed during the constant rate period. Mainly, the results show that the drying rate decreases with the initial mass increase (from 0.45 kg·kg−1·min−1 for 90 g to 0.25 kg·kg−1·min−1 for 150 g) and increases with an increase in power level (from 0.15 kg·kg−1·min−1 at 480 W to 0.45 kg·kg−1·min−1 at 1,080 W). The measurement of the sample dimensions shows that shrinkage can occur and, depending on the drying conditions, it ranged between 0.42 and 0.37 of the sample initial volume. Presenting a more a...
- Published
- 2015
32. Effect of processing parameters on the pulsed-spouted microwave vacuum drying of puffed salted duck egg white/starch products
- Author
-
Tao Wang, Min Zhang, Yaping Liu, and Zhongxiang Fang
- Subjects
Chemistry ,Starch ,General Chemical Engineering ,Microwave power ,04 agricultural and veterinary sciences ,medicine.disease ,040401 food science ,Vacuum drying ,chemistry.chemical_compound ,0404 agricultural biotechnology ,Volume expansion ,medicine ,Dehydration ,Food science ,Physical and Theoretical Chemistry ,Water content ,Microwave ,Egg white - Abstract
A puffed food using salted duck egg white and starch as ingredients was produced by using a novel pulsed-spouted microwave vacuum drying (PSMVD) technique. In this study, three types of samples (ratios of salted duck egg white to starch 1:10, 3:10, and 5:10) were prepared and the moisture content of these samples was dehydrated to about 12% in a PSMVD dryer, then the samples were under different microwave powers (1.34 kW, 2.01 kW, and 2.68 kW) for puffing. The product volume expansion ratio, textural crispness (breaking forces), color parameters (L*, a* and b*), and sensory scores were determined. It was observed that microwave power and different ratios of salted duck egg white to starch had a significant effect on the expansion effect of the samples. The results indicated that the best product quality was obtained under the ratio of salted duck egg white to starch at 3:10 and microwave power at 2.01 kW.
- Published
- 2015
33. Drying of Burdock Root Cubes Using a Microwave-Assisted Pulsed Spouted Bed Dryer and Quality Evaluation of the Dried Cubes
- Author
-
Benu Adhikari, Jincai Sun, Xinfeng Cheng, Yi Lu, and Min Zhang
- Subjects
Burdock root ,Chromatography ,Chemistry ,General Chemical Engineering ,Microwave power ,Air drying ,Physical and Theoretical Chemistry ,Cube ,Microwave assisted ,Flavor ,Microwave - Abstract
Burdock cube samples were dried using hot air and microwave pulsed spouted bed drying (MPSBD). Hot air drying was carried out at three temperatures (70, 80, and 90°C). MPSBD was carried out at three microwave power levels (1.0, 2.0, and 3.0 W/g). The results showed that MPSBD samples dried at 2.0 W/g for 30 min and at 1.0 W/g for 40 min had desirable color, flavor, and textural attributes. Gas chromatography–mass spectrometry results showed that the samples dried using MPSBD were richer in flavor compounds, especially in esters, compared to the hot air–dried samples.
- Published
- 2014
34. Freeze Drying of Apple Slices with and without Application of Microwaves
- Author
-
Arun S. Mujumdar, Ruijie Li, Lue-lue Huang, Yu Chuan Wang, and Min Zhang
- Subjects
Freeze-drying ,Dried apple ,Chromatography ,Moisture ,Chemistry ,General Chemical Engineering ,Vacuum pressure ,Microwave power ,Analytical chemistry ,Physical and Theoretical Chemistry ,Microwave assisted ,Water content ,Microwave - Abstract
In this study, Fuji apple slices were dehydrated using freeze drying (FD) combined with microwave assisted with vacuum drying (VMD). The optimal parameter for the diversion point of moisture content from FD to VMD process was at the moisture level of 21%, and for VMD the optimal parameter for vacuum pressure was at 9.15 kPa and microwave power density was at a level of 3.18 w/g. The results show that the two-step technique can significantly reduce total FD time required by up to 40%, while the nutritional value of the dried apple chips remained unchanged compared to FD used alone.
