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This study examines the movement patterns and comminution of magnetic Ni particles in pure water in a flask. This flask is on top of an actuator which contains a rotating bar magnet, and is surrounded by circulating water at a constant temperature. A digital camera, a particle size analyzer and a field emission electron microscope were adopted to record the moving patterns, particle size distributions and micrographs of magnetic Ni particles. A thermocouple was employed to measure the temperature of pure water in the flask during Ni particle attrition. The effect of the temperature of the water that circulated around the periphery of the flask and the effect of the shape of the flask were analyzed. This study also investigated the effects of the water‐to‐particulate mass ratio and the placement of a bar magnet with an interface between the positive and negative poles in a bar magnet at an inclination angle on the shrinking and the moving pattern of the Ni particles.

The programmed‐temperature‐vaporizing (PTV) injector has been used as a thermal desorption chamber for analysis of volatile sulfur compounds. A trap employing the solid adsorbent Tenax‐TA was used to enrich ambient levels of volatile sulfur compounds, then the sulfur gases were thermally released according to programmed temperature from the adsorbent trap and directly transferred to the system of PLOT‐column gas chromatography/flame‐photometric detector for analysis. The sulfur compounds known to cause nuisance odors in the air from various sewerage treatment tanks of a chemical petroleum company are determined.