- Published
- 2014
35. Color and Microstructure Properties of Tomatoes Dried by Microwave, Convective, and Microwave-Convective Methods
- Author
-
Nazmi Izli, Esref Isik, Uludağ Üniversitesi/Ziraat Fakültesi/Biyosistem Mühendisliği Bölümü., İzli, Nazmi, Işık, Eşref, and R-7996-2016
- Subjects
Convection ,Scanning electron microscopy (SEM) ,Materials science ,Vacuum ,Scanning electron microscope ,Scanning electron microscopy image ,Analytical chemistry ,Color ,Food science & technology ,Tomato ,Fruits ,Structure (composition) ,Lycopene ,Drying time ,Microwave-convective drying ,Microwaves ,Microstructure ,Drying ,Drying temperature ,Parsley ,Microwave power ,Thin-Layer Drying ,Solar Dryers ,Structure ,Microstructure changes ,Quality ,Microwave power levels ,Microwave heating ,Drying kinetics ,Drying condition ,Microstructure properties ,Scanning electron microscopy ,Microwave ,Food Science - Abstract
In this study, color and microstructure changes of tomato samples were investigated after microwave (90, 160, 350, and 500W), convective (50 and 75 degrees C), and microwave-convective (90W-50 degrees C, 90W-75 degrees C, 160W-50 degrees C, and 160W-75 degrees C) drying treatments using a laboratory microwave-convective oven. The combined microwave-convective drying decreased the drying time required when compared to drying with either convective or microwave drying alone. The color of the samples dried at 50 degrees C was closest to the fresh samples compared to other drying conditions. All color values of fresh tomato were affected by drying. Scanning electron microscopy images showed that disruption of the tomato samples significantly elevated with increasing drying temperature or microwave power level.
- Published
- 2014
36. Influence of Varying Microwave Power during Microwave–Vacuum Drying on the Drying Time and Quality of Beetroot and Carrot Slices
- Author
-
Alicja Kieca and Grzegorz Musielak
- Subjects
Quality (physics) ,Drying time ,Chemistry ,General Chemical Engineering ,Material quality ,Microwave power ,Analytical chemistry ,Physical and Theoretical Chemistry ,Process time ,Pulp and paper industry ,Microwave ,Vacuum drying - Abstract
The aim of this work was to study the influence of microwave power variation during microwave–vacuum drying on both drying time and dried material quality. Red beetroot and carrot were chosen as the material. The quality of the dried material was described by its color change and β-carotene loss (for carrot) due to drying. The first series of experiments consisted of drying under constant microwave power. Only the lowest microwave power gave an undamaged product. During the second series of experiments, the microwave power was changed in time intervals. However, the use of interval conditions either had a small influence on the process time or did not provide satisfactory quality of the dried samples. During the third series of experiments, initial drying was performed with higher microwave power and then the process was continued with the lowest applied power. This method shortened the process time and gave the best quality of material.
- Published
- 2014
37. Comparative SAR Analysis of Some Indian Fruits as per the Revised RF Exposure Guideline
- Author
-
Bhaskar Gupta and Ardhendu Kundu
- Subjects
Electromagnetic field ,business.industry ,Rf exposure ,Microwave power ,Electrical engineering ,Guideline ,Computer Science Applications ,Theoretical Computer Science ,Absorption rate ,Environmental science ,Radio frequency ,Electrical and Electronic Engineering ,Radiation protection ,business ,Microwave ,Remote sensing - Abstract
Specific absorption rate (SAR) is used as the measure of rate at which radio frequency (RF) energy is absorbed by an object when exposed to an electromagnetic field. The word “SAR” is usually associated with the human exposure to RF/microwave energy from different electromagnetic sources and, therefore, SAR limits have been defined only for human by the government of India. ICNIRP (International Commission on Non-Ionizing Radiation Protection) RF exposure guideline was maintained in India up to 31 August 2012, and thereafter Indian government has reduced the maximum permissible RF exposure levels to one-tenth of ICNIRP guideline with effect from 1 September 2012. On the other side, the whole plant kingdom gets exposed to continuous RF electromagnetic field (24 hours a day, 365 days a year) from cell phone towers that transmit high RF/microwave power for radio coverage. High permittivity and loss parameters are observed in most plants, fruits and vegetables due to high water content and ionic conce...
- Published
- 2014
38. Color, Mechanical, and Microstructural Properties of Vacuum Assisted Microwave Dried Saskatoon Berries
- Author
-
S. Avanthika Nagalakshmi, Venkatesh Meda, and Pranabendu Mitra
- Subjects
Lightness ,Materials science ,Vacuum assisted ,Chewiness ,Microwave power ,Analytical chemistry ,Berry ,Response surface methodology ,Food science ,Microstructure ,Microwave ,Food Science - Abstract
Saskatoon berries were dried using a vacuum assisted microwave technique. Central composite rotate design and response surface methodology were used to develop the regression models and to study the influence of drying processing variables (microwave power, drying time, and fruit load) on color, mechanical properties, and microstructure of dried berries. All the three variables had significant effects on the above mentioned properties (p< 0.05). Drying affected the color at variable levels and increased the lightness of dried berries compared to frozen berries. Hardness, gumminess, and chewiness of dried berries increased and springiness and cohesiveness of dried berries decreased with microwave power and drying time. The porosity and the destruction level in the microstructure of dried berries increased with the microwave power. The findings of this study will be useful to identify desirable microwave-vacuum drying operating conditions for targeted dried Saskatoon berry products.
- Published
- 2014
39. Optimization of Potato Cube Drying in a Microwave-Assisted Pulsed Spouted Bed
- Author
-
Yi Lu, Arun S. Mujumdar, Min Zhang, Zheng Dandan, Huihua Liu, and Jincai Sun
- Subjects
Chromatography ,Materials science ,Transition point ,General Chemical Engineering ,Homogeneity (statistics) ,Microwave power ,Physical and Theoretical Chemistry ,Composite material ,Cube ,Water content ,Microwave assisted ,Microwave ,Drying - Abstract
The drying homogeneity of the microwave–pulsed spouted bed drying (MPSBD) method was studied via preparing tubers granules by MPSBD under different predefined conditions. The effects of three parameters (microwave power, moisture content transition point, and loading) on the homogeneity of prepared tubers granules were studied. Based on response surface analysis results, it was concluded that the optimum conditions for tuber granules prepared by MPSBD method is 1.10 W/g microwave power, 80% moisture content transition point, and 90 g material loading. It was proven that the experimental result from the predicted optimal condition agreed with the model-predicted results, which evidenced the accuracy of the response surface analysis. Furthermore, the brighter color and higher rehydration capacity of samples prepared by MPSBD indicates that MPSBD is a promising method that can be applied in the food dehydration industry.
- Published
- 2014
40. A Review on Thin-Layer Drying-Curve Equations
- Author
-
Ibrahim Dincer, Adnan Midilli, Aydin Kilic, and Haydar Kucuk
- Subjects
Air velocity ,Chemistry ,General Chemical Engineering ,Microwave power ,Thin layer ,Analytical chemistry ,Layer thickness ,law.invention ,Pressure measurement ,Excitation amplitude ,law ,Relative humidity ,Physical and Theoretical Chemistry ,Composite material ,Sound wave - Abstract
This paper presents a comprehensive review of thin-layer drying-curve models available in the literature and their comparisons for single-layer drying applications from 2003 to 2013. In this regard, a total of 67 models are selected and classified under 28 performance assessment criteria for comparison purposes. These models are then evaluated by considering the following parameters: (1) product type; (2) pretreatment type; (3) drying parameters, such as temperature, air velocity, layer thickness, microwave power levels, amount of solar radiation, vacum pressure, frequency of sound wave, excitation amplitude, relative humidity, bed depth, product shape, pH, salt content, absolute pressure, etc.; and (4) drying method employed. Furthermore, the best models obtained are employed for product drying applications and compared for different drying methods, drying parameters, and dried products.
- Published
- 2014
41. Optimization of Microwave-Assisted Extraction of Cherry Laurel Fruit
- Author
-
Ivana Karabegović, Miodrag L. Lazić, Saša S. Stojičević, Dragan T. Veličković, and Nada Č. Nikolić
- Subjects
biology ,Chemistry ,Process Chemistry and Technology ,General Chemical Engineering ,Microwave power ,Extraction (chemistry) ,Filtration and Separation ,General Chemistry ,Quadratic function ,Prunus laurocerasus ,biology.organism_classification ,Microwave assisted ,Horticulture ,Yield (chemistry) ,Response surface methodology ,Microwave - Abstract
Response surface methodology was used to optimize the influence of microwave power (300–600 W), plant material-to-solvent ratio (0.05–0.2 g/cm3), and extraction time (10–30 min) on the efficiency of microwave-assisted extraction of the cherry laurel (Prunus laurocerasus L.) fruit. From experimental data, a quadratic polynomial mathematical model (R2 = 0.9949) was developed to predict the extract yield. All considered factors were statistically significant for extraction efficiency, while the most important factor was extraction time. Microwave power of 550 W, plant material-to-solvent ratio of 0.05 g/cm3, and time of 25 min were determined as optimal conditions with a maximum yield of 9.36 g/100 g fresh plant material, which was confirmed through laboratory experiments (9.12 ± 0.61 g/100 g fresh plant material). An economic condition for simultaneous maximum extract yield (7.58 g/100 g fresh plant material) with minimal energy and solvent consumption was determined by the desirability function method (18....
- Published
- 2014
42. Effective Optimization of Temperature Uniformity and Power Efficiency in Two-ports Microwave Ovens
- Author
-
Guo Zhu Jia, Xiao Ling Hu, and Xiao Qing Yang
- Subjects
Materials science ,business.industry ,Microwave oven ,Microwave power ,Metals and Alloys ,Laboratory scale ,Condensed Matter Physics ,Chemical reaction ,Electronic, Optical and Magnetic Materials ,Power (physics) ,Microwave chemistry ,Ceramics and Composites ,Electrical and Electronic Engineering ,Process engineering ,business ,Electrical efficiency ,Microwave - Abstract
Microwave assisted chemical reaction is increasingly studied in recent years by using the modified domestic microwave oven to heating on chemical reaction in the laboratory scale study. But the problems of temperature distribution non-uniformity and low power efficiency in the heating process are becoming a new obstacle in the application of microwave chemistry. An optimized microwave oven with two sources is proposed in this paper from the view of feeding system to overcome these disadvantages. As water is usually concerned as important solvent and reactant, a beaker of water is used as heating load in this study. By modeling the process of heating water for 180 s, the standard deviation and the average temperature are compared between the domestic microwave oven and the optimized microwave oven with two sources. As a result, the power is utilized more efficiently as a 20.14% increase can be seen by using the optimized microwave oven under the same microwave power and more uniformity is obtained ...
- Published
- 2014
43. Microwave synthesis, charaterisation and electrochemical property of cucurbit[n]urils
- Author
-
L. Y. Hu, Qin Yang, Yongli Yang, Jiang Ying, and Li Xiaoli
- Subjects
Materials science ,Infrared ,Mechanical Engineering ,Microwave power ,Analytical chemistry ,Condensed Matter Physics ,Electrochemistry ,symbols.namesake ,Fourier transform ,Mechanics of Materials ,Yield (chemistry) ,Microwave irradiation ,symbols ,General Materials Science ,Cyclic voltammetry ,Microwave - Abstract
Cucurbit[n]urils (CBs) were synthesised using microwave irradiation technique, and the factors to affect the yields of CBs such as total reaction time, interval time and microwave power were investigated. The structure and electrochemical property of CBs were characterised by 1H nuclear magnetic resonance, Fourier transform infrared and cyclic voltammetry. The results showed that CB powder with yield of 85·72% can be obtained under optimal conditions of total reaction time 300 s, heating 1 min with interval 90 s and microwave power 280 W, and electrochemical property of Fe3O4 is intensified significantly after CBs were loaded on the surface of Fe3O4. Surprisingly, compared with the conventional techniques, microwave preparation time of CBs is shortened 60 times.
- Published
- 2013
44. Effects of Magnetron Arrangement and Power Combination of Microwave on Drying Uniformity of Carrot
- Author
-
Shunmin Wang, Yongbin Han, Zhenxin Gu, and Hu Zhichao
- Subjects
Materials science ,business.industry ,General Chemical Engineering ,Microwave power ,Cavity magnetron ,Analytical chemistry ,Optoelectronics ,Physical and Theoretical Chemistry ,business ,Microwave ,Power (physics) - Abstract
The effects of magnetron arrangement and microwave power combination on the drying uniformity of carrot were investigated in this study. The drying uniformity was influenced by magnetron location and quantity. Using one magnetron resuted in poor drying uniformity. However, when two magnetrons were applied, the drying uniformity was 80% after drying for 16 min, which was 93.49% when power combination of three magnetrons at powers of 400, 500, and 600 W were used. The optimal magnetron locations and a suitable microwave power combinations were determined to improve the drying uniformity of carrot.
- Published
- 2013
45. Effect of Drying Conditions and Level of Condensed Distillers Solubles on Protein Quality of Wheat Distillers Dried Grain with Solubles
- Author
-
Lope G. Tabil, Maria Rosario P Mosqueda, and Colleen R. Christensen
- Subjects
Protein content ,Animal feed ingredient ,Chemistry ,General Chemical Engineering ,Air temperature ,Microwave power ,Food science ,Physical and Theoretical Chemistry ,Forced air convection ,Protein quality ,Microwave - Abstract
Reduced protein quality is one of the concerns currently confronting the supply and utilization of wheat distillers dried grain with solubles (DDGS) as an animal feed ingredient. This study assessed the protein quality of wheat DDGS, expressed as acid detergent insoluble crude protein (ADICP) and lysine content, by blending wet distillers grain (WDG) with varying condensed distillers solubles (CDS) levels and drying using forced air convection, microwave, and microwave–convection methods. As the CDS level was increased, the protein content of wheat DDGS generated from the three drying methods increased. Interactions of CDS level with drying air temperature, microwave power, and microwave–convection settings had a significant effect (p
- Published
- 2013
46. Effect of Vacuum, Microwave, and Convective Drying on Selected Parsley Quality
- Author
-
Nuray Akbudak, Bülent Akbudak, Uludağ Üniversitesi/Ziraat Fakültesi/Bahçe Bitkileri Bölümü., Akbudak, Nuray, and Akbudak, Bülent
- Subjects
Chlorophyll ,Convection ,Convective dying ,Meteorology ,Color ,Microwave drying ,Food science & technology ,Atmospheric sciences ,Air temperature ,Chlophyil ,Quality (physics) ,Organic acids ,Heat convection ,Microwave power ,Petroselinum crispum ,Microwaves ,Drying ,Convective drying ,Chemistry ,Air ,Thin-Layer Drying ,Solar Dryers ,Quality attributes ,Carotenoids ,Vacum dying ,Appropriate techniques ,Microwave heating ,Ascorbic acid ,Microwave ,Model ,Vacuum drying ,Food Science - Abstract
This study was conducted to evaluate the quality of and structural changes in parsley (Petroselinum crispum Mill.) during vacuum, microwave, and convective (hot air) drying. The selected quality attributes of the dehydrated parsley samples were investigated on the basis of ascorbic acid and chlorophyll retention, as well as color change and overall appearance. Ascorbic acid is an important indicator of quality, and its selection was due to its heat-labile nature. Ascorbic acid deterioration depends on air temperature, microwave power, and drying time. The lowest ascorbic acid value was found after convective drying, followed by vacuum drying and microwave drying. With convective drying, the appearance values of the dried parsley decreased when the drying period was extended. However, with microwave drying, appearance values were not drastically changed. The color values obtained from leaves supported the chlorophyll findings. At the end of the study, microwave drying at 750-850 W ensured the shortest drying time and the best overall quality of parsley; thus, it was chosen as the most appropriate technique for parsley drying.
- Published
- 2012
47. Optimization of Osmotic Dehydration of Potato Cubes Under Pulsed Microwave Vacuum Environment in Ternary Solution
- Author
-
G. V. S. Raghavan, Suresh Prasad, A. Trivedi, Yvan Gariepy, and P. P. Sutar
- Subjects
chemistry.chemical_compound ,Sucrose ,chemistry ,General Chemical Engineering ,Microwave power ,Composite number ,Analytical chemistry ,Response surface methodology ,Physical and Theoretical Chemistry ,Ternary operation ,Osmosis ,Microwave ,Osmotic dehydration - Abstract
Optimization of the process parameters for osmotic dehydration of 12.2-mm potato cubes was carried out using response surface methodology. The experiments were conducted using a central composite rotatable design (CCRD) with four factors, viz. sucrose concentration (27.5–42.5% w/w), salt concentration (7.5–12.5% w/w), total osmosis time (26.25–68.75 min), and microwave power density for the initial 4 min (0.375–1.125 W/g of total weight of solution and potato cubes) at two levels each to take into account the individual and interaction effects of the factors. A sample-to-solution ratio of 1:10 and pressure of 0.16 kPa for the initial 4 min were kept constant throughout all of the experiments. It was found that the linear effects of all factors on the water loss (WL) and solids gain (SG) were highly significant. The optimum condition was found at a sucrose concentration of 36.35%, salt concentration of 12.50%, osmosis time of 68.72 min, and microwave power density of 0.38 W/g for the initial 4 min, with a ...
- Published
- 2012
48. Microwave-Assisted Spouted Bed Drying of Lettuce Cubes
- Author
-
Jin Cai Sun, Hao Jiang, Yu Fei Feng, and Min Zhang
- Subjects
Freeze-drying ,Chlorophyll content ,Materials science ,Drying time ,Waste management ,General Chemical Engineering ,Air temperature ,Microwave power ,Response surface methodology ,Physical and Theoretical Chemistry ,Composite material ,Microwave assisted ,Microwave - Abstract
Microwave-assisted spouted bed (MSBD) drying of lettuce cubes was investigated experimentally. Response surface methodology was used to optimize the process with spouting air temperature, microwave power level, and superficial air velocity. The dried product obtained was compared with that obtained using other drying technologies such as hot air drying, air spouted bed drying, vacuum microwave drying, and vacuum freeze drying. The comparison is based on the rehydration ratio, chlorophyll content of the product, color, and the drying time required.
- Published
- 2012
49. Preparation of microwave-phosphorylated soy protein isolates through a Box–Behnken model optimization
- Author
-
Yu-Jie Chi and Xi-Bo Wang
- Subjects
Chromatography ,Stability index ,Chemistry ,General Chemical Engineering ,Microwave power ,General Chemistry ,Activity index ,Box–Behnken design ,Industrial and Manufacturing Engineering ,Microwave irradiation ,Response surface methodology ,Soy protein ,Microwave ,Food Science - Abstract
Microwave phosphorylation was applied to modify soy protein isolates (SPI) to improve their emulsifying properties. A Box–Behnken model was obtained to optimize preparation conditions by response surface methodology. The four factors investigated were SPI content, sodium tripolyphosphate (STP) addition, microwave power, and reaction time with the emulsifying activity index (EAI) of the modified product as evaluation index. The optimized conditions were found to be SPI content of 71 g/L, STP addition of 115 g/kg, microwave power of 480 W, and reaction time of 3 min. Under these conditions, the EAI and emulsifying stability index (ESI) of the modified SPI were 0.878 and 33.9 min, respectively. Compared to the original SPI, the EAI and ESI of the modified SPI increased about 113.1% and 26.6%, respectively. Modification of SPI with STP under microwave irradiation might be a potential way to increase the emulsifying properties of SPI.
- Published
- 2012
50. Microwave Freeze Drying of Apple Slices Based on the Dielectric Properties
- Author
-
Guang Yue Ren, Xu Duan, and Wen Xue Zhu
- Subjects
Freeze-drying ,Materials science ,Drying time ,General Chemical Engineering ,Microwave power ,Analytical chemistry ,Dielectric ,Physical and Theoretical Chemistry ,Dissipation ,Composite material ,Water content ,Corona discharge ,Microwave - Abstract
Freeze drying (FD) yields the best quality of dried apple slices but requires a long drying time and is not cost-effective. To mitigate these problems, a microwave freeze drying (MFD) technique was developed to dry apple slices. The relationship between corona discharge and microwave power at various pressures and initial moisture content conditions was studied to avoid the possibility of corona discharge during MFD. It was found that with change of moisture content and temperature of samples during MFD, the dielectric property also changed, which resulted in dynamic microwave dissipation. Based on the dielectric property of samples, a changed microwave loading scheme can lead to perfect product quality and greatly reduce the drying time; thus, MFD can be used to replace the traditional FD technique.
- Published
- 2012
